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Journal of Materials Science: Materials in Electronics
Published in: Journal of Materials Science: Materials in Electronics 11/2017

22-02-2017

Effect of sintering temperature on morphology, dielectric and ferroelectric properties of five layer Aurivillius oxides: A2Bi4Ti5O18 (A=Ba, Pb and Sr) synthesized by co-precipitation route

Authors: Shivangi Dubey, Rajnish Kurchania

Published in: Journal of Materials Science: Materials in Electronics | Issue 11/2017

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Abstract

Polycrystalline ceramics with chemical formula Ba2Bi4Ti5O18, Pb2 Bi4Ti5O18 and Sr2Bi4Ti5O18 have been synthesized using co-precipitation route. In the present study optimization of calcination and sintering temperature is carried out and the relationship between sintering temperature and morphology, dielectric, and ferroelectric properties of the as-prepared samples is extensively investigated. Pellets of these samples were sintered at a range of temperatures 850, 950 and 1050 °C for 2 h. The phase formation of compounds calcined at different temperatures was studied using X-ray diffraction and scanning electron microscopy was used to examine the surface morphology. Crystallite and grain size was seen to increases with an increase in the calcination and sintering temperature respectively. The dielectric and ferroelectric properties of the ceramics were found to improve at a higher sintering temperature.
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Metadata
Title
Effect of sintering temperature on morphology, dielectric and ferroelectric properties of five layer Aurivillius oxides: A2Bi4Ti5O18 (A=Ba, Pb and Sr) synthesized by co-precipitation route
Authors
Shivangi Dubey
Rajnish Kurchania
Publication date
22-02-2017
Publisher
Springer US
Published in
Journal of Materials Science: Materials in Electronics / Issue 11/2017
Print ISSN: 0957-4522
Electronic ISSN: 1573-482X
DOI
https://doi.org/10.1007/s10854-017-6540-3

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