Skip to main content
Top
Published in: Journal of Materials Science 4/2018

23-10-2017 | Metals

Hot compressive deformation behavior and electron backscattering diffraction analysis of Mg95.50Zn3.71Y0.79 fine-grained alloy solidified under high pressure

Authors: Fan Zhibin, Lin Xiaoping, Dong Yun, Xu Rui, Wang Lin

Published in: Journal of Materials Science | Issue 4/2018

Log in

Activate our intelligent search to find suitable subject content or patents.

search-config
loading …

Abstract

An Mg95.50Zn3.71Y0.79 fine-grained solidified alloy with a grain size of 16 μm was prepared by high-pressure solidification. The microstructure characteristics and hot compressive deformation behavior of the alloy solidified under high pressure were compared with the atmospheric-pressure solidified alloy by carrying out the unilateral compression tests under a strain rate in the range of 0.001–1.0 s−1 and at a deformation temperature in the range of 523–573 K. The true stress-true strain curve of the high-pressure solidified alloy shows the typical dynamic recrystallization rheological curve. EBSD results show that when the deformation was carried out at 573 K, nearly 90% dynamic recrystallization occurred in the high-pressure solidified alloy, and the newly formed grains were distortionless and had low dislocation density. The high-pressure solidified alloy showed a double-peak basal texture at a strain rate of 1.0 s−1. The two peak points showed a maximum pole density of 9.88 and 7.91, less than that in atmospheric-pressure alloy. When the deformation was carried out at the following conditions: deformation temperature = 573 K, strain rate = 0.001, and true strain = 0.9, the average Schmid factor (SF) for basal slip of the grains in the high-pressure solidified alloy was 0.419, and SF value for basal slip in 91% grains was greater than 0.3.

Dont have a licence yet? Then find out more about our products and how to get one now:

Springer Professional "Wirtschaft+Technik"

Online-Abonnement

Mit Springer Professional "Wirtschaft+Technik" erhalten Sie Zugriff auf:

  • über 102.000 Bücher
  • über 537 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Finance + Banking
  • Management + Führung
  • Marketing + Vertrieb
  • Maschinenbau + Werkstoffe
  • Versicherung + Risiko

Jetzt Wissensvorsprung sichern!

Springer Professional "Technik"

Online-Abonnement

Mit Springer Professional "Technik" erhalten Sie Zugriff auf:

  • über 67.000 Bücher
  • über 390 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Maschinenbau + Werkstoffe




 

Jetzt Wissensvorsprung sichern!

Literature
1.
go back to reference Wen K, Liu K, Wang ZW, Li SB, Du WB (2015) Effect of microstructure evolution on mechanical property of extruded Mg–12Gd–2E−1Zn–0.6Zr alloys. J Magnes Alloy 3:23–28CrossRef Wen K, Liu K, Wang ZW, Li SB, Du WB (2015) Effect of microstructure evolution on mechanical property of extruded Mg–12Gd–2E−1Zn–0.6Zr alloys. J Magnes Alloy 3:23–28CrossRef
2.
go back to reference Tahreen N, Zhang DF, Pan FS, Jiang XQ, Li DY, Chen DL (2015) Hot deformation and processing map of an as-extruded Mg–Zn–Mn–Y alloy containing I and W phases. Mater Des 87:245–255CrossRef Tahreen N, Zhang DF, Pan FS, Jiang XQ, Li DY, Chen DL (2015) Hot deformation and processing map of an as-extruded Mg–Zn–Mn–Y alloy containing I and W phases. Mater Des 87:245–255CrossRef
3.
go back to reference Chang H, Wang XJ, Hu SH, Wang YQ, Nie KB, Wu K (2014) Effects of reinforced particles on dynamic recrystallization of Mg base alloys during hot extrusion. Rare Metal Mater Eng 43:1821–1825CrossRef Chang H, Wang XJ, Hu SH, Wang YQ, Nie KB, Wu K (2014) Effects of reinforced particles on dynamic recrystallization of Mg base alloys during hot extrusion. Rare Metal Mater Eng 43:1821–1825CrossRef
4.
go back to reference Tong LB, Li X, Zhang DP, Cheng LR, Meng J, Zhang HJ (2014) Dynamic recrystallization and texture evolution of Mg–Y–Zn alloy during hot extrusion process. Mater Charact 92:77–83CrossRef Tong LB, Li X, Zhang DP, Cheng LR, Meng J, Zhang HJ (2014) Dynamic recrystallization and texture evolution of Mg–Y–Zn alloy during hot extrusion process. Mater Charact 92:77–83CrossRef
5.
go back to reference Wu WX, Jin L, Dong J, Zhang ZY, Ding WJ (2012) Effect of initial microstructure on the dynamic recrystallization behavior of Mg–Gd–Y–Zr alloy. Mater Sci Eng, A 556:519–525CrossRef Wu WX, Jin L, Dong J, Zhang ZY, Ding WJ (2012) Effect of initial microstructure on the dynamic recrystallization behavior of Mg–Gd–Y–Zr alloy. Mater Sci Eng, A 556:519–525CrossRef
6.
go back to reference Koike J, Ohyama R (2005) Geometrical criterion for the activation of prismatic slip in AZ61 Mg alloy sheets deformed at room temperature. Acta Mater 53:1963–1972CrossRef Koike J, Ohyama R (2005) Geometrical criterion for the activation of prismatic slip in AZ61 Mg alloy sheets deformed at room temperature. Acta Mater 53:1963–1972CrossRef
7.
go back to reference Barnett MR, Beer AG, Atwell D, Oudin A (2004) Influence of grain size on hot working stresses and microstructures in Mg–3Al–lZn. Scripta Mater 51:19–24CrossRef Barnett MR, Beer AG, Atwell D, Oudin A (2004) Influence of grain size on hot working stresses and microstructures in Mg–3Al–lZn. Scripta Mater 51:19–24CrossRef
8.
go back to reference Li NL, Huang GJ, Zhong XY, Liu Q (2013) Deformation mechanisms and dynamic crystallization of AZ31 Mg alloy with different initial textures during hot tension. Mater Design 50:382–391CrossRef Li NL, Huang GJ, Zhong XY, Liu Q (2013) Deformation mechanisms and dynamic crystallization of AZ31 Mg alloy with different initial textures during hot tension. Mater Design 50:382–391CrossRef
9.
go back to reference Li NL, Huang GJ, Xin RL, Liu Q (2013) Effect of initial texture on dynamic recrystallization and deformation mechanisms in AZ31 Mg alloy extruded at 573 K. Mater Sci Eng, A 569:18–26CrossRef Li NL, Huang GJ, Xin RL, Liu Q (2013) Effect of initial texture on dynamic recrystallization and deformation mechanisms in AZ31 Mg alloy extruded at 573 K. Mater Sci Eng, A 569:18–26CrossRef
10.
go back to reference Lv BJ, Peng J, Zhu LL, Wang YJ, Tang AT (2014) The effect of 14H LPSO phase on dynamic recrystallization behavior and hot workability of Mg–2.0Zn–0.3Zr–5.8Y alloy. Mater Sci Eng, A 599:150–159CrossRef Lv BJ, Peng J, Zhu LL, Wang YJ, Tang AT (2014) The effect of 14H LPSO phase on dynamic recrystallization behavior and hot workability of Mg–2.0Zn–0.3Zr–5.8Y alloy. Mater Sci Eng, A 599:150–159CrossRef
11.
go back to reference Lin XP, Dong Y, Xu R, Sun GF, Jiao SH (2011) Crystal morphologies and the phases in the Mg–6Zn–3Y alloy solidified under super-high pressure. Acta Metall Sin 47:1550–1554 Lin XP, Dong Y, Xu R, Sun GF, Jiao SH (2011) Crystal morphologies and the phases in the Mg–6Zn–3Y alloy solidified under super-high pressure. Acta Metall Sin 47:1550–1554
12.
go back to reference Lin XP, Dong Y, Xu R, Zheng RG, Jiao SH (2013) Solidification microstructures and crystalline morphologies of Mg–6Zn–Y alloy solidified under GPa level super-high pressure. Rare Metal Mater Eng 42:2309–2314 Lin XP, Dong Y, Xu R, Zheng RG, Jiao SH (2013) Solidification microstructures and crystalline morphologies of Mg–6Zn–Y alloy solidified under GPa level super-high pressure. Rare Metal Mater Eng 42:2309–2314
13.
go back to reference Lin XP, Dong Y, Xu R, Liu SJ, Tian SS (2014) Solidification process and formation of quasi-crystal phase in Mg–6Zn–1Y alloy under pressure in the order of GPa. Rare Metal Mater Eng 43:1117–1122CrossRef Lin XP, Dong Y, Xu R, Liu SJ, Tian SS (2014) Solidification process and formation of quasi-crystal phase in Mg–6Zn–1Y alloy under pressure in the order of GPa. Rare Metal Mater Eng 43:1117–1122CrossRef
14.
go back to reference Jie JC, Zou CM, Wang HW, Wei ZJ (2010) Microstructure evolution and precipitation of Al–12 Mg alloy solidified under high pressure. J Alloy Compd 506:L12–L15CrossRef Jie JC, Zou CM, Wang HW, Wei ZJ (2010) Microstructure evolution and precipitation of Al–12 Mg alloy solidified under high pressure. J Alloy Compd 506:L12–L15CrossRef
15.
go back to reference Zhao SS, Peng QM, Li H (2014) Effects of super-high pressure on microstructures, nano-mechanical behaviors and corrosion properties of Mg–Al alloys. J Alloy Compd 584:56–58CrossRef Zhao SS, Peng QM, Li H (2014) Effects of super-high pressure on microstructures, nano-mechanical behaviors and corrosion properties of Mg–Al alloys. J Alloy Compd 584:56–58CrossRef
16.
go back to reference Quey R, Driver JH (2011) Microtexture tracking of sub-boundary evolution during hot deformation of aluminium. Mater Charact 62:1222–1227CrossRef Quey R, Driver JH (2011) Microtexture tracking of sub-boundary evolution during hot deformation of aluminium. Mater Charact 62:1222–1227CrossRef
17.
go back to reference Liu MP, Roven HJ, Murashkin M, Valiev RZ (2009) Structural characterization by high-resolution electron microscopy of an Al–Mg alloy processed by high-pressure torsion. Mater Sci Eng, A 503:122–125CrossRef Liu MP, Roven HJ, Murashkin M, Valiev RZ (2009) Structural characterization by high-resolution electron microscopy of an Al–Mg alloy processed by high-pressure torsion. Mater Sci Eng, A 503:122–125CrossRef
18.
go back to reference Tang LH, Liu CM, Chen ZY, Ji DW, Xiao HC (2013) Microstructures and tensile properties of Mg–Gd–Y–Zr alloy during multidirectional forging at 773 K. Mater Des 50:587–596CrossRef Tang LH, Liu CM, Chen ZY, Ji DW, Xiao HC (2013) Microstructures and tensile properties of Mg–Gd–Y–Zr alloy during multidirectional forging at 773 K. Mater Des 50:587–596CrossRef
19.
go back to reference Mao PL, Yu JH, Liu Z, Dong Y (2013) Microstructure evolution of extruded Mg–Gd–Y magnesium alloy under dynamic compression. J Magnes Alloy 1:64–75CrossRef Mao PL, Yu JH, Liu Z, Dong Y (2013) Microstructure evolution of extruded Mg–Gd–Y magnesium alloy under dynamic compression. J Magnes Alloy 1:64–75CrossRef
20.
go back to reference Wu LY, Yang Z, Xia WJ, Chen ZH, Yang L (2012) The cyclic softening and evolution of microstructures for Mg–10Gd–2.0Y–0.46Zr alloy under low cycle fatigue at 573 K. Mater Des 36:47–53CrossRef Wu LY, Yang Z, Xia WJ, Chen ZH, Yang L (2012) The cyclic softening and evolution of microstructures for Mg–10Gd–2.0Y–0.46Zr alloy under low cycle fatigue at 573 K. Mater Des 36:47–53CrossRef
Metadata
Title
Hot compressive deformation behavior and electron backscattering diffraction analysis of Mg95.50Zn3.71Y0.79 fine-grained alloy solidified under high pressure
Authors
Fan Zhibin
Lin Xiaoping
Dong Yun
Xu Rui
Wang Lin
Publication date
23-10-2017
Publisher
Springer US
Published in
Journal of Materials Science / Issue 4/2018
Print ISSN: 0022-2461
Electronic ISSN: 1573-4803
DOI
https://doi.org/10.1007/s10853-017-1698-x

Other articles of this Issue 4/2018

Journal of Materials Science 4/2018 Go to the issue

Premium Partners