1 Introduction
2 Experimental procedures
2.1 Base materials
2.2 MPEA production
Sample | Al | Cr | Fe | Ni | Ti | Co | Mo | Nb |
---|---|---|---|---|---|---|---|---|
Al [ma.-%] | 99.70 | 0.00 | 0.00 | 0.00 | 0.00 | 0.00 | 0.00 | 0.00 |
Cr [ma.-%] | 0.38 | 99.24 | 0.14 | 0.00 | 0.00 | 0.00 | 0.00 | 0.00 |
Ti [ma.-%] | 0.00 | 0.00 | 0.20 | 0.00 | 99.50 | 0.00 | 0.00 | 0.00 |
W722 [ma.-%] | 0.00 | 0.00 | 66.90 | 18.00 | 1.00 | 9.25 | 4.85 | 0.00 |
L718 [ma.-%] | 0.50 | 18.00 | 18.50 | 53.68 | 0.95 | 0.00 | 3.00 | 5.30 |
MPEA5 [mol%] | 19.21 | 19.21 | 19.21 | 19.21 | 19.21 | 1.77 | 1.11 | 0.98 |
MPEA_Ti10 [mol%] | 21.41 | 21.41 | 21.41 | 21.41 | 10.00 | 1.97 | 1.24 | 1.09 |
2.3 Dilatometry
2.4 In situ synchrotron X-ray diffraction
2.5 Strain analysis
2.6 Microstructure and properties analyses
3 Results and discussion
3.1 Macroscopic stress–strain development of MPEA5 and MPEA_Ti10
3.2 Detected phases in MPEA5 and MPEA_Ti10
3.3 Lattice-dependent elastic moduli as function of macro stress in MPEA5
3.4 Lattice-dependent elastic moduli as function of macro stress in MPEA_Ti10
3.5 Lattice strain in dependence of phases in MPEA5 and MPEA_Ti10
Phase | Plane | Stage | \(E_{{\mathrm {hkl}}}\) (GPa) | (\(E_{\mathrm {hkl,} j}-E_{\mathrm {hkl, I}})/E_{\mathrm {hkl, I}}\) (%) | \(\nu _{{\mathrm {hkl}}}\) (–) |
---|---|---|---|---|---|
H_L21 | 220 | I | 211.8 ± 0.7 | 0.0 | 0.254 ± 0.002 |
II | 151.2 ± 1.3 | \(-\) 28.6 | 0.265 ± 0.012 | ||
III | 141.8 ± 1.1 | \(-\) 33.0 | 0.252 ± 0.004 | ||
400 | I | 165.9 ± 0.6 | 0.0 | 0.305 ± 0.002 | |
II | 128.1 ± 1.1 | \(-\) 22.8 | 0.336 ± 0.014 | ||
III | 111.4 ± 1.0 | \(-\) 32.8 | 0.317 ± 0.006 | ||
422 | I | 206.1 ± 0.7 | 0.0 | 0.250 ± 0.002 | |
II | 159.1 ± 1.4 | \(-\) 22.8 | 0.274 ± 0.013 | ||
III | 143.6 ± 1.2 | \(-\) 30.3 | 0.259 ± 0.004 | ||
BCC | 110 | I | 293.4 ± 2.8 | 0.0 | 0.372 ± 0.008 |
II | 202.7 ± 2.1 | \(-\) 30.9 | 0.303 ± 0.020 | ||
III | 142.1 ± 3.8 | \(-\) 51.6 | 0.237 ± 0.011 | ||
200 | I | 301.5 ± 4.0 | 0.0 | 0.348 ± 0.010 | |
II | 142.4 ± 1.9 | \(-\) 52.8 | 0.212 ± 0.019 | ||
III | 156.0 ± 2.0 | \(-\) 48.3 | 0.237 ± 0.010 | ||
211 | I | 232.3 ± 0.7 | 0.0 | 0.285 ± 0.003 | |
II | 182.0 ± 1.3 | \(-\) 21.7 | 0.305 ± 0.016 | ||
III | 158.1 ± 1.8 | \(-\) 32.0 | 0.260 ± 0.008 | ||
C14 | 110 | I | 207.2 ± 3.3 | 0.0 | 0.314 ± 0.029 |
II | 148.9 ± 9.8 | \(-\) 28.1 | 0.417 ± 0.078 | ||
III | 144.2 ± 5.4 | \(-\) 30.4 | 0.375 ± 0.089 | ||
103 | I | 195.0 ± 1.8 | 0.0 | 0.298 ± 0.016 | |
II | 166.0 ± 3.7 | \(-\) 14.9 | 0.338 ± 0.039 | ||
III | 137.0 ± 2.6 | \(-\) 29.7 | 0.285 ± 0.027 | ||
302 | I | 192.5 ± 0.6 | 0.0 | 0.283 ± 0.003 | |
II | 143.4 ± 1.6 | \(-\) 25.5 | 0.282 ± 0.013 | ||
III | 108.0 ± 2.1 | \(-\) 43.9 | 0.223 ± 0.009 |
Phase | Plane | Stage | \(E_{{\mathrm {hkl}}}\) (GPa) | (\(E_{\mathrm {hkl,} j}-E_{\mathrm {hkl, I}})/E_{\mathrm {hkl, I}}\) (%) | \(\nu _{{\mathrm {hkl}}}\) (–) |
---|---|---|---|---|---|
H_L21 | 220 | I | 225.5 ± 0.4 | 0.0 | 0.231 ± 0.002 |
II | 238.0 ± 0.9 | 5.6 | 0.255 ± 0.002 | ||
III | 206.7 ± 3.0 | \(-\) 8.4 | 0.248 ± 0.007 | ||
400 | I | 164.9 ± 0.2 | 0.0 | 0.321 ± 0.002 | |
II | 180.7 ± 1.0 | 9.6 | 0.316 ± 0.004 | ||
III | 164.1 ± 0.9 | \(-\) 0.5 | 0.344 ± 0.006 | ||
422 | I | 211.6 ± 0.4 | 0.0 | 0.263 ± 0.002 | |
II | 239.5 ± 1.1 | 13.2 | 0.262 ± 0.003 | ||
III | 211.5 ± 1.3 | \(-\) 0.1 | 0.263 ± 0.004 | ||
BCC | 110 | I | 283.5 ± 1.5 | 0.0 | 0.249 ± 0.006 |
II | 333.0 ± 2.1 | 17.5 | 0.306 ± 0.015 | ||
III | 257.5 ± 3.4 | \(-\) 9.2 | 0.197 ± 0.011 | ||
200 | I | 266.1 ± 4.8 | 0.0 | 0.352 ± 0.012 | |
II | 224.9 ± 3.1 | \(-\) 15.5 | 0.233 ± 0.006 | ||
III | 235.8 ± 1.8 | \(-\) 11.4 | 0.308 ± 0.009 | ||
211 | I | 238.2 ± 0.4 | 0.0 | 0.263 ± 0.004 | |
II | 276.0 ± 2.7 | 15.9 | 0.304 ± 0.005 | ||
III | 250.8 ± 1.8 | 5.3 | 0.315 ± 0.006 | ||
C14 | 110 | I | 235.3 ± 3.7 | 0.0 | 0.286 ± 0.018 |
II | 265.3 ± 5.5 | 12.7 | 0.308 ± 0.024 | ||
III | 242.7 ± 6.7 | 3.1 | 0.312 ± 0.036 | ||
103 | I | 216.1 ± 1.6 | 0.0 | 0.276 ± 0.008 | |
II | 283.4 ± 3.7 | 31.1 | 0.295 ± 0.010 | ||
III | 238.5 ± 5.8 | 10.4 | 0.336 ± 0.031 | ||
302 | I | 189.7 ± 1.3 | 0.0 | 0.303 ± 0.005 | |
II | 229.1 ± 1.6 | 20.7 | 0.390 ± 0.009 | ||
III | 195.0 ± 1.8 | 2.8 | 0.282 ± 0.011 |