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06-07-2020 | Original Paper

Optimization of biodegradable starch adhesives using response surface methodology

Authors: Alejandro Ortiz-Fernández, Carlos Rolando Ríos-Soberanis, Yasser Alejandro Chim-Chi, Víctor Manuel Moo-Huchin, Raciel Javier Estrada-León, Emilio Pérez-Pacheco

Published in: Polymer Bulletin | Issue 7/2021

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Abstract

Sago and yucca commercial starches were used in order to evaluate their best possible response adhesive properties. The application of response surface methodology in the optimization of properties was used. A central composite design to evaluate the effect of four independent variables (starch percentage, NaOH percentage, temperature and cooking time) with respect to one response variable (peel strength) was also used. The properties of sago and yucca starches were compared with the properties of corn starch as reference. DSC showed that sago and yucca starches possess similar gelatinization temperatures when compared to corn starch (68.4 °C, 65.7 °C and 69.7 °C, respectively). Adhesion tests indicated that sago and yucca starches presented maximum peel strengths of 125 N/m and 115 N/m, respectively. In this work, the coefficient of determination R² remained between 0.84 and 0.90; consequently, the quality and effectiveness of the statistical models are considered adequate. These results suggested that sago and yucca starches have potential to be competitive in the global starch market for adhesive applications.

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Title: Optimization of biodegradable starch adhesives using response surface methodology
Authors: Alejandro Ortiz-Fernández
Carlos Rolando Ríos-Soberanis
Yasser Alejandro Chim-Chi
Víctor Manuel Moo-Huchin
Raciel Javier Estrada-León
Emilio Pérez-Pacheco
Publication date: 06-07-2020
Publisher: Springer Berlin Heidelberg
Published in: Polymer Bulletin / Issue 7/2021
Print ISSN: 0170-0839
Electronic ISSN: 1436-2449
DOI: https://doi.org/10.1007/s00289-020-03297-y

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