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Published in: Journal of Sol-Gel Science and Technology 3/2019

16-03-2019 | Original Paper: Sol–gel and hybrid materials for dielectric, electronic, magnetic and ferroelectric applications

Effect of the processing temperature on the electrical properties of lead-free 0.965Bi0.5Na0.5TiO3–0.035BaTiO3 piezoelectric ceramics synthesized by sol–gel method

Authors: Muhammad Munir, Muhammad Habib, Salman Ali Khan, Ali Hussain, Ibrahim Qazi, Yeon Bin Choi, Jeong-Hun Son, Rizwan Ahmad Malik, Dong-Sik Bae

Published in: Journal of Sol-Gel Science and Technology | Issue 3/2019

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Abstract

In this work, lead-free 0.965Bi0.5Na0.5TiO3–0.035BaTiO3 (BNT–BT) piezoelectric ceramics were synthesized by a sol–gel process. X-ray diffraction pattern of the BNT–BT samples revealed that powder calcined at 600 °C, exhibit a pure perovskite structure. Scanning electron microscopy (SEM) was used to find the surface morphology and grain size of the investigated ceramics. At an optimized sintering temperature of 1150 °C, well-saturated ferroelectric (PE) hysteresis loops with high remnant polarization (Pr = 34.8 µC/cm2) and low corrosive field (Ec = 23 kV/cm) were obtained. Electric field-induced strain of 0.137% with a dynamic piezoelectric coefficient (d33* = 196 pm/V) was observed under 75 kV/cm drawing field. In addition, high static piezoelectric constant (d33 = 138 pC/N) was recorded for the sample sintered at 1150 °C. This value of d33 is comparable to that of BNT-based bulk piezoelectric ceramics.

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Metadata
Title
Effect of the processing temperature on the electrical properties of lead-free 0.965Bi0.5Na0.5TiO3–0.035BaTiO3 piezoelectric ceramics synthesized by sol–gel method
Authors
Muhammad Munir
Muhammad Habib
Salman Ali Khan
Ali Hussain
Ibrahim Qazi
Yeon Bin Choi
Jeong-Hun Son
Rizwan Ahmad Malik
Dong-Sik Bae
Publication date
16-03-2019
Publisher
Springer US
Published in
Journal of Sol-Gel Science and Technology / Issue 3/2019
Print ISSN: 0928-0707
Electronic ISSN: 1573-4846
DOI
https://doi.org/10.1007/s10971-018-04913-0

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