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The International Journal of Advanced Manufacturing Technology

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31-08-2022 | ORIGINAL ARTICLE

Effect of milling time on the structural, microstructure, and magnetic properties of nanocrystalline Fe₉₀Sb₁₀ powders obtained by high-energy ball milling

Authors: Nassima Guemmoud, Ali Hafs, Toufik Hafs

Published in: The International Journal of Advanced Manufacturing Technology | Issue 3-4/2022

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Abstract

Nanocrystalline binary powders Fe₉₀Sb₁₀ (wt.%) have been elaborated by high-energy ball milling in order to study the effect of the milling time on the microstructural and magnetic properties of these alloys. The evolution of structural, morphological, and magnetic properties was investigated, as a function of milling time, using X-ray diffraction (XRD), scanning electron microscopy (SEM) coupled with energy-dispersive X-ray spectrometry (EDX), and the vibrating sample magnetometer (VSM). A disordered Fe (Sb) solid solution with body-centered cubic (bcc) crystal structure is formed after 12 h of milling from XRD results. When the milling time increases, the lattice parameter progressively increases from 0.2861 for the Fe₉₀Sb₁₀ (0 h milling) compound down to 0.2870 nm for 36 h of milling. The sample with the longest milling time has exhibited the lowest value for the mean grain size of 18.16 nm as well as the microstrain of 0.19%. Grain morphology of the powders at different formation stages was examined using scanning electron microscopy (SEM). The chemical composition homogeneity and the powder form Fe₉₀Sb₁₀ (wt.%) were studied with EDX experiments. For Fe-10Sb (wt.%) nanostructured powders, magnetisation saturation, coercive fields, and remnant magnetisation derived from the hysteresis curves were discussed as a function of milling time.

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Suryanarayana C (2005) Recent developments in nanostructured materials. Adv Eng Mater 7:983. https://doi.org/10.1002/adem.200500135CrossRef

Kang W-K, Yılmaz F, Kim H-S, Koo J-M, Hong S-J (2012) Fabrication of Al–20 wt %Si powder using scrap Si by ultra high-energy milling process. J Alloys Compd 536:S45–S49. https://doi.org/10.1016/j.jallcom.2012.01.106CrossRef

Gleiter H (2000) Nanostructured materials: basic concepts and microstructure. Acta mater 48:1. https://doi.org/10.1016/S1359-6454(99)00285-2CrossRef

Fogagnolo J, Velasco F, Robert M, Torralba J (2003) Effect of mechanical alloying on the morphology, microstructure and properties of aluminium matrix composite powders. Mater Sci Eng A 342:131–143. https://doi.org/10.1016/S0921-5093(02)00246-0CrossRef

Polkin IS, Borzov AB (1995) New materials produced by mechanical alloying. Adv Perform Mater 2:99–109. https://doi.org/10.1007/BF00711655CrossRef

Benjamin JS (1970) Dispersion strengthened superalloys by mechanical alloying. Metall Trans 1:2943–2951. https://doi.org/10.1007/BF03037835CrossRef

Znaidi L (2010) Sol–gel-deposited ZnO thin films: a review. Mater Sci Eng B 174:18–30. https://doi.org/10.1016/j.mseb.2010.07.001CrossRef

Jing Xu, Yang H, Wuyou Fu, Kai Du, Sui Y, Chen J, Zeng Yi, Li M, Zou G (2007) Preparation and magnetic properties of magnetite nanoparticles by sol–gel method. J Magn Magn Mater 309:307–311. https://doi.org/10.1016/j.jmmm.2006.07.037CrossRef

Zhang D, Ye K, Yao Y, Liang F, Qu T, Ma W, Yang B, Dai Y, Watanabe T (2019) controllable synthesis of carbon nanomaterials by direct current arc discharge from the inner wall of the chamber. Carbon 142:278–284. https://doi.org/10.1016/j.carbon.2018.10.062CrossRef

10.

Wu Q, Wongwiriyapan W, Park J-H, Park S, Jung SJ, Jeong T, Lee S, Lee YH, Song YJ (2016) In situ chemical vapor deposition of graphene and hexagonal boron nitride heterostructures. Curr Appl Phys 16:1175–1191. https://doi.org/10.1016/j.cap.2016.04.024CrossRef

11.

Son HH, Seo GH, Jeong U, Shin DY, Kim SJ (2017) Capillary wicking effect of a Cr-sputtered superhydrophilic surface on enhancement of pool boiling critical heat flux. Int J Heat Mass Transfer 113:115–128. https://doi.org/10.1016/j.ijheatmasstransfer.2017.05.055CrossRef

12.

Poolakkandy RR, Menamparambath MM (2020) Soft-template-assisted synthesis: a promising approach for the fabrication of transition metal oxides. Nanoscale Adv 2:5015–5045. https://doi.org/10.1039/D0NA00599ACrossRef

13.

Zhuang S, Lee ES, Lei L, Nunna BB, Kuang L, Zhang W (2016) Synthesis of nitrogen-doped graphene catalyst by high-energy wet ball milling for electrochemical systems. Int J Energy Res 40:2136–2149. https://doi.org/10.1002/er.3595CrossRef

14.

Koch CC (1997) Synthesis of nanostructured materials by mechanical milling: problems and opportunities. Nanostruct Mater 9(1–8):13–22. https://doi.org/10.1016/S0965-9773(97)00014-7CrossRef

15.

Hasnaouia N, Hafs A, Hafs T, Bendjedaa F (2022) Structural, microstructural characterisation and magnetic properties of nanocrystalline Fe-10 wt% Pb alloy powders synthesised by mechanical alloying process. J Alloys Compd 899:163338. ISSN 0925–8388. https://doi.org/10.1016/j.jallcom.2021.163338

16.

Ambrose T, Gavrin A, Chien CL (1993) Magnetic properties of metastable fcc Fe-Cu alloys prepared by high energy ball milling. J Magn Magn Mater 124(1–2):15–19. ISSN 0304–8853. https://doi.org/10.1016/0304-8853(93)90063-8

17.

Suryanarayana C (2001) Mechanical alloying and milling. Prog Mater Sci 46(1–2):1–184. ISSN 0079–6425. https://doi.org/10.1016/S0079-6425(99)00010-9

18.

Khajepour M, Sharafi S (2011) Structural and magnetic properties of nanostructured Fe50(Co50)–6.5wt% Si powder prepared by high energy ball milling. J Alloys Compd 509(29):7729–7737. ISSN 0925–8388. https://doi.org/10.1016/j.jallcom.2011.04.095

19.

Bahrami A, Hosseini HRM, Abachi P, Miraghaei S (2006) Structural and soft magnetic properties of nanocrystalline Fe85Si10Ni5 powders prepared by mechanical alloying. Mater Lett 60(8):1068–1070. ISSN 0167–577X. https://doi.org/10.1016/j.matlet.2005.10.078

20.

Froes FHS, Suryanarayana C, Russell K, Li C-G (1995) Synthesis of intermetallics by mechanical alloying. Mater Sci Eng A 192–193(Part 2):612–623. ISSN 0921–5093. https://doi.org/10.1016/0921-5093(94)03285-8

21.

Bhoi B, Srinivas V, Singh V (2010) Evolution of microstructure and magnetic properties of nanocrystalline Fe70−xCuxCo30 alloy prepared by mechanical alloying. J Alloys Compd 496(1–2):423–428. ISSN 0925–8388. https://doi.org/10.1016/j.jallcom.2010.01.155

22.

Wang W, Lu Y, Qin H, Wei B (2009) Dendrite growth characteristics within liquid Fe-Sb alloy. Sci China Ser G-Phys Mech Astron 52(5):720–728. https://doi.org/10.1007/s11433-009-0100-7CrossRef

23.

Kis-Varga M, Beke DL, Mészáros S, Vad K, Kerekes G, Daróczi L (1998) Mechanical alloying and magnetic properties of Fe₉₀ Sb₁₀ and Fe₁₅ Sb₈₅ systems. Mater Sci Forum 269–272:961–968. https://doi.org/10.4028/www.scientificmetMSF269-272.961

24.

Lutterotti L (2000) Laboratorio Scienza e Tecnologia dei Materiali. Universita di Torino, Corso

25.

Rietveld HM (1969). J Appl Crystallogr. https://doi.org/10.1107/S0021889869006558CrossRef

26.

Scherrer P (1918) nachrichten von der Gesellschaft der Wissenschaften, Gottingen, Mathematisch- Physikalische Klasse

27.

Stokes AR, Wilson AJC (1994) I Proc Phys Soc Lond

28.

Branger V, Briand E, Kusmeruck C, Morin N, Corot F, Auburtin Ph (2002) J Phys IV France 12:165. https://doi.org/10.1051/jp4:20020224CrossRef

29.

Boukherroub N, Guittoum A, Souami N, Akkouche K, Boutarfaia S (2012) EPJ web of conferences 29:00010. https://doi.org/10.1051/epjconf/20122900010CrossRef

30.

Avar B, Gogebakan M, Ozcan S, Kerli S (2014) Structural, mechanical and magnetic properties of Fe – 40-at% Al powders during mechanical alloying. J Korean Phys Soc. https://doi.org/10.3938/jkps.65.664CrossRef

31.

Kezrane M, Guittoum A, Boukherroub N, Lamrani S, Sahraoui T (2012) J Alloy Compd 536:S304. https://doi.org/10.1016/j.jallcom.2011.11.043CrossRef

32.

Ryu J, Hong SH, Baek WH (1997) Mechanical alloying process of 93W–5.6Ni-1.4Fe tungsten heavy alloy. J Mater Process Technol 63:292–297. https://doi.org/10.1016/S0924-0136(96)02638-6CrossRef

33.

Kezrane M, Guittoum A, Boukherroub N, Lamrani S, Sahraoui ST (2012) Mössbauer and X-ray diffraction studies of nanostructured Fe₇₀Al₃₀ powders elaborated by mechanical alloying. J Alloy Compd. https://doi.org/10.1016/j.jallcom.2011.11.043CrossRef

34.

Benjamin JS, Volin TE (1974) The mechanism of mechanical alloying. Metall Mater Trans. https://doi.org/10.1007/BF02644161CrossRef

35.

Davis RM, Mc Dermont B, Koch CC (1988) Mechanical alloying of brittle materials. Met Trans A 19:2867–2874. https://doi.org/10.1007/BF02647712CrossRef

36.

Djekoun A, Otmani A, Bouzabata B, Bechiri L, Randrianantoandro N, Greneche JM (2006) Synthesis and characterization of high-energy ball milled nanostructured Fe₅₀Ni₅₀. Catal Today 113:235–239. https://doi.org/10.1016/j.cattod.2005.11.084CrossRef

37.

Arunkumar S, Kumaravel P, Velmurugan C, Senthilkumar V (2018) Microstructures and mechanical properties of nanocrystalline NiTi intermetallics formed by mechanosynthesis. Int J Miner Metall Mater 25(1):80–87. https://doi.org/10.1007/s12613-018-1549-zCrossRef

38.

Mhadhbi M, Khitouni M, Escoda L, Sunol JJ, Dammak M (2010) Characterization of mechanically alloyed nanocrystalline Fe(Al): crystallite size and dislocation density. J Nanomater. https://doi.org/10.1155/2010/712407CrossRef

39.

Alleg S, Kartout S, Ibrir M, Azzaza S, Fenineche NE, Suñol JJ (2013) Magnetic, structural and thermal properties of the Finemet-type powders prepared by mechanical alloying. J Phys Chem Solids 74:550. https://doi.org/10.1016/j.jpcs.2012.12.002CrossRef

40.

Chater R, Bououdina M, Chaanbi D, Abbas H (2013) Synthesis and magnetization studies of nanopowder Fe₇₀Ni₂₀Cr₁₀ alloys prepared by high energy milling. J Solid State Chem 201:317. https://doi.org/10.1016/j.jssc.2013.02.028CrossRef

41.

Blanco DM, Gorria P, Blanco JA (2006) Nanostructured Fe obtained by high-energy ball milling. J Magn Magn Mater 300:e339. https://doi.org/10.1016/j.jmmm.2005.10.115CrossRef

42.

Shokrollahi H (2009) The magnetic and structural properties of the most important alloys of iron produced by mechanical alloying. Mater Des 30:3374. https://doi.org/10.1016/j.matdes.2009.03.035CrossRef

43.

Zeng Q, Baker I, McCreary V, Yan Z (2007) Soft ferromagnetism in nanostructured mechanical alloying FeCo-based powders. J Magn Magn Mater 318:28. https://doi.org/10.1016/j.jmmm.2007.04.037CrossRef

44.

Skjerpe P (1987) Intermetallic phases formed during DC-casting of an Al−0.25 Wt Pct Fe−0.13 Wt Pct Si alloy. Metall Trans A 18(1):189. https://doi.org/10.1007/BF02825700CrossRef

45.

Qamar S, Akhtar MN, Batoo KM, Raslan EH (2020) Structural and magnetic features of Ce doped Co-Cu-Zn spinel nanoferrites prepared using sol gel self-ignition method. Ceram Int 46:14487. https://doi.org/10.1016/j.ceramint.2020.02.246CrossRef

46.

Inoue K, Shima H, Fujita A, Ishida K (2006) Temperature dependence of magnetocrystalline anisotropy constants in the single variant state of L1₀-type FePt bulk single crystal. Appl Phys Lett 88:102503. https://doi.org/10.1063/1.2177355CrossRef

47.

Zener C (1954) Classical theory of the temperature dependence of magnetic anisotropy energy. Phys Rev 96:1335. https://doi.org/10.1103/PhysRev.96.1335CrossRef

48.

Callen ER, Callen HB (1966) The present status of the temperature dependence of magnetocrystalline anisotropy, and l(l+2) the power law. J Phys Chem Solids 27:1271. https://doi.org/10.1016/0022-3697(66)90012-6CrossRef

Title: Effect of milling time on the structural, microstructure, and magnetic properties of nanocrystalline Fe90Sb10 powders obtained by high-energy ball milling
Authors: Nassima Guemmoud
Ali Hafs
Toufik Hafs
Publication date: 31-08-2022
Publisher: Springer London
Published in: The International Journal of Advanced Manufacturing Technology / Issue 3-4/2022
Print ISSN: 0268-3768
Electronic ISSN: 1433-3015
DOI: https://doi.org/10.1007/s00170-022-10003-x

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