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Journal of Materials Science: Materials in Electronics
Published in: Journal of Materials Science: Materials in Electronics 10/2014

01-10-2014

Synthesis, characterization and electrical property of nanocrystalline Cu0.5Ni0.5Ce3O5

Authors: H. V. Jadhav, S. G. Jadhav, S. M. Khetre

Published in: Journal of Materials Science: Materials in Electronics | Issue 10/2014

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Abstract

Nanocrystalline Cu0.5Ni0.5Ce3O5 with particle size of about 28 nm was directly synthesized by sol–gel auto-combustion method at room temperature. The overall process involves three steps: formation of homogeneous sol; formation of dried gel; and combustion of the dried gel. Experiments revealed that Cu0.5Ni0.5Ce3O5 dried gel derived from glycine and nitrate sol exhibits self-propagating combustion at room temperature once it is ignited in air. After auto-combustion, the desired nanocrystalline Cu0.5Ni0.5Ce3O5 was acquired and further calcination was needed. The auto-combustion was considered as a heat-induced exothermic oxidation–reduction reaction between nitrate ions and carboxyl group. The synthesized powder was characterized by XRD, TG/DTA, SEM and TEM. Nanocrystalline Cu0.5Ni0.5Ce3O5 was p type semiconducting material. Shapes of the particles are nanocoralloids in nature. The I–V characteristic and electrical properties of the nanocrystalline Cu0.5Ni0.5Ce3O5 were studied.
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Metadata
Title
Synthesis, characterization and electrical property of nanocrystalline Cu0.5Ni0.5Ce3O5
Authors
H. V. Jadhav
S. G. Jadhav
S. M. Khetre
Publication date
01-10-2014
Publisher
Springer US
Published in
Journal of Materials Science: Materials in Electronics / Issue 10/2014
Print ISSN: 0957-4522
Electronic ISSN: 1573-482X
DOI
https://doi.org/10.1007/s10854-014-2176-8

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