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Glass and Ceramics
Published in: Glass and Ceramics 1-2/2013

01-05-2013 | Science for Ceramic Production

Formation of Open Porosity Materials Based on Nickel, Aluminum and Cobalt in Self-Propagating High-Temperature Synthesis in Vacuum

Authors: V. I. Uvarov, I. P. Borovinskaya, E. S. Lukin

Published in: Glass and Ceramics | Issue 1-2/2013

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Abstract

As a result of a calculation of the influence of the volume effect of a chemical reaction on the porosity of the final product for the system Al–Ni–Co in vacuum it is shown that the porosity of the synthesized material will be 7.6% higher than the initial porosity Po of the starting sample. For synthesis of SHS material with open porosity the initial batch powders were mixed in a ball mill with Al2O3 balls for 1 h. The ready batch was poured into a graphite mold, which was placed into a vacuum furnace, and the batch temperature was raised to the self-inflammation temperature, after which spontaneous combustion of the batch occurred. Phase analysis of the samples, performed with a DRON-3M diffractometer, showed the presence of the main phase (CoNi)3Ni and free Ni. The pore size of the samples obtained was 2 – 2.5 μm. The open porosity of the samples, determined by hydrostatic weighing, was 42%.
previous article Computational Methods for Determining the Effect of Stress on Cutting Quality1
next article Structural Changes on Heating and High-Temperature Deformation of Composites Based on Pyrophyllite Raw Material from the Kul’-Yurt-Tau Deposit

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Metadata
Title
Formation of Open Porosity Materials Based on Nickel, Aluminum and Cobalt in Self-Propagating High-Temperature Synthesis in Vacuum
Authors
V. I. Uvarov
I. P. Borovinskaya
E. S. Lukin
Publication date
01-05-2013
Publisher
Springer US
Published in
Glass and Ceramics / Issue 1-2/2013
Print ISSN: 0361-7610
Electronic ISSN: 1573-8515
DOI
https://doi.org/10.1007/s10717-013-9499-4

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