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Journal of Materials Engineering and Performance
Published in: Journal of Materials Engineering and Performance 4/2022

29-11-2021 | Technical Article

Role of Initial Surface Roughness in Different Oxidation Stages of TP347H at 700 °C

Authors: Jian Li, Tieshan Cao, Conghui Zhang, Congqian Cheng, Jie Zhao

Published in: Journal of Materials Engineering and Performance | Issue 4/2022

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Abstract

The role of surface roughness in different oxidation stages of TP347H was investigated in detail at 700 °C. At the initial stage, the increase in roughness increased the growth rate of the oxide on the surface, prompting the oxidation to enter the diffusion-controlled stage due to the formation of the continuous Cr-rich oxide film. In long-term oxidation, a structurally stable dual-layer oxide film, including the (Cr, Fe, Mn)3O4 (spinel-type) outer layer and the inner layer mixed of Cr2O3 and FeCr2O4, is formed on the rough samples. Instead, a three-layer structure with a thick magnetite layer is formed on the out surface of the smooth samples. The critical strain value for oxide scale fracture decreases as the thickness of the magnetite layer increases, which may cause the spalling of the oxide. The mechanism of the effect of roughness on oxidation was also discussed.
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Metadata
Title
Role of Initial Surface Roughness in Different Oxidation Stages of TP347H at 700 °C
Authors
Jian Li
Tieshan Cao
Conghui Zhang
Congqian Cheng
Jie Zhao
Publication date
29-11-2021
Publisher
Springer US
Published in
Journal of Materials Engineering and Performance / Issue 4/2022
Print ISSN: 1059-9495
Electronic ISSN: 1544-1024
DOI
https://doi.org/10.1007/s11665-021-06452-2

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