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Published in: Microsystem Technologies 3/2017

04-11-2015 | Technical Paper

Ultrasonic fabrication of micro nozzles from a stack of PVDF foils for generating and characterizing microfluidic dispersions

Authors: S. Liao, J. Sackmann, A. Tollkötter, M. Pasterny, N. Kockmann, W. K. Schomburg

Published in: Microsystem Technologies | Issue 3/2017

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Abstract

Nozzles with circular cross-section and a diameter varying in axial direction have been fabricated in a microfluidic channel from polyvinylidene fluoride as chemically resistive thermoplastic polymer. Smallest diameter and length of the nozzle are approximately 150 µm and 3.4 mm, respectively. The nozzle and the entire channel system have been fabricated from two halves generated by ultrasonic hot embossing and bonded to each other by ultrasonic welding. Alignment during ultrasonic welding was assisted by a fit of energy directors and an accuracy of 35 and 10 µm in normal and lateral direction, respectively, was obtained. Thermoplastic molding of the two halves of the channel structures was performed by ultrasonic hot embossing with a cycle time of a few seconds. The development was significantly accelerated by milling the tools directly into aluminum plates. This way, new designs were realized within a day. The micro nozzles have been proven generating liquid/liquid dispersions of different flow patterns as a function of flow velocity and Capillary number.

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Literature
go back to reference Burns JR, Ramshaw C (2001) The intensification of rapid reactions in multiphase systems using slug flow in capillaries. Lab Chip 1:10–15CrossRef Burns JR, Ramshaw C (2001) The intensification of rapid reactions in multiphase systems using slug flow in capillaries. Lab Chip 1:10–15CrossRef
go back to reference Christopher GF, Anna SL (2007) Microfluidic methods for generating continuous droplet streams. J Phys D Appl Phys 40:R319–R336CrossRef Christopher GF, Anna SL (2007) Microfluidic methods for generating continuous droplet streams. J Phys D Appl Phys 40:R319–R336CrossRef
go back to reference de Menech M, Garstecki P, Jousse F, Stone HA (2008) Transition from squeezing to dripping in a microfluidic T-shaped junction. J Fluid Mech 595:141–161CrossRefMATH de Menech M, Garstecki P, Jousse F, Stone HA (2008) Transition from squeezing to dripping in a microfluidic T-shaped junction. J Fluid Mech 595:141–161CrossRefMATH
go back to reference Forrester SE, Rielly CD (1998) Bubble formation from cylindrical, flat and concave sections exposed to a strong liquid cross-flow. Chem Eng Sci 53:1517–1527CrossRef Forrester SE, Rielly CD (1998) Bubble formation from cylindrical, flat and concave sections exposed to a strong liquid cross-flow. Chem Eng Sci 53:1517–1527CrossRef
go back to reference Fu T, Ma Y, Funfschilling D, Zhu C, Li HZ (2010) Squeezing-to-dripping transition for bubble formation in a microfluidic T-junction. Chem Eng Sci 65:3739–3748CrossRef Fu T, Ma Y, Funfschilling D, Zhu C, Li HZ (2010) Squeezing-to-dripping transition for bubble formation in a microfluidic T-junction. Chem Eng Sci 65:3739–3748CrossRef
go back to reference Garstecki P (2010) Formation of droplets and bubbles in microfluidic systems. microfluidics based microsystems. Springer, Dordrecht Garstecki P (2010) Formation of droplets and bubbles in microfluidic systems. microfluidics based microsystems. Springer, Dordrecht
go back to reference Gu H, Duits MHG, Mugele F (2011) Droplets formation and merging in two-phase flow microfluidics. Int J Mol Sci 12:2572–2597CrossRef Gu H, Duits MHG, Mugele F (2011) Droplets formation and merging in two-phase flow microfluidics. Int J Mol Sci 12:2572–2597CrossRef
go back to reference Gupta A, Kumar R (2010) Effect of geometry on droplet formation in the squeezing regime in a microfluidic T-junction. Microfluid Nanofluid 8:799–812CrossRef Gupta A, Kumar R (2010) Effect of geometry on droplet formation in the squeezing regime in a microfluidic T-junction. Microfluid Nanofluid 8:799–812CrossRef
go back to reference Harsch S, Ehrfeld W, Maner A (1988) Untersuchungen zur Herstellung von Mikrostrukturen großer Strukturhöhe durch Galvanoformung in Nickelsulfamatelektrolyten. KfK-Bericht 4455, Kernforschungszentrum Karlsruhe, ISSN 0303-4003 Harsch S, Ehrfeld W, Maner A (1988) Untersuchungen zur Herstellung von Mikrostrukturen großer Strukturhöhe durch Galvanoformung in Nickelsulfamatelektrolyten. KfK-Bericht 4455, Kernforschungszentrum Karlsruhe, ISSN 0303-4003
go back to reference Holvey C, Macchi A, Kockmann N, Roberge DM (2011) Pressure drop and mixing in single phase microreactors: simplified designs of micromixers. Chem Eng Proc 50:1069–1075CrossRef Holvey C, Macchi A, Kockmann N, Roberge DM (2011) Pressure drop and mixing in single phase microreactors: simplified designs of micromixers. Chem Eng Proc 50:1069–1075CrossRef
go back to reference Kashid MN, Agar DW (2007) Hydrodynamics of liquid–liquid slug flow capillary microreactor: flow regimes, slug size and pressure drop. Chem Eng J 131:1–13CrossRef Kashid MN, Agar DW (2007) Hydrodynamics of liquid–liquid slug flow capillary microreactor: flow regimes, slug size and pressure drop. Chem Eng J 131:1–13CrossRef
go back to reference Khuntontong P, Blaser T, Schomburg WK (2008) Ultrasonic micro hot embossing of thermoplastic polymers. In: Proceedings of 24th Annual Meeting of the Polymer Processing Society, PPS24, Salerno, Italy, June 15–19. p 364 Khuntontong P, Blaser T, Schomburg WK (2008) Ultrasonic micro hot embossing of thermoplastic polymers. In: Proceedings of 24th Annual Meeting of the Polymer Processing Society, PPS24, Salerno, Italy, June 15–19. p 364
go back to reference Kockmann N (2008) Pressure loss and transport rates in microstructured devices with chemical reactions. Chem Eng echn 31:1188–1195 Kockmann N (2008) Pressure loss and transport rates in microstructured devices with chemical reactions. Chem Eng echn 31:1188–1195
go back to reference Kockmann N, Gottsponer M (2010) Heat transfer limitations of gas-liquid exothermic reactions in micro-channels. In: Proceedings of ASME-ICNMM2010. 30389, Montreal Kockmann N, Gottsponer M (2010) Heat transfer limitations of gas-liquid exothermic reactions in micro-channels. In: Proceedings of ASME-ICNMM2010. 30389, Montreal
go back to reference Kockmann N, Roberge DM (2011) Scale-up concept for modular microstructured reactors based on mixing, heat transfer, and reactor safety. Chem Eng Pro 50:1017–1026CrossRef Kockmann N, Roberge DM (2011) Scale-up concept for modular microstructured reactors based on mixing, heat transfer, and reactor safety. Chem Eng Pro 50:1017–1026CrossRef
go back to reference Kulkarni AA, Joshi JB (2005) Bubble Formation and Bubble Rise Velocity in Gas-Liquid Systems: a Review. Ind Eng Chem Res 44:5873–5931CrossRef Kulkarni AA, Joshi JB (2005) Bubble Formation and Bubble Rise Velocity in Gas-Liquid Systems: a Review. Ind Eng Chem Res 44:5873–5931CrossRef
go back to reference Liepe F, Meusel W, Möckel H, Platzer B, Weissgärber H (1988) Stoffvereinigen in fluiden Phasen. Verfahrens-technische Berechnungsmethoden. Wiley-VCH, Weinheim Liepe F, Meusel W, Möckel H, Platzer B, Weissgärber H (1988) Stoffvereinigen in fluiden Phasen. Verfahrens-technische Berechnungsmethoden. Wiley-VCH, Weinheim
go back to reference Lin C-H, Chen R (2006) Ultrasonic nanoimprint lithography: a new approach to nanopatterning. J Micro/Nanolith MEMS MOEMS 5:1. doi:10.1117/1.2172992 Lin C-H, Chen R (2006) Ultrasonic nanoimprint lithography: a new approach to nanopatterning. J Micro/Nanolith MEMS MOEMS 5:1. doi:10.​1117/​1.​2172992
go back to reference Matsuyama K, Mine K, Kubo H, Aoki N, Mae K (2010) Optimization methodology of operation of orifice-shaped micromixer based on micro-jet concept. Chem Eng Sci 65:5912–5920CrossRef Matsuyama K, Mine K, Kubo H, Aoki N, Mae K (2010) Optimization methodology of operation of orifice-shaped micromixer based on micro-jet concept. Chem Eng Sci 65:5912–5920CrossRef
go back to reference Mekaru H, Nakamura O, Maruyama O, Maeda R, Hattori T (2006) Development of precision transfer technology of atmospheric hot embossing by ultrasonic vibration. Microsyst Technol 13:385–391. doi:10.1007/s00542-006-0203-2 CrossRef Mekaru H, Nakamura O, Maruyama O, Maeda R, Hattori T (2006) Development of precision transfer technology of atmospheric hot embossing by ultrasonic vibration. Microsyst Technol 13:385–391. doi:10.​1007/​s00542-006-0203-2 CrossRef
go back to reference Okubo Y, Maki T, Aoki N, Khoo TH, Ohmukai Y, Mae K (2008) Liquid-liquid extraction for efficient synthesis and separation by utilizing micro spaces. Chem Eng Sci 63:4070–4077CrossRef Okubo Y, Maki T, Aoki N, Khoo TH, Ohmukai Y, Mae K (2008) Liquid-liquid extraction for efficient synthesis and separation by utilizing micro spaces. Chem Eng Sci 63:4070–4077CrossRef
go back to reference Park JM, Kim NH, Lee B-K, Lee K-H, Kwon TH (2008) Nickel stamp fabrication and hot embossing for mass-production of micro/nano combined structures using anodic aluminum oxide. Microsyst Technol 14:1689–1694. doi:10.1007/s00542-007-0504-0 CrossRef Park JM, Kim NH, Lee B-K, Lee K-H, Kwon TH (2008) Nickel stamp fabrication and hot embossing for mass-production of micro/nano combined structures using anodic aluminum oxide. Microsyst Technol 14:1689–1694. doi:10.​1007/​s00542-007-0504-0 CrossRef
go back to reference Parmar R, Majumder SK (2013) Microbubble generation and microbubble-aided transport process intensification—A state-of-the-art report. Chem Eng Proc 64:79–97CrossRef Parmar R, Majumder SK (2013) Microbubble generation and microbubble-aided transport process intensification—A state-of-the-art report. Chem Eng Proc 64:79–97CrossRef
go back to reference Potente H (2004) Fügen von Kunststoffen—Grundlagen, Verfahren, Anwendung. Carl Hanser, München Potente H (2004) Fügen von Kunststoffen—Grundlagen, Verfahren, Anwendung. Carl Hanser, München
go back to reference Schubert H (2003) Handbuch der Mechanischen Verfahrenstechnik. Wiley-VCH, Weinheim Schubert H (2003) Handbuch der Mechanischen Verfahrenstechnik. Wiley-VCH, Weinheim
go back to reference Seemann R, Brinkmann M, Pfohl T, Herminghaus S (2012) Droplet based microfluidics. Rep Prog Phys 75:1–41CrossRef Seemann R, Brinkmann M, Pfohl T, Herminghaus S (2012) Droplet based microfluidics. Rep Prog Phys 75:1–41CrossRef
go back to reference Shao N, Gavriilidis A, Angeli P (2009) Flow regimes for adiabatic gas-liquid flow in microchannels. Chem Eng Sci 64:2749–2761CrossRef Shao N, Gavriilidis A, Angeli P (2009) Flow regimes for adiabatic gas-liquid flow in microchannels. Chem Eng Sci 64:2749–2761CrossRef
go back to reference Song H, Chen DL, Ismagilov RF (2006) Reactions in droplets in microfluidic channels. Angew Chem Int Ed 45:7336–7356CrossRef Song H, Chen DL, Ismagilov RF (2006) Reactions in droplets in microfluidic channels. Angew Chem Int Ed 45:7336–7356CrossRef
go back to reference Tollkoetter A, Kockmann N (2014) A modular microfluidic system for high flow rate re-dispersion of gas–liquid. In: Proceedings of ASME-ICNMM2014-22048, Chicago, Illinois Tollkoetter A, Kockmann N (2014) A modular microfluidic system for high flow rate re-dispersion of gas–liquid. In: Proceedings of ASME-ICNMM2014-22048, Chicago, Illinois
go back to reference Tollkoetter A, Schirmbeck F, Wesholowski J, Kockmann N (2015) High flow rate micro orifice dispersion of gas–liquid flow. In: Proceedings of ASME-ICNMM2015-48221, San Francisco, California Tollkoetter A, Schirmbeck F, Wesholowski J, Kockmann N (2015) High flow rate micro orifice dispersion of gas–liquid flow. In: Proceedings of ASME-ICNMM2015-48221, San Francisco, California
go back to reference Tollkoetter A, Sackmann J, Baldhoff T, Schomburg WK, Kockmann N (2015) Modulares Mikroreaktorsystem aus ultraschallheißgeprägten Polymerfolien. Chem Ing Techn, early view, Feb 2015 Tollkoetter A, Sackmann J, Baldhoff T, Schomburg WK, Kockmann N (2015) Modulares Mikroreaktorsystem aus ultraschallheißgeprägten Polymerfolien. Chem Ing Techn, early view, Feb 2015
go back to reference Yue J, Luo L, Gonthier Y, Chen G, Yuan Q (2008) An experimental investigation of gas–liquid two-phase flow in single microchannel contactors. Chem Eng Sci 63:4189–4202CrossRef Yue J, Luo L, Gonthier Y, Chen G, Yuan Q (2008) An experimental investigation of gas–liquid two-phase flow in single microchannel contactors. Chem Eng Sci 63:4189–4202CrossRef
go back to reference Zhao C-H (2013) Multiphase flow microfluidics for the production of single or multiple emulsions for drug delivery. Adv Drug Deli Rev 65:1420–1446CrossRef Zhao C-H (2013) Multiphase flow microfluidics for the production of single or multiple emulsions for drug delivery. Adv Drug Deli Rev 65:1420–1446CrossRef
go back to reference Zhao C-X, Middelberg APJ (2011) Two-phase microfluidic flows. Chem Eng Sci 66:1394–1411CrossRef Zhao C-X, Middelberg APJ (2011) Two-phase microfluidic flows. Chem Eng Sci 66:1394–1411CrossRef
Metadata
Title
Ultrasonic fabrication of micro nozzles from a stack of PVDF foils for generating and characterizing microfluidic dispersions
Authors
S. Liao
J. Sackmann
A. Tollkötter
M. Pasterny
N. Kockmann
W. K. Schomburg
Publication date
04-11-2015
Publisher
Springer Berlin Heidelberg
Published in
Microsystem Technologies / Issue 3/2017
Print ISSN: 0946-7076
Electronic ISSN: 1432-1858
DOI
https://doi.org/10.1007/s00542-015-2708-z

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