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Journal of Materials Science: Materials in Electronics

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08-04-2021

Impedance and Mössbauer spectroscopy study of BiCu₃Ti₃FeO₁₂ dielectric matrix

Authors: D. B. Freitas, M. H. Bezerra Júnior, R. G. M. Oliveira, J. E. V. de Morais, V. L. Bessa, F. F. Carmo, M. S. Pereira, I. F. Vasconcelos, M. A. S. Silva, H. D. de Andrade, I. S. Queiroz Júnior, R. S. Silva, A. S. B. Sombra

Published in: Journal of Materials Science: Materials in Electronics | Issue 9/2021

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Abstract

In the present work, an electroceramic of the perovskite family, BiCu₃Ti₃FeO₁₂ (BCTFO), was synthesized by the solid-state reaction method. The structural study was performed by X-ray diffraction and Mössbauer and Raman spectroscopy. Electric and dielectric properties were analyzed by impedance spectroscopy and the Hakki-Coleman method. Due to the BCTFO is isostructural of the CaCu₃Ti₄O₁₂ (CCTO), the BCTFO presents as a promissory electroceramic. Mössbauer spectroscopy reveals paramagnetic spectra to BCTFO, with two octahedral sites for iron ions. Regarding dielectric properties, for 1 Hz, BCTFO presents a high relative dielectric permittivity (ε_r ≈ 1 × 10⁴) and dielectric loss (tan δ > 1) and ε_r = 230.88, tan δ ≈ 1 × 10^–2 in the microwave range. The produced ceramic exhibited a high resonance frequency temperature coefficient (τ_f) with a value of + 2852 ppm °C⁻¹, making it a candidate for fabrication of the thermostable electroceramic composites with other ceramic matrices with negative τ_f values improving the thermal stability.

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Title: Impedance and Mössbauer spectroscopy study of BiCu3Ti3FeO12 dielectric matrix
Authors: D. B. Freitas
M. H. Bezerra Júnior
R. G. M. Oliveira
J. E. V. de Morais
V. L. Bessa
F. F. Carmo
M. S. Pereira
I. F. Vasconcelos
M. A. S. Silva
H. D. de Andrade
I. S. Queiroz Júnior
R. S. Silva
A. S. B. Sombra
Publication date: 08-04-2021
Publisher: Springer US
Published in: Journal of Materials Science: Materials in Electronics / Issue 9/2021
Print ISSN: 0957-4522
Electronic ISSN: 1573-482X
DOI: https://doi.org/10.1007/s10854-021-05768-y

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