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Published in: Journal of Materials Science: Materials in Electronics 9/2014

01-09-2014

One step synthesis of β-FeOOH nanowire bundles/graphene oxide nanocomposites

Authors: Hao-Jie Song, Xueqiang Zhang, Tao Chen

Published in: Journal of Materials Science: Materials in Electronics | Issue 9/2014

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Abstract

A nanocomposite of graphene oxide (GO) and β-ferric oxyhydroxide (β-FeOOH) nanowire bundles is synthesized by in situ hydrolysis of the precursor ferric chloride and GO nanosheets. Characterization by X-ray diffraction, transmission electron microscopy, and thermogravimetric analysis established the composite structure of the synthesized sample. The results revealed that the surface of GO nanosheets was uniformly assembled by numerous nanowire bundles with diameters in the range of 30–50 nm and lengths of 100–150 nm. Furthermore, β-FeOOH/GO nanocomposites showed a very high adsorption capacity of Congo red and thus these nanocomposites can be used as good adsorbents and can be used for the removal of organic dye from the waste water system.

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Literature
1.
go back to reference M.C.S. Faria, R.S. Rosemberg, C.A. Bomfeti, D.S. Monteiro, F. Barbosa, L.C.A. Oliveira, M. Rodriguez, M.C. Pereira, J.L. Rodrigues, Arsenic removal from contaminated water by ultrafine FeOOH adsorbents. Chem. Eng. J. 237, 47–54 (2014)CrossRef M.C.S. Faria, R.S. Rosemberg, C.A. Bomfeti, D.S. Monteiro, F. Barbosa, L.C.A. Oliveira, M. Rodriguez, M.C. Pereira, J.L. Rodrigues, Arsenic removal from contaminated water by ultrafine FeOOH adsorbents. Chem. Eng. J. 237, 47–54 (2014)CrossRef
2.
go back to reference B. Nowack, A.T. Stone, Competitive adsorption of phosphate and phosphonates onto goethite. Water Res. 40, 2201–2209 (2006)CrossRef B. Nowack, A.T. Stone, Competitive adsorption of phosphate and phosphonates onto goethite. Water Res. 40, 2201–2209 (2006)CrossRef
3.
go back to reference B. Wang, H.B. Wu, L. Yu, R. Xu, T.T. Lim, X.W. Lou, Template-free formation of uniform urchin-like α-FeOOH hollow spheres with superior capability for water treatment. Adv. Mater. 24, 1111–1116 (2012)CrossRef B. Wang, H.B. Wu, L. Yu, R. Xu, T.T. Lim, X.W. Lou, Template-free formation of uniform urchin-like α-FeOOH hollow spheres with superior capability for water treatment. Adv. Mater. 24, 1111–1116 (2012)CrossRef
4.
go back to reference K. Amstaetter, T. Borch, P. Larese-Casanova, A. Kappler, Redox transformation of arsenic by FeII-activated goethite (α-FeOOH). Environ. Sci. Technol. 44, 102–108 (2010)CrossRef K. Amstaetter, T. Borch, P. Larese-Casanova, A. Kappler, Redox transformation of arsenic by FeII-activated goethite (α-FeOOH). Environ. Sci. Technol. 44, 102–108 (2010)CrossRef
5.
go back to reference H. Li, W. Li, Y.J. Zhang, T.S. Wang, B. Wang, W. Xu, L. Jiang, W.G. Song, C.Y. Shu, C.R. Wang, Chrysanthemum-like α-FeOOH microspheres produced by a simple green method and their outstanding ability in heavy metal ion removal. J. Mater. Chem. 21, 7878–7881 (2011) H. Li, W. Li, Y.J. Zhang, T.S. Wang, B. Wang, W. Xu, L. Jiang, W.G. Song, C.Y. Shu, C.R. Wang, Chrysanthemum-like α-FeOOH microspheres produced by a simple green method and their outstanding ability in heavy metal ion removal. J. Mater. Chem. 21, 7878–7881 (2011)
6.
7.
go back to reference G. Eda, M. Chhowalla, Chemically derived graphene oxide: towards large-area thin-film electronics and optoelectronics. Adv. Mater. 22, 2392–2415 (2010)CrossRef G. Eda, M. Chhowalla, Chemically derived graphene oxide: towards large-area thin-film electronics and optoelectronics. Adv. Mater. 22, 2392–2415 (2010)CrossRef
8.
go back to reference J. Liu, Y. Xue, Y. Gao, D. Yu, M. Durstock, L. Dai, Hole and electron extraction layers based on graphene oxide derivatives for high-performance bulk heterojunction solar cells. Adv. Mater. 24, 2228–2233 (2012)CrossRef J. Liu, Y. Xue, Y. Gao, D. Yu, M. Durstock, L. Dai, Hole and electron extraction layers based on graphene oxide derivatives for high-performance bulk heterojunction solar cells. Adv. Mater. 24, 2228–2233 (2012)CrossRef
9.
go back to reference X. Li, W. Qi, D. Mei, M.L. Sushko, I. Aksay, J. Liu, Functionalized graphene sheets as molecular templates for controlled nucleation and self-assembly of metal oxide-graphene nanocomposites. Adv. Mater. 24, 5136–5141 (2012)CrossRef X. Li, W. Qi, D. Mei, M.L. Sushko, I. Aksay, J. Liu, Functionalized graphene sheets as molecular templates for controlled nucleation and self-assembly of metal oxide-graphene nanocomposites. Adv. Mater. 24, 5136–5141 (2012)CrossRef
10.
go back to reference X.H. Jia, H.J. Song, Hydrothermal synthesis of flower-like TiO2 nanocrystals/graphene oxide nanocomposites. Appl. Phys. A 109, 261–265 (2013)CrossRef X.H. Jia, H.J. Song, Hydrothermal synthesis of flower-like TiO2 nanocrystals/graphene oxide nanocomposites. Appl. Phys. A 109, 261–265 (2013)CrossRef
11.
go back to reference H.J. Song, X.H. Jia, N. Li, X.F. Yang, H. Tang, Synthesis of α-Fe2O3 nanorod/graphene oxide composites and their tribological properties. J. Mater. Chem. 22, 895–902 (2012) H.J. Song, X.H. Jia, N. Li, X.F. Yang, H. Tang, Synthesis of α-Fe2O3 nanorod/graphene oxide composites and their tribological properties. J. Mater. Chem. 22, 895–902 (2012)
12.
go back to reference L.S. Zhou, F.P. Shen, X.K. Tian, D.H. Wang, T. Zhang, W. Chen, Stable Cu2O nanocrystals grown on functionalized graphene sheets and room temperature H2S gas sensing with ultrahigh sensitivity. Nanoscale 5, 1564–1569 (2013)CrossRef L.S. Zhou, F.P. Shen, X.K. Tian, D.H. Wang, T. Zhang, W. Chen, Stable Cu2O nanocrystals grown on functionalized graphene sheets and room temperature H2S gas sensing with ultrahigh sensitivity. Nanoscale 5, 1564–1569 (2013)CrossRef
13.
go back to reference Y. Liang, Y. Li, H. Wang, J. Zhou, J. Wang, T. Regier, H. Dai, Co3O4 nanocrystals on graphene as a synergistic catalyst for oxygen reduction reaction. Nat. Mater. 10, 780–788 (2011) Y. Liang, Y. Li, H. Wang, J. Zhou, J. Wang, T. Regier, H. Dai, Co3O4 nanocrystals on graphene as a synergistic catalyst for oxygen reduction reaction. Nat. Mater. 10, 780–788 (2011)
14.
go back to reference H.L. Wang, L.F. Cui, Y.A. Yang, H.S. Casalongue, J.T. Robinson, Y.Y. Liang, Y. Cui, H.J. Dai, Mn3O4–graphene hybrid as a high-capacity anode material for lithium ion batteries. J. Am. Chem. Soc. 132, 13978–13980 (2010)CrossRef H.L. Wang, L.F. Cui, Y.A. Yang, H.S. Casalongue, J.T. Robinson, Y.Y. Liang, Y. Cui, H.J. Dai, Mn3O4–graphene hybrid as a high-capacity anode material for lithium ion batteries. J. Am. Chem. Soc. 132, 13978–13980 (2010)CrossRef
15.
go back to reference N. Li, G. Liu, C. Zhen, F. Li, L.L. Zhang, H.M. Cheng, Battery performance and photocatalytic activity of mesoporous anatase TiO2 nanospheres/graphene composites by template-free self-assembly. Adv. Funct. Mater. 21, 1717–1722 (2011)CrossRef N. Li, G. Liu, C. Zhen, F. Li, L.L. Zhang, H.M. Cheng, Battery performance and photocatalytic activity of mesoporous anatase TiO2 nanospheres/graphene composites by template-free self-assembly. Adv. Funct. Mater. 21, 1717–1722 (2011)CrossRef
16.
go back to reference Y.M. Sun, X.L. Hu, W. Luo, H.H. Xu, C.C. Hu, Y.H. Huang, Synthesis of amorphous FeOOH/reduced graphene oxide composite by infrared irradiation and its superior lithium storage performance. ACS Appl. Mater. Interfaces 5, 10145–10150 (2013)CrossRef Y.M. Sun, X.L. Hu, W. Luo, H.H. Xu, C.C. Hu, Y.H. Huang, Synthesis of amorphous FeOOH/reduced graphene oxide composite by infrared irradiation and its superior lithium storage performance. ACS Appl. Mater. Interfaces 5, 10145–10150 (2013)CrossRef
17.
go back to reference G.B. Huang, C.C. Zhang, Y. Long, J. Wynn, Y. Liu, W. Wang, J.P. Gao, Low temperature preparation of alpha-FeOOH/reduced graphene oxide and its catalytic activity for the photodegradation of an organic dye. Nanotechnology 24, 395601 (2013)CrossRef G.B. Huang, C.C. Zhang, Y. Long, J. Wynn, Y. Liu, W. Wang, J.P. Gao, Low temperature preparation of alpha-FeOOH/reduced graphene oxide and its catalytic activity for the photodegradation of an organic dye. Nanotechnology 24, 395601 (2013)CrossRef
18.
go back to reference F.M. Peng, T. Luo, L.G. Qiu, Y.P. Yuan, An easy method to synthesize graphene oxide–FeOOH composites and their potential application in water purification. Mater. Res. Bull. 48, 2180–2185 (2013)CrossRef F.M. Peng, T. Luo, L.G. Qiu, Y.P. Yuan, An easy method to synthesize graphene oxide–FeOOH composites and their potential application in water purification. Mater. Res. Bull. 48, 2180–2185 (2013)CrossRef
19.
go back to reference W.S. Hummers, R.E. Offeman, Preparation of graphitic oxide. J. Am. Chem. Soc. 80, 1339 (1958)CrossRef W.S. Hummers, R.E. Offeman, Preparation of graphitic oxide. J. Am. Chem. Soc. 80, 1339 (1958)CrossRef
20.
go back to reference B.J. Tan, K.J. Klabunde, P.M.A. Sherwood, X-ray photoelectron spectroscopy studies of solvated metal atom dispersed catalysts. Monometallic iron and bimetallic iron-cobalt particles on alumina. Chem. Mater. 2, 186–191 (1990)CrossRef B.J. Tan, K.J. Klabunde, P.M.A. Sherwood, X-ray photoelectron spectroscopy studies of solvated metal atom dispersed catalysts. Monometallic iron and bimetallic iron-cobalt particles on alumina. Chem. Mater. 2, 186–191 (1990)CrossRef
Metadata
Title
One step synthesis of β-FeOOH nanowire bundles/graphene oxide nanocomposites
Authors
Hao-Jie Song
Xueqiang Zhang
Tao Chen
Publication date
01-09-2014
Publisher
Springer US
Published in
Journal of Materials Science: Materials in Electronics / Issue 9/2014
Print ISSN: 0957-4522
Electronic ISSN: 1573-482X
DOI
https://doi.org/10.1007/s10854-014-2075-z

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