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Metallurgical and Materials Transactions A
Published in: Metallurgical and Materials Transactions A 9/2015

01-09-2015

Evolution of Minor Phases in a 9PctCr Steel: Effect of Tempering Temperature and Relation with Hydrogen Trapping

Authors: Carolina Hurtado-Noreña, Claudio Ariel Danón, María Inés Luppo, Pablo Bruzzoni

Published in: Metallurgical and Materials Transactions A | Issue 9/2015

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Abstract

The evolution of minor phases in ASTM A335 P91 steel has been studied on specimens submitted to different thermal treatments including a tempering step. Particular emphasis has been put on the tempering temperature range 573 K to 873 K (300 °C to 600 °C), which has not been yet intensively studied. The techniques used in this investigation were X-ray diffraction with synchrotron light, scanning electron microscopy with field emission gun and transmission electron microscopy. In the low tempering temperature range [573 K to 673 K (300 °C to 400 °C)], retained austenite, Fe3C and MX precipitates are observed. In the high tempering temperature range [773 K to 1053 K (500 °C to 780 °C)], M23C6-type carbides, MX-type carbonitrides and M2X precipitates are observed. The effect of the microstructure on hydrogen trapping is analyzed. The distorted matrix around the M2X and MX particles provides the most important trap sites in the P91 steel.
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Metadata
Title
Evolution of Minor Phases in a 9PctCr Steel: Effect of Tempering Temperature and Relation with Hydrogen Trapping
Authors
Carolina Hurtado-Noreña
Claudio Ariel Danón
María Inés Luppo
Pablo Bruzzoni
Publication date
01-09-2015
Publisher
Springer US
Published in
Metallurgical and Materials Transactions A / Issue 9/2015
Print ISSN: 1073-5623
Electronic ISSN: 1543-1940
DOI
https://doi.org/10.1007/s11661-015-3045-7

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