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Journal of Materials Science
Published in: Journal of Materials Science 19/2018

24-04-2018 | Mechanochemical Synthesis

On the influence of water on the mechanochemical synthesis of low F-doped Al-hydroxide fluorides

Authors: V. Scalise, G. Scholz, E. Kemnitz

Published in: Journal of Materials Science | Issue 19/2018

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Abstract

The significant role played by water in the mechanochemical synthesis of highly distorted aluminum hydroxide fluorides is on the main focus of this research paper. The importance of water in the synthesis was evaluated considering separately combinations of O/OH sources (Al(OH)3, Al2O3) and fluorine sources with or without structural water (β-AlF3.3H2O, α-AlF3). Each system was studied by typical bulk and surface characterization techniques (XRD, MAS NMR, DTA-TG, NH3-TPD) and compared to each other in order to gain a more comprehensive insight of the importance of including water in the synthesis of amorphous aluminum hydroxide fluorides.
previous article Mechanochemical preparation of nanocrystalline metal halide phosphors
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Appendix
Available only for authorised users
Literature
1.
Dhand C, Dwivedi N, Loh XJ, Ying ANJ, Verma NK, Beuerman RW, Lakshminarayanan R, Ramakrishna S (2015) Methods and strategies for the synthesis of diverse nanoparticles and their applications: a comprehensive overview. RSC Adv 5:105003–105037CrossRef
2.
Düvel A, Romanova E, Sharifi M, Freude D, Wark M, Heitjans P, Wilkening M (2011) Mechanically induced phase transformation of γ-Al2O3 into α-Al2O3. Access to structurally disordered γ-Al2O3 with a controllable amount of pentacoordinated Al Sites. J Phys Chem C 115:22770–22780CrossRef
3.
Mackenzie KJD, Temuujin J, Smith ME, Angerer P, Kameshima Y (2000) Effect of mechanochemical activation on the thermal reactions of boehmite (γ-AlOOH) and γ-Al2O3. Thermochim Acta 359:87–94CrossRef
4.
Mackenzie KJD, Temuujin J, Okada K (1999) Thermal decomposition of mechanically activated gibbsite. Thermochim Acta 327:103–108CrossRef
5.
Pflitsch C, Siddiqui RA, Eckert C, Atakan B (2008) Sol–gel deposition of chromium doped aluminium oxide films (ruby) for surface temperature sensor application. Chem Mater 12:2773–2778CrossRef
6.
Yao M, Xiao R, Peng Y, Chen J, Hu B, Yao X (2015) The influence of titanium doping on the electric properties of amorphous alumina films prepared by sol–gel technology. J Sol-Gel Sci Technol 74:39–44CrossRef
7.
Schembri V, Heijmen BJM (2007) Optically stimulated luminescence (OSL) of carbon-doped aluminum oxide (Al2O3:C) for film dosimetry in radiotherapy. Med Phys 34:2113–2118CrossRef
8.
Kemnitz E, Noack J (2015) The non-aqueous fluorolytic sol–gel synthesis of nanoscaled metal fluorides. Dalt. Trans. 44:19411–19431CrossRef
9.
Chupas P, Corbin D, Rao V, Hanson J, Grey C (2003) A combined solid-state NMR and diffraction study of the structures and acidity of fluorinated aluminas: implications for catalysis. J Phys Chem B 107:8327–8336CrossRef
10.
König R, Scholz G, Bertram R, Kemnitz E (2008) Crystalline aluminium hydroxy fluorides-Suitable reference compounds for 19F chemical shift trend analysis of related amorphous solids. J Fluor Chem 129:598–606CrossRef
11.
Scholz G, Brehme S, Balski M, König R, Kemnitz E (2010) Structure and properties of mechanochemically synthesised aluminium hydroxide fluoride phases AlFx(OH)3−x·nH2O. Solid State Sci 12:1500–1506CrossRef
12.
Fukuda T, Shimamura K, Kochurikhin VV, Chani VI, Epelbaum BM (1999) Crystal growth of oxide and fluoride materials for optical, piezoelectric and other applications. J Mater Sci Mater Electron 10:571–580CrossRef
13.
Scalise V, Scholz G, Kemnitz E (2016) Mechanochemical synthesis of low-fluorine doped aluminum hydroxide fluorides. J Solid State Chem 243:154–161CrossRef
14.
Ahrem L, Scholz G, Bertram R, Kemnitz E (2016) Thermal evolution of 4- and 5-fold coordinated al-sites in aluminum hydroxide fluorides with low fluorination degree. J Phys Chem C 120:9236–9244CrossRef
15.
Bowen P, Carry C, Luxembourg D, Hofmann H (2005) Colloidal processing and sintering of nanosized transition aluminas. Powder Technol 157:100–107CrossRef
16.
Kemnitz E, Menz DH (1998) Fluorinated metal oxides and metal fluorides as heterogeneous catalysts. Prog Solid State Chem 26:97–153CrossRef
17.
Manzer EL (1990) The CFC-Ozone issue: progress on the development of alternatives to CFCs. Science 249(4964):31–35CrossRef
18.
Ritter B, Haida P, Krahl T, Scholz G, Kemnitz E (2017) Core–shell metal fluoride nanoparticles via fluorolytic sol–gel synthesis—a fast and efficient construction kit. J Mater Chem C 5:5444–5450CrossRef
19.
JCPDS-ICDD, International Centre for Diffraction Data: PDF-2 Database (sets 1–51 plus 70–89), PA, Release 2001-PCPDFWIN Version 2.2
20.
Cory DG, Ritchey WM (1988) Suppression of signals from the probe in Bloch decay spectra. J Magn Reson 80:128–132
21.
Isobe T, Watanabe T, d’Espinose de la Caillerie JP, Legrand P, Massiot D (2003) Solid-state 1H and 27Al NMR studies of amorphous aluminum hydroxides. J Colloid Interface Sci 261:320–324CrossRef
22.
Scalise V, Scholz G, Bertram R, Kemnitz E (2018) Identification of F-species after adsorption at the surface of milled and unmilled γ-Al2O3. Surf Interfaces 10:117–122CrossRef
23.
Scholz G, Feist M, Kemnitz E (2008) On the influence of humidity on the mechanochemical reaction between NaF and AlF3. Solid State Sci 10:1640–1650CrossRef
24.
Kitamura M, Senna M (2001) Effects of preheating on mechanochemical amorphization and enhanced reactivity of aluminum hydroxide. Adv Powder Technol 12:215–226CrossRef
25.
Baranyai ZV, Kristály F, Szűcs I (2013) Influence of the short time grinding on the thermal decomposition processes of gibbsite produced by the Bayer process. Mater Sci Eng 38:15–27
26.
Li J, Wu Y, Pan Y, Liu W, Guo J (2007) Influence of fluorides on phase transition of α-Al2O3 formation. Ceram Int 33:919–923CrossRef
Metadata
Title
On the influence of water on the mechanochemical synthesis of low F-doped Al-hydroxide fluorides
Authors
V. Scalise
G. Scholz
E. Kemnitz
Publication date
24-04-2018
Publisher
Springer US
Published in
Journal of Materials Science / Issue 19/2018
Print ISSN: 0022-2461
Electronic ISSN: 1573-4803
DOI
https://doi.org/10.1007/s10853-018-2347-8

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