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Published in: Physics of Metals and Metallography 9/2018

01-09-2018 | STRUCTURE, PHASE TRANSFORMATIONS, AND DIFFUSION

Recrystallization Texture of Submicrocrystalline Niobium after Annealing

Authors: L. M. Voronova, T. I. Chashchukhina, M. V. Degtyarev

Published in: Physics of Metals and Metallography | Issue 9/2018

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Abstract

Scanning electron microscopy shows that in pure niobium deformed by shear under pressure, a grain structure characterized by an axial texture of recrystallization is formed from the textureless deformed state during annealing. The sharpest texture is formed during annealing at 800°C. The fraction of the area occupied by recrystallized grains, in which planes (110) are parallel to the sample plane, reaches 90%; the fraction of high-angle boundaries (HABs) is 40%; and the average grain-boundary (misorientation) angle is 17°. The texture forms during selective growth of recrystallization centers. The formation of new recrystallization centers in addition to deformation-induced growing centers during 900°C annealing slightly increases the fraction of HABs, the average misorientation angle, and creates a blurred recrystallization texture.

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Metadata
Title
Recrystallization Texture of Submicrocrystalline Niobium after Annealing
Authors
L. M. Voronova
T. I. Chashchukhina
M. V. Degtyarev
Publication date
01-09-2018
Publisher
Pleiades Publishing
Published in
Physics of Metals and Metallography / Issue 9/2018
Print ISSN: 0031-918X
Electronic ISSN: 1555-6190
DOI
https://doi.org/10.1134/S0031918X18090156

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