Skip to main content
Top
Published in: Journal of Materials Engineering and Performance 2/2022

12-10-2021

Microstructure and Properties of Cu-0.4 wt.% Al2O3 Composites Fabricated by Hot Extrusion and Cold Drawing

Authors: Xiaowei Feng, Dongping Zhang, Bo Feng, Yingfei Lin, Juan Wang, Kaihong Zheng

Published in: Journal of Materials Engineering and Performance | Issue 2/2022

Log in

Activate our intelligent search to find suitable subject content or patents.

search-config
loading …

Abstract

In the present study, Cu-0.4 wt.% Al2O3 composites were successfully prepared by internal oxidation and hot extrusion followed by cold drawing. Microstructure, texture, mechanical properties and electrical conductivity of the Cu-0.4 wt.% Al2O3 composites were systematically studied. Our results show that the cold drawn S2 sample contains a much finer grain (about 1 μm) than the extruded S1 sample (about 3 μm). The S1 and S2 samples have a typical double fiber texture, with <100> and <111> parallel to extrusion direction (ED) or drawing direction (DD). The ultimate tensile strength, tensile yield strength and electrical conductivity of S1 sample are 460 MPa, 375 MPa and 90% IACS, respectively. After cold drawing, the S2 sample possesses a higher ultimate tensile strength (560 MPa) and tensile yield strength (520 MPa) than S1 sample, but a slightly lower electrical conductivity (87.5% IACS) than S1 sample. After annealing at 900 °C, the S1 and S2 samples also have a high microhardness of about 125 HV, which indicates that the Cu-0.4 wt.% Al2O3 composites have an excellent thermal stability.

Dont have a licence yet? Then find out more about our products and how to get one now:

Springer Professional "Wirtschaft+Technik"

Online-Abonnement

Mit Springer Professional "Wirtschaft+Technik" erhalten Sie Zugriff auf:

  • über 102.000 Bücher
  • über 537 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Finance + Banking
  • Management + Führung
  • Marketing + Vertrieb
  • Maschinenbau + Werkstoffe
  • Versicherung + Risiko

Jetzt Wissensvorsprung sichern!

Springer Professional "Technik"

Online-Abonnement

Mit Springer Professional "Technik" erhalten Sie Zugriff auf:

  • über 67.000 Bücher
  • über 390 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Maschinenbau + Werkstoffe




 

Jetzt Wissensvorsprung sichern!

Literature
1.
go back to reference W. Zeng, D. Zheng, H. Li, D. Zhou and D. Zhang, Using Intragranular and Intergranular Second Phase Particles Simultaneously to Achieve High Temperature Stabilization of Ultrafine Grained Cu, Mat. Sci. Eng. A, 2016, 670, p 41–48.CrossRef W. Zeng, D. Zheng, H. Li, D. Zhou and D. Zhang, Using Intragranular and Intergranular Second Phase Particles Simultaneously to Achieve High Temperature Stabilization of Ultrafine Grained Cu, Mat. Sci. Eng. A, 2016, 670, p 41–48.CrossRef
2.
go back to reference W. Zeng, J. Xie, D. Zhou, Z. Fu, D. Zhang and E.J. Lavernia, Bulk Cu-NbC Nanocomposites with High Strength and High Electrical Conductivity, J. Alloys Compd., 2018, 745, p 55–62.CrossRef W. Zeng, J. Xie, D. Zhou, Z. Fu, D. Zhang and E.J. Lavernia, Bulk Cu-NbC Nanocomposites with High Strength and High Electrical Conductivity, J. Alloys Compd., 2018, 745, p 55–62.CrossRef
3.
go back to reference I. Dinaharan, R. Sathiskumar and N. Murugan, Effect of Ceramic Particulate Type on Microstructure and Properties of Copper Matrix Composites Synthesized by Friction Stir Processing, J. Mater. Res. Technol., 2016, 5(4), p 302–316.CrossRef I. Dinaharan, R. Sathiskumar and N. Murugan, Effect of Ceramic Particulate Type on Microstructure and Properties of Copper Matrix Composites Synthesized by Friction Stir Processing, J. Mater. Res. Technol., 2016, 5(4), p 302–316.CrossRef
4.
go back to reference S.B. Chandrasekhar, N.P. Wasekar, M. Ramakrishna, P. Suresh Babu, T.N. Rao and B.P. Kashyap, Dynamic Strain Ageing in Fine Grained Cu-1 wt.%Al 2 O 3 Composite Processed by Two Step Ball Milling and Spark Plasma Sintering, J. Alloys Compd., 2016, 656, p 423–430.CrossRef S.B. Chandrasekhar, N.P. Wasekar, M. Ramakrishna, P. Suresh Babu, T.N. Rao and B.P. Kashyap, Dynamic Strain Ageing in Fine Grained Cu-1 wt.%Al 2 O 3 Composite Processed by Two Step Ball Milling and Spark Plasma Sintering, J. Alloys Compd., 2016, 656, p 423–430.CrossRef
5.
go back to reference D. Zhou, H. Geng, D. Zhang, W. Zeng, C. Kong and P. Munroe, An Insight into the Strain Rate Dependence of Tensile Ductility of an Ultrafine Grained Cu Matrix Nanocomposite, Mat. Sci. Eng. A, 2017, 688, p 164–168.CrossRef D. Zhou, H. Geng, D. Zhang, W. Zeng, C. Kong and P. Munroe, An Insight into the Strain Rate Dependence of Tensile Ductility of an Ultrafine Grained Cu Matrix Nanocomposite, Mat. Sci. Eng. A, 2017, 688, p 164–168.CrossRef
6.
go back to reference S.B. Chandrasekhar, S. Sudhakara Sarma, M. Ramakrishna, P. Suresh Babu, T.N. Rao and B.P. Kashyap, Microstructure and Properties of Hot Extruded Cu–1wt.% Al2O3 Nano-Composites Synthesized by Various Techniques, Mat. Sci. Eng. A, 2014, 591, p 46–53.CrossRef S.B. Chandrasekhar, S. Sudhakara Sarma, M. Ramakrishna, P. Suresh Babu, T.N. Rao and B.P. Kashyap, Microstructure and Properties of Hot Extruded Cu–1wt.% Al2O3 Nano-Composites Synthesized by Various Techniques, Mat. Sci. Eng. A, 2014, 591, p 46–53.CrossRef
7.
go back to reference V. Rajkovic, D. Bozic and M.T. Jovanovic, Effects of Copper and Al2O3 Particles on Characteristics of Cu–Al2O3 Composites, Mater. Design, 2010, 31, p 1962–1970.CrossRef V. Rajkovic, D. Bozic and M.T. Jovanovic, Effects of Copper and Al2O3 Particles on Characteristics of Cu–Al2O3 Composites, Mater. Design, 2010, 31, p 1962–1970.CrossRef
8.
go back to reference M.X. Guo, M.P. Wang, L.F. Cao and R.S. Lei, Work Softening Characterization of Alumina Dispersion Strengthened Copper Alloys, Mater. Charact., 2007, 58, p 928–935.CrossRef M.X. Guo, M.P. Wang, L.F. Cao and R.S. Lei, Work Softening Characterization of Alumina Dispersion Strengthened Copper Alloys, Mater. Charact., 2007, 58, p 928–935.CrossRef
9.
go back to reference D. Zhou, X. Wang, O. Muránsky, X. Wang, Y. Xie, C. Yang and D. Zhang, Heterogeneous Microstructure of an Al2O3 Dispersion Strengthened Cu by Spark Plasma Sintering and Extrusion and its Effect on Tensile Properties and Electrical Conductivity, Mat. Sci. Eng. A, 2018, 730, p 328–335.CrossRef D. Zhou, X. Wang, O. Muránsky, X. Wang, Y. Xie, C. Yang and D. Zhang, Heterogeneous Microstructure of an Al2O3 Dispersion Strengthened Cu by Spark Plasma Sintering and Extrusion and its Effect on Tensile Properties and Electrical Conductivity, Mat. Sci. Eng. A, 2018, 730, p 328–335.CrossRef
10.
go back to reference Y. Pan, S. Xiao, X. Lu, C. Zhou, Y. Li, Z. Liu, B. Liu, W. Xu, C. Jia and X. Qu, Fabrication, Mechanical Properties and Electrical Conductivity of Al2O3 Reinforced Cu/CNTs Composites, J. Alloys Compd., 2019, 782, p 1015–1023.CrossRef Y. Pan, S. Xiao, X. Lu, C. Zhou, Y. Li, Z. Liu, B. Liu, W. Xu, C. Jia and X. Qu, Fabrication, Mechanical Properties and Electrical Conductivity of Al2O3 Reinforced Cu/CNTs Composites, J. Alloys Compd., 2019, 782, p 1015–1023.CrossRef
11.
go back to reference Y. Shi, W. Chen, L. Dong, H. Li and Y. Fu, Enhancing Copper Infiltration into Alumina Using Spark Plasma Sintering to Achieve High Performance Al2O3/Cu Composites, Ceram. Int., 2018, 44, p 57–64.CrossRef Y. Shi, W. Chen, L. Dong, H. Li and Y. Fu, Enhancing Copper Infiltration into Alumina Using Spark Plasma Sintering to Achieve High Performance Al2O3/Cu Composites, Ceram. Int., 2018, 44, p 57–64.CrossRef
12.
go back to reference K. Ďurišinová, J. Ďurišin, M. Orolínová, M. Ďurišin and J. Szabó, Effect of Mechanical Milling on Nanocrystalline Grain Stability and Properties of Cu–Al2O3 Composite Prepared by Thermo-Chemical Technique and Hot Extrusion, J. Alloys Compd., 2015, 618, p 204–209.CrossRef K. Ďurišinová, J. Ďurišin, M. Orolínová, M. Ďurišin and J. Szabó, Effect of Mechanical Milling on Nanocrystalline Grain Stability and Properties of Cu–Al2O3 Composite Prepared by Thermo-Chemical Technique and Hot Extrusion, J. Alloys Compd., 2015, 618, p 204–209.CrossRef
13.
go back to reference Y. Dong, X. Wang, Y. Xie, C. Yang and D. Zhou, Tunable Microstructures and Tensile Mechanical Properties of Oxide-Dispersion-Strengthened Cu by Extrusion and Secondary Processing, J. Alloys Compd., 2020, 812, p 152112.CrossRef Y. Dong, X. Wang, Y. Xie, C. Yang and D. Zhou, Tunable Microstructures and Tensile Mechanical Properties of Oxide-Dispersion-Strengthened Cu by Extrusion and Secondary Processing, J. Alloys Compd., 2020, 812, p 152112.CrossRef
14.
go back to reference X.-H. Zhang, X.-X. Li, H. Chen, T.-B. Li, W. Su and S.-D. Guo, Investigation on Microstructure and Properties of Cu–Al2O3 Composites Fabricated by a Novel In-situ Reactive Synthesis, Mater. Design, 2016, 92, p 58–63.CrossRef X.-H. Zhang, X.-X. Li, H. Chen, T.-B. Li, W. Su and S.-D. Guo, Investigation on Microstructure and Properties of Cu–Al2O3 Composites Fabricated by a Novel In-situ Reactive Synthesis, Mater. Design, 2016, 92, p 58–63.CrossRef
15.
go back to reference H. Zhuo, J. Tang and N. Ye, A Novel Approach for Strengthening Cu–Y2O3 Composites by In situ Reaction at Liquidus Temperature, Mat. Sci. Eng. A, 2013, 584, p 1–6.CrossRef H. Zhuo, J. Tang and N. Ye, A Novel Approach for Strengthening Cu–Y2O3 Composites by In situ Reaction at Liquidus Temperature, Mat. Sci. Eng. A, 2013, 584, p 1–6.CrossRef
16.
go back to reference J. Lee, Y.C. Kim, S. Lee, S. Ahn and N.J. Kim, Correlation of the Microstructure and Mechanical Properties of Oxide-Dispersion-Strengthened Coppers Fabricated by Internal Oxidation, Metall. Mater. Trans. A-Phys. Metall. Mater. Sci., 2004, 35A, p 493–502.CrossRef J. Lee, Y.C. Kim, S. Lee, S. Ahn and N.J. Kim, Correlation of the Microstructure and Mechanical Properties of Oxide-Dispersion-Strengthened Coppers Fabricated by Internal Oxidation, Metall. Mater. Trans. A-Phys. Metall. Mater. Sci., 2004, 35A, p 493–502.CrossRef
17.
go back to reference K. Song, J. Xing, Q. Dong, P. Liu, B. Tian and X. Cao, Internal Oxidation of Dilute Cu–Al alloy Powers with Oxidant of Cu2O, Mat. Sci. Eng. A, 2004, 380, p 117–122.CrossRef K. Song, J. Xing, Q. Dong, P. Liu, B. Tian and X. Cao, Internal Oxidation of Dilute Cu–Al alloy Powers with Oxidant of Cu2O, Mat. Sci. Eng. A, 2004, 380, p 117–122.CrossRef
18.
go back to reference C. Li, Y. Xie, D. Zhou, W. Zeng, J. Wang, J. Liang and D. Zhang, A Novel Way for Fabricating Ultrafine Grained Cu-4.5 vol% Al2O3 Composite with High Strength and Electrical Conductivity, Mater. Charact., 2019, 155, p 109775.CrossRef C. Li, Y. Xie, D. Zhou, W. Zeng, J. Wang, J. Liang and D. Zhang, A Novel Way for Fabricating Ultrafine Grained Cu-4.5 vol% Al2O3 Composite with High Strength and Electrical Conductivity, Mater. Charact., 2019, 155, p 109775.CrossRef
19.
go back to reference F. Ren, A. Zhi, D. Zhang, B. Tian, A.A. Volinsky and X. Shen, Preparation of Cu–Al2O3 Bulk Nano-Composites by Combining Cu–Al Alloy Sheets Internal Oxidation with Hot Extrusion, J. Alloys Compd., 2015, 633, p 323–328.CrossRef F. Ren, A. Zhi, D. Zhang, B. Tian, A.A. Volinsky and X. Shen, Preparation of Cu–Al2O3 Bulk Nano-Composites by Combining Cu–Al Alloy Sheets Internal Oxidation with Hot Extrusion, J. Alloys Compd., 2015, 633, p 323–328.CrossRef
20.
go back to reference G.K. Williamson and W.H. Hall, X-ray Line Broadening from Filed Aluminium and Wol-fram, Acta Metall., 1953, 1, p 22–31.CrossRef G.K. Williamson and W.H. Hall, X-ray Line Broadening from Filed Aluminium and Wol-fram, Acta Metall., 1953, 1, p 22–31.CrossRef
21.
go back to reference G.K. Williamson, R.E. Smallman (1956) Dislocation Densities in Some Annealed and Cold-Worked Metals from Measurements on the x-ray Debye-Scherrer Spectrum, Philos. Mag.: 134–46. G.K. Williamson, R.E. Smallman (1956) Dislocation Densities in Some Annealed and Cold-Worked Metals from Measurements on the x-ray Debye-Scherrer Spectrum, Philos. Mag.: 134–46.
22.
go back to reference C. Li, W. Zeng, Y. Xie, J. Wang, J. Liang, R.E. Logé and D. Zhang, Annealing Hardening and Softening of an Ultrafine Grained Cu-4.5vol.%Al2O3 Nanocomposite, Mat. Sci. Eng. A, 2020, 778, p 139126.CrossRef C. Li, W. Zeng, Y. Xie, J. Wang, J. Liang, R.E. Logé and D. Zhang, Annealing Hardening and Softening of an Ultrafine Grained Cu-4.5vol.%Al2O3 Nanocomposite, Mat. Sci. Eng. A, 2020, 778, p 139126.CrossRef
23.
go back to reference L. Guobin, S. Jibing, G. Quanmei and W. Ru, Fabrication of the Nanometer Al2O3/Cu Composite by Internal Oxidation, J. Mater. Process. Tech., 2005, 170, p 336–340.CrossRef L. Guobin, S. Jibing, G. Quanmei and W. Ru, Fabrication of the Nanometer Al2O3/Cu Composite by Internal Oxidation, J. Mater. Process. Tech., 2005, 170, p 336–340.CrossRef
24.
go back to reference D. Zhou, W. Zeng and D. Zhang, A Feasible Ultrafine Grained Cu Matrix Composite Microstructure for Achieving High Strength and High Electrical Conductivity, J. Alloys Compd., 2016, 682, p 590–593.CrossRef D. Zhou, W. Zeng and D. Zhang, A Feasible Ultrafine Grained Cu Matrix Composite Microstructure for Achieving High Strength and High Electrical Conductivity, J. Alloys Compd., 2016, 682, p 590–593.CrossRef
25.
go back to reference F. Wang, Y. Li, K. Yamanaka, K. Wakon, K. Harata and A. Chiba, Influence of Two-step Ball-Milling Condition on Electrical and Mechanical Properties of TiC-Dispersion-Strengthened Cu Alloys, Mater. Design, 2014, 64, p 441–449.CrossRef F. Wang, Y. Li, K. Yamanaka, K. Wakon, K. Harata and A. Chiba, Influence of Two-step Ball-Milling Condition on Electrical and Mechanical Properties of TiC-Dispersion-Strengthened Cu Alloys, Mater. Design, 2014, 64, p 441–449.CrossRef
26.
go back to reference J. Lee, J.Y. Jung, E.-S. Lee, W.J. Park, S. Ahn and N.J. Kim, Microstructure and Properties of Titanium Boride Dispersed Cu Alloys Fabricated by Spray Forming, Mat. Sci. Eng. A, 2000, 277, p 274–283.CrossRef J. Lee, J.Y. Jung, E.-S. Lee, W.J. Park, S. Ahn and N.J. Kim, Microstructure and Properties of Titanium Boride Dispersed Cu Alloys Fabricated by Spray Forming, Mat. Sci. Eng. A, 2000, 277, p 274–283.CrossRef
27.
go back to reference K. Huang, Q. Zhao, Y. Li and K. Marthinsen, Two-stage Annealing of a Cold-Rolled Al–Mn–Fe–Si Alloy with Different Microchemistry States, J. Mater. Process. Tech., 2015, 221, p 87–99.CrossRef K. Huang, Q. Zhao, Y. Li and K. Marthinsen, Two-stage Annealing of a Cold-Rolled Al–Mn–Fe–Si Alloy with Different Microchemistry States, J. Mater. Process. Tech., 2015, 221, p 87–99.CrossRef
28.
go back to reference Z. Zhang and D. Chen, Consideration of Orowan Strengthening Effect in Particulate-Reinforced Metal Matrix Nanocomposites: A Model for Predicting Their Yield Strength, Scripta Mater., 2006, 54, p 1321–1326.CrossRef Z. Zhang and D. Chen, Consideration of Orowan Strengthening Effect in Particulate-Reinforced Metal Matrix Nanocomposites: A Model for Predicting Their Yield Strength, Scripta Mater., 2006, 54, p 1321–1326.CrossRef
Metadata
Title
Microstructure and Properties of Cu-0.4 wt.% Al2O3 Composites Fabricated by Hot Extrusion and Cold Drawing
Authors
Xiaowei Feng
Dongping Zhang
Bo Feng
Yingfei Lin
Juan Wang
Kaihong Zheng
Publication date
12-10-2021
Publisher
Springer US
Published in
Journal of Materials Engineering and Performance / Issue 2/2022
Print ISSN: 1059-9495
Electronic ISSN: 1544-1024
DOI
https://doi.org/10.1007/s11665-021-06247-5

Other articles of this Issue 2/2022

Journal of Materials Engineering and Performance 2/2022 Go to the issue

Premium Partners