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Journal of Materials Science: Materials in Electronics

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02-01-2019 | Review

Solvothermal synthesis, characterization and magnetic properties of nearly superparamagnetic Zn-doped Fe₃O₄ nanoparticles

Authors: Xia Li, Er Liu, Zhi Zhang, Zhan Xu, Feng Xu

Published in: Journal of Materials Science: Materials in Electronics | Issue 4/2019

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Abstract

We report a facile solvothermal method for synthesizing nearly superparamagnetic Zn-doped Fe₃O₄ nanoparticles with controllable doping concentration. All samples demonstrate a typical spinel structure with small size (less than 20 nm). The Zn ion doping effect on the structure, morphology and magnetism of Fe₃O₄ nanoparticles have been systematically studied by XRD, TEM, FTIR, XPS and FMR. It is found that the saturation magnetization of Fe₃O₄ first increases then decreases with increasing Zn doping concentration due to the different site occupation of Zn ions. In contrast, dynamic magnetic measurements demonstrate that the Lande g-factor shows a monotonic increasing trend by the increase of Zn doping concentration.

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Title: Solvothermal synthesis, characterization and magnetic properties of nearly superparamagnetic Zn-doped Fe3O4 nanoparticles
Authors: Xia Li
Er Liu
Zhi Zhang
Zhan Xu
Feng Xu
Publication date: 02-01-2019
Publisher: Springer US
Published in: Journal of Materials Science: Materials in Electronics / Issue 4/2019
Print ISSN: 0957-4522
Electronic ISSN: 1573-482X
DOI: https://doi.org/10.1007/s10854-018-00640-y

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