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Journal of Materials Science
Published in: Journal of Materials Science 19/2018

11-04-2018 | Mechanochemical Synthesis

Effect of ball milling on the first hydrogenation of TiFe alloy doped with 4 wt% (Zr + 2Mn) additive

Authors: Gabriela Romero, Peng Lv, Jacques Huot

Published in: Journal of Materials Science | Issue 19/2018

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Abstract

In this paper, we report the microstructure and hydrogen storage properties of TiFe + 4 wt% (Zr + 2Mn) alloy before and after high-energy milling. The as-cast sample was made of a main TiFe phase with a Zr- and Mn-rich secondary phase. We found that ball milling can significantly reduce the crystallite size of TiFe + 4 wt% (Zr + 2Mn) alloy. First hydrogenation measurements showed that the sample milled for 15 min displayed a faster hydrogenation than the as-cast sample but with a slight loss of capacity. Further milling made the samples totally inert to hydrogen. It may be concluded that the as-cast alloy has a special microstructure that is possibly destroyed by milling.
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Metadata
Title
Effect of ball milling on the first hydrogenation of TiFe alloy doped with 4 wt% (Zr + 2Mn) additive
Authors
Gabriela Romero
Peng Lv
Jacques Huot
Publication date
11-04-2018
Publisher
Springer US
Published in
Journal of Materials Science / Issue 19/2018
Print ISSN: 0022-2461
Electronic ISSN: 1573-4803
DOI
https://doi.org/10.1007/s10853-018-2301-9

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