Skip to main content
Top
Published in: Journal of Materials Engineering and Performance 7/2018

30-05-2018

Effect of Zener–Holloman Parameter on the Prior Austenite Grain size in a 12Cr-10Ni Precipitation-Hardenable Stainless Steel

Authors: C. R. Anoop, Aditya Prakash, S. V. S. Narayana Murty, Indradev Samajdar

Published in: Journal of Materials Engineering and Performance | Issue 7/2018

Log in

Activate our intelligent search to find suitable subject content or patents.

search-config
loading …

Abstract

Hot isothermal plane strain compression (PSC) tests were carried out on a 12Cr-10Ni martensitic precipitation-hardenable (PH) stainless steel, in the temperature range of 750-1050 °C, to study microstructural evolution during large strain deformation. The nature of stress–strain curves varies with Zener–Holloman parameter (Z) with specimens deformed at high Z showing steady-state behavior and those deformed at lower Z showing flow softening. Prior austenite grain size (PAGS), d, exhibited a strong correlation to Z showing a bilinear behavior represented as: d = (1803.9)Z−0.094 for high Z deformation and d = (1456.2)Z−0.058 for low Z deformation. Based on the above study, it is recommended to thermomechanically process 12Cr-10Ni steel at Z ≥ 1022 for obtaining products with good strength–toughness balance.

Dont have a licence yet? Then find out more about our products and how to get one now:

Springer Professional "Wirtschaft+Technik"

Online-Abonnement

Mit Springer Professional "Wirtschaft+Technik" erhalten Sie Zugriff auf:

  • über 102.000 Bücher
  • über 537 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Finance + Banking
  • Management + Führung
  • Marketing + Vertrieb
  • Maschinenbau + Werkstoffe
  • Versicherung + Risiko

Jetzt Wissensvorsprung sichern!

Springer Professional "Technik"

Online-Abonnement

Mit Springer Professional "Technik" erhalten Sie Zugriff auf:

  • über 67.000 Bücher
  • über 390 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Maschinenbau + Werkstoffe




 

Jetzt Wissensvorsprung sichern!

Literature
1.
go back to reference R.K. Wilson, Ed., Maraging Steels: Recent Developments and Applications, The Minerals Metals & Materials Society, Pittsburgh, 1998, p 1–39 R.K. Wilson, Ed., Maraging Steels: Recent Developments and Applications, The Minerals Metals & Materials Society, Pittsburgh, 1998, p 1–39
2.
go back to reference M.F. McGuire, Stainless Steels for Design Engineers, ASM International, Almere, 2008, p 137–146 M.F. McGuire, Stainless Steels for Design Engineers, ASM International, Almere, 2008, p 137–146
3.
go back to reference Y.V.R.K. Prasad and S. Sasidhara, Hot Working Guide, ASM International, Almere, 2015, p 1–24 Y.V.R.K. Prasad and S. Sasidhara, Hot Working Guide, ASM International, Almere, 2015, p 1–24
4.
go back to reference Y.V.R.K. Prasad and T. Seshacharyalu, Modelling of Hot Deformation for Microstructural Control, Int. Mater. Rev., 1998, 43, p 243–258CrossRef Y.V.R.K. Prasad and T. Seshacharyalu, Modelling of Hot Deformation for Microstructural Control, Int. Mater. Rev., 1998, 43, p 243–258CrossRef
5.
go back to reference S.V.S. Narayana Murty, B. Nageswara Rao, and B.P. Kashyap, Instability Criteria for Hot Deformation of Materials, Int. Mater. Rev., 2000, 45, p 15–26CrossRef S.V.S. Narayana Murty, B. Nageswara Rao, and B.P. Kashyap, Instability Criteria for Hot Deformation of Materials, Int. Mater. Rev., 2000, 45, p 15–26CrossRef
6.
go back to reference G.E. Dieter, H.A. Kuhn, and S.L. Semiatin, Ed., Handbook of Workability and Process Design, ASM International, Almere, 2003 G.E. Dieter, H.A. Kuhn, and S.L. Semiatin, Ed., Handbook of Workability and Process Design, ASM International, Almere, 2003
7.
go back to reference G.E. Dieter, Mechanical Metallurgy, McGraw Hill, New York, 1986 G.E. Dieter, Mechanical Metallurgy, McGraw Hill, New York, 1986
8.
go back to reference S. Morito, H. Saito, T. Ogawa, T. Furuhara, and T. Maki, Effect of Austenite Grain size on the Morphology and Crystallography of Lath Martensite in Low Carbon Steels, ISIJ Int., 2005, 45, p 91–94CrossRef S. Morito, H. Saito, T. Ogawa, T. Furuhara, and T. Maki, Effect of Austenite Grain size on the Morphology and Crystallography of Lath Martensite in Low Carbon Steels, ISIJ Int., 2005, 45, p 91–94CrossRef
9.
go back to reference M. Pietrzyk, J.G. Lenard, and G.M. Dalton, A Study of Plane Strain Compression Test, Ann. CIRP, 1993, 42, p 331–334CrossRef M. Pietrzyk, J.G. Lenard, and G.M. Dalton, A Study of Plane Strain Compression Test, Ann. CIRP, 1993, 42, p 331–334CrossRef
10.
go back to reference S.V.S. Narayana Murty, S. Torizuka, and K. Nagai, Microstructural Evolution During Simple Heavy Warm Compression of a Low Carbon Steel: Development of a Processing Map, Mater. Sci. Eng. A, 2005, 410–411, p 319–323CrossRef S.V.S. Narayana Murty, S. Torizuka, and K. Nagai, Microstructural Evolution During Simple Heavy Warm Compression of a Low Carbon Steel: Development of a Processing Map, Mater. Sci. Eng. A, 2005, 410–411, p 319–323CrossRef
11.
go back to reference N. Nayan, N.P. Gurao, S.V.S. Narayana Murty, A.K. Jha, B. Pant, and K.M. George, Microstructure and Microtexture Evolution During Larges Strain Deformation of Inconel Alloy IN718, Mater. Charact., 2010, 110, p 236–241CrossRef N. Nayan, N.P. Gurao, S.V.S. Narayana Murty, A.K. Jha, B. Pant, and K.M. George, Microstructure and Microtexture Evolution During Larges Strain Deformation of Inconel Alloy IN718, Mater. Charact., 2010, 110, p 236–241CrossRef
12.
go back to reference N. Nayan, N.P. Gurao, S.V.S. Narayana Murty, A.K. Jha, B. Pant, and S.C. Sharma, Microstructure and Microtexture Evolution During Larges Strain Deformation of an Aluminium-Copper-Lithium Alloy AA2195, Mater. Des., 2015, 65, p 862–868CrossRef N. Nayan, N.P. Gurao, S.V.S. Narayana Murty, A.K. Jha, B. Pant, and S.C. Sharma, Microstructure and Microtexture Evolution During Larges Strain Deformation of an Aluminium-Copper-Lithium Alloy AA2195, Mater. Des., 2015, 65, p 862–868CrossRef
13.
go back to reference C. Boldetti, C. Pinna, and I.C. Howard, Measurement and Prediction of Deformation in Plane Strain Compression Tests of AA5182, Mater. Sci. Technol., 2006, 22, p 1380–1386CrossRef C. Boldetti, C. Pinna, and I.C. Howard, Measurement and Prediction of Deformation in Plane Strain Compression Tests of AA5182, Mater. Sci. Technol., 2006, 22, p 1380–1386CrossRef
14.
go back to reference S.A. Aksenov, J. Kliber, Y.A. Puzino, and S.A. Bober, Processing of Plane Strain Compression Test Results for Investigation of AISI, 304 Stainless Steel Constitutive Behaviour, J. Chem. Technol. Metall., 2015, 50(6), p 644–650 S.A. Aksenov, J. Kliber, Y.A. Puzino, and S.A. Bober, Processing of Plane Strain Compression Test Results for Investigation of AISI, 304 Stainless Steel Constitutive Behaviour, J. Chem. Technol. Metall., 2015, 50(6), p 644–650
15.
go back to reference K. Pawlak, B. Białobrzeska, and Ł. Konat, The Influence of Austenitizing Temperature on Prior Austenite Grain Size and Resistance to Abrasion Wear of Selected Low-Alloy Boron Steel, Arch. Civ. Mech. Eng., 2016, 16, p 913–926CrossRef K. Pawlak, B. Białobrzeska, and Ł. Konat, The Influence of Austenitizing Temperature on Prior Austenite Grain Size and Resistance to Abrasion Wear of Selected Low-Alloy Boron Steel, Arch. Civ. Mech. Eng., 2016, 16, p 913–926CrossRef
16.
go back to reference J.W. Morris, Jr., C. Kinney, K. Ptylweski, and Y. Adachi, Microstructure and Cleavage in Lath Martensitic Steels, Sci. Technol. Adv. Mater., 2013, 14, p 1–9CrossRef J.W. Morris, Jr., C. Kinney, K. Ptylweski, and Y. Adachi, Microstructure and Cleavage in Lath Martensitic Steels, Sci. Technol. Adv. Mater., 2013, 14, p 1–9CrossRef
17.
go back to reference J.W. Morris, Jr., On Ductile–Brittle Transition in Lath Martensitic Steels, ISIJ Int., 2011, 51, p 1569–1575CrossRef J.W. Morris, Jr., On Ductile–Brittle Transition in Lath Martensitic Steels, ISIJ Int., 2011, 51, p 1569–1575CrossRef
18.
go back to reference C.R. Anoop, A. Prakash, S.V.S. Narayana Murty, and I. Samajdar, Optimization of Hot Workability and Microstructure Control in a 12Cr-10Ni Precipitation Hardenable Stainless Steel: An Approach Using Processing Maps, (Submitted to Materials Characterisation, under revision) C.R. Anoop, A. Prakash, S.V.S. Narayana Murty, and I. Samajdar, Optimization of Hot Workability and Microstructure Control in a 12Cr-10Ni Precipitation Hardenable Stainless Steel: An Approach Using Processing Maps, (Submitted to Materials Characterisation, under revision)
19.
go back to reference C.R. Anoop, A. Prakash, S.V.S. Narayana Murty, and I. Samajdar, Origin of Low Temperature Toughness in a 12Cr-10Ni Martensitic Precipitation Hardenable Stainless Steel, Mater. Sci. Eng. A, 2018, 709, p 1–8CrossRef C.R. Anoop, A. Prakash, S.V.S. Narayana Murty, and I. Samajdar, Origin of Low Temperature Toughness in a 12Cr-10Ni Martensitic Precipitation Hardenable Stainless Steel, Mater. Sci. Eng. A, 2018, 709, p 1–8CrossRef
20.
go back to reference R.D. Doherthy, D.A. Hughes, F.J. Humphreys, J.J. Jonas, D.J. Jensen, M.E. Kassner, W.E. King, T.R. McNelley, H.J. McQuen, and A.D. Rollet, Current Issues in Recrystallisation: A Review, Mater. Sci. Eng. A, 1997, 238, p 219–274CrossRef R.D. Doherthy, D.A. Hughes, F.J. Humphreys, J.J. Jonas, D.J. Jensen, M.E. Kassner, W.E. King, T.R. McNelley, H.J. McQuen, and A.D. Rollet, Current Issues in Recrystallisation: A Review, Mater. Sci. Eng. A, 1997, 238, p 219–274CrossRef
21.
go back to reference Y.V.R.K. Prasad and N. Ravichandran, Effect of SFE on the Dynamic Recrystallisation During Hot Working of FCC Metals: A Study Using Processing Maps, Bull. Mater. Sci., 1991, 14(5), p 1241–1248CrossRef Y.V.R.K. Prasad and N. Ravichandran, Effect of SFE on the Dynamic Recrystallisation During Hot Working of FCC Metals: A Study Using Processing Maps, Bull. Mater. Sci., 1991, 14(5), p 1241–1248CrossRef
22.
go back to reference H. Mirzadeh and A. Najafizadeh, Hot Deformation and Dynamic Recrystallisation of 17-4 PH Stainless Steel, ISIJ Int., 2013, 53, p 680–689CrossRef H. Mirzadeh and A. Najafizadeh, Hot Deformation and Dynamic Recrystallisation of 17-4 PH Stainless Steel, ISIJ Int., 2013, 53, p 680–689CrossRef
23.
go back to reference ASM International, ASM Handbook, Vol 14A, ASM International, Almere, 2010, p 261–268 ASM International, ASM Handbook, Vol 14A, ASM International, Almere, 2010, p 261–268
24.
go back to reference I. Salvatori, T. Inoue, and K. Nagai, Ultra Fin Grain Structure Through Dynamic Recrystallisation for Type 304 Stainless Steel, ISIJ Int., 2002, 42, p 744–750CrossRef I. Salvatori, T. Inoue, and K. Nagai, Ultra Fin Grain Structure Through Dynamic Recrystallisation for Type 304 Stainless Steel, ISIJ Int., 2002, 42, p 744–750CrossRef
25.
go back to reference T. Simm, L. Sun, S. McAdam, P. Hill, M. Rawson, and K. Perkins, The Influence of Lath, Block and Prior Austenite Grain (PAG) Size on the Tensile, Creep and Fatigue Properties of Novel Maraging Steel, Materials, 2017, 10, p 730CrossRef T. Simm, L. Sun, S. McAdam, P. Hill, M. Rawson, and K. Perkins, The Influence of Lath, Block and Prior Austenite Grain (PAG) Size on the Tensile, Creep and Fatigue Properties of Novel Maraging Steel, Materials, 2017, 10, p 730CrossRef
26.
go back to reference P.P. Sinha, Influence of Heat Treatment on Microstructure and Mechanical Properties of 18Ni Co-free (T-250 Grade) Maraging Steel, Ph.D. thesis, Banaras Hindu University (BHU), 1993 P.P. Sinha, Influence of Heat Treatment on Microstructure and Mechanical Properties of 18Ni Co-free (T-250 Grade) Maraging Steel, Ph.D. thesis, Banaras Hindu University (BHU), 1993
27.
go back to reference H.J. Rack, Age Hardening-Grainsize Relationship in 18Ni Maraging Steels, Mater. Sci. Eng., 1978, 34, p 263–270CrossRef H.J. Rack, Age Hardening-Grainsize Relationship in 18Ni Maraging Steels, Mater. Sci. Eng., 1978, 34, p 263–270CrossRef
Metadata
Title
Effect of Zener–Holloman Parameter on the Prior Austenite Grain size in a 12Cr-10Ni Precipitation-Hardenable Stainless Steel
Authors
C. R. Anoop
Aditya Prakash
S. V. S. Narayana Murty
Indradev Samajdar
Publication date
30-05-2018
Publisher
Springer US
Published in
Journal of Materials Engineering and Performance / Issue 7/2018
Print ISSN: 1059-9495
Electronic ISSN: 1544-1024
DOI
https://doi.org/10.1007/s11665-018-3431-6

Other articles of this Issue 7/2018

Journal of Materials Engineering and Performance 7/2018 Go to the issue

Premium Partners