Skip to main content
Disciplines
Automotive Business IT + Informatics Construction + Real Estate Electrical Engineering + Electronics Energy + Sustainability Insurance + Risk Finance + Banking Management + Leadership Marketing + Sales Mechanical Engineering + Materials
Events
DE
EN
Books
Journals
Topic Page
Marketing
Start single access now
Access for companies
EXTENDED SEARCH
Log in
Top
Journal of Materials Science: Materials in Electronics
Published in: Journal of Materials Science: Materials in Electronics 4/2019

02-01-2019

Synthesis of phosphate-modified zeolite as a modifier in carbon paste electrode for nitrite electrochemical detection

Authors: Adamu Idris, Tawfik Saleh, Oki Muraza, Mohammed Sanhoob, Md. Abdul Aziz, Abdul-Rahman Al-Betar

Published in: Journal of Materials Science: Materials in Electronics | Issue 4/2019

Log in

Activate our intelligent search to find suitable subject content or patents.

search-config
loading …

Abstract

In this work, template-free synthesis of phosphate mordenite zeolites was carried out. Post synthesis impregnation using phosphoric acid was applied to add phosphate group to zeolite framework, i.e. P-loading. Phosphate modification led to disruption of bridging hydroxyl and silanol groups as confirmed by FT-IR spectra. EDX spectra showed that the Si/Al ratio of the zeolite increases with the amount of P-loading and 27Al NMR revealed the formation of aluminophosphate on mordenite. The modified electrodes of phosphate mordenite zeolite were used for the electrocatalytic oxidation of nitrite, which was investigated by using square wave voltammetry. The effect of different electrolytes and pH values were also investigated and the calibration curve of nitrite oxidation at phosphate mordenite carbon paste electrodes showed a linear dependence.
previous article Design and fabrication of double AlGaN/GaN distributed Bragg reflector stack mirror for the application of GaN-based optoelectronic devices
next article High capable visible light driven photocatalytic activity of WO3/g-C3N4 hetrostructure catalysts synthesized by a novel one step microwave irradiation route

Dont have a licence yet? Then find out more about our products and how to get one now:

Springer Professional "Wirtschaft+Technik"

Online-Abonnement

Mit Springer Professional "Wirtschaft+Technik" erhalten Sie Zugriff auf:

  • über 102.000 Bücher
  • über 537 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Finance + Banking
  • Management + Führung
  • Marketing + Vertrieb
  • Maschinenbau + Werkstoffe
  • Versicherung + Risiko

Jetzt Wissensvorsprung sichern!

inform now

Springer Professional "Technik"

Online-Abonnement

Mit Springer Professional "Technik" erhalten Sie Zugriff auf:

  • über 67.000 Bücher
  • über 390 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Maschinenbau + Werkstoffe




 

Jetzt Wissensvorsprung sichern!

inform now

Springer Professional "Wirtschaft"

Online-Abonnement

Mit Springer Professional "Wirtschaft" erhalten Sie Zugriff auf:

  • über 67.000 Bücher
  • über 340 Zeitschriften

aus folgenden Fachgebieten:

  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Finance + Banking
  • Management + Führung
  • Marketing + Vertrieb
  • Versicherung + Risiko




Jetzt Wissensvorsprung sichern!

inform now
Literature
1.
A. Wachter, Sodium nitrite as corrosion inhibitor for water. Ind. Eng. Chem. 37, 749–751 (1945)CrossRef
2.
A. Rahim, L.S.S. Santos, S.B.A. Barros, L.T. Kubota, R. Landers, Y. Gushikem, Electrochemical detection of nitrite in meat and water samples using a mesoporous carbon ceramic SiO2/c electrode modified with in situ generated manganese(II) phthalocyanine. Electroanalysis 26, 541–547 (2014)CrossRef
3.
K. Fan, J. Wu, Construction of a carbon paste electrode based on ionic liquid for trace electrochemical detection of nitrite in food samples. Anal. Methods 5, 5146–5153 (2013)CrossRef
4.
A. Ianoul, T. Coleman, S.A. Asher, UV resonance Raman spectroscopic detection of nitrate and nitrite in wastewater treatment processes. Anal. Chem. 74, 1458–1461 (2002)CrossRef
5.
D.C. Siu, A. Henshall, Ion chromatographic determination of nitrate and nitrite in meat products. J. Chromatogr. A 804, 157–160 (1998)CrossRef
6.
E. Martínková, T. Křžek, P. Coufal, Determination of nitrites and nitrates in drinking water using capillary electrophoresis. Chem. Pap. 68, 1008–1014 (2014)CrossRef
7.
E. Nagababu, J. Rifkind, Measurement of plasma nitrite by chemiluminescence. In: Free Radicals and Antioxidant Protocols, eds. by R.M. Uppu, S.N. Murthy, W.A. Pryor, N.L. Parinandi (Humana Press, New York, 2010), pp. 41–49
8.
Y. Cui, C. Yang, W. Zeng, M. Oyama, W. Pu, J. Zhang, Electrochemical determination of nitrite using a gold nanoparticles-modified glassy carbon electrode prepared by the seed-mediated growth technique. Anal. Sci. 23, 1421–1425 (2007)CrossRef
9.
A. Walcarius, P. Mariaulle, C. Louis, L. Lamberts, Amperometric detection of nonelectroactive cations in electrolyte-free flow systems at zeolite modified electrodes. Electroanalysis 11, 393–400 (1999)CrossRef
10.
W. Xiong, M.D. Baker, Electrochemistry of zeolites on thickness shear mode oscillators. J. Phys. Chem. B 109, 13590–13596 (2005)CrossRef
11.
B.R. Shaw, K.E. Creasy, Carbon composite electrodes containing alumina, layered double hydroxides, and zeolites. J. Electroanal. Chem. Interfacial Electrochem. 243, 209–217 (1988)CrossRef
12.
L.M. Muresan, Zeolite-modified electrodes with analytical applications. Pure Appl. Chem. 83, 325–343 (2010)CrossRef
13.
C. Senaratne, J. Zhang, M.D. Baker, C.A. Bessel, D.R. Rolison, Zeolite-modified electrodes: intra-versus extrazeolite electron transfer. J. Phys. Chem. 100, 5849–5862 (1996)CrossRef
14.
Y. Zheng, X. Li, P.K. Dutta, Exploitation of unique properties of zeolites in the development of gas sensors, Sensors (Basel), 12, 5170–5194 (2012)CrossRef
15.
D.B. Lukyanov, T. Vazhnova, N. Cherkasov, J.L. Casci, J.J. Birtill, Insights into Brønsted acid sites in the zeolite mordenite. J. Phys. Chem. C 118, 23918–23929 (2014)CrossRef
16.
A. Corma, J. Mengual, P.J. Miguel, Stabilization of ZSM-5 zeolite catalysts for steam catalytic cracking of naphtha for production of propene and ethene. Appl. Catal. A 421–422, 121–134 (2012)CrossRef
17.
M. Dyballa, E. Klemm, J. Weitkamp, M. Hunger, Effect of phosphate modification on the Brønsted acidity and methanol-to-olefin conversion activity of zeolite ZSM-5. Chem. Ing. Tec. 85, 1719–1725 (2013)CrossRef
18.
J. Li, H. Ma, H. Zhang, Q. Sun, W. Ying, Catalytic cracking of butene to propylene over modified HZSM-5 zeolites. Int. J. Chem. Nucl. Metall. Mater. Eng. 8, 590–593 (2014)
19.
P. Zeng, Y. Liang, S. Ji, B. Shen, H. Liu, B. Wang, H. Zhao, M. Li, Preparation of phosphorus-modified PITQ-13 catalysts and their performance in 1-butene catalytic cracking. J. Energy Chem. 23, 193–200 (2014)CrossRef
20.
N. Chen, T.F. Degnan Jr., C.M. Smith, Molecular Transport And Reaction in Zeolites: Design and Application of Shape Selective Catalysis (Wiley, New York, 1994)
21.
H.E. van der Bij, L.R. Aramburo, B. Arstad, J.J. Dynes, J. Wang, B.M. Weckhuysen, Phosphatation of zeolite H-ZSM-5: a combined microscopy and spectroscopy study, ChemPhysChem 15, 283–292 (2014)CrossRef
22.
M.M. Ardakani, Z. Akrami, H. Kazemian, H. Zare, Accumulation and voltammetric determination of cobalt at zeolite-modified electrodes. J. Anal. Chem. 63, 184–191 (2008)CrossRef
23.
B.O. Hincapie, L.J. Garces, Q. Zhang, A. Sacco, S.L. Suib, Synthesis of mordenite nanocrystals. Microporous Mesoporous Mater. 67, 19–26 (2004)CrossRef
24.
Y. Mao, Y. Zhou, H. Wen, J. Xie, W. Zhang, J. Wang, Morphology-controlled synthesis of large mordenite crystals, New J. Chem. 38, 3295–3301 (2014)CrossRef
25.
S. Patwardhan, Sol-gel synthesis of zeolites: effect of process parameters. Zeolites: synthesis, characterization and applications. Project 20-254-689 (2001)
26.
J. Pinkas, Chemistry of silicates and aluminosilicates. Ceramics−Silikáty 49, 287–298 (2005)
27.
J. Caro, M. Bülow, M. Derewinski, J. Haber, M. Hunger, J. Kärger, H. Pfeifer, W. Storek, B. Zibrowius, NMR and IR studies of zeolite H-ZSM-5 modified with orthophosphoric acid. J. Catal. 124, 367–375 (1990)CrossRef
28.
S. van Donk, J. Bitter, M. Versluijs-Helder, A. Verberckmoes, K. de Jong, Probing the micropore accessibility in mordenite crystals using diffusion and coking studies, in: NAM-18 (2003)
29.
C.B. Ahlers, J.B. Talbot, Voltammetric behavior of zeolite-modified electrodes fabricated by electrophoretic deposition. Electrochim. Acta 45, 3379–3387 (2000)CrossRef
30.
H.M.J. Li, H. Zhang, Q. Sun, W. Ying, Catalytic cracking of butene to propylene over modified HZSM-5 zeolites. Int. J. Chem. Nucl. Metall. Mater. Eng. 8, 604–608 (2014)
31.
H.E. van der Bij, D. Cicmil, J. Wang, F. Meirer, F.M.F. de Groot, B.M. Weckhuysen, Aluminum-phosphate binder formation in zeolites as probed with X-ray absorption microscopy. J. Am. Chem. Soc. 136, 17774–17787 (2014)CrossRef
32.
T. Blasco, A. Corma, J. Martínez-Triguero, Hydrothermal stabilization of ZSM-5 catalytic-cracking additives by phosphorus addition. J. Catal. 237, 267–277 (2006)CrossRef
33.
X.D. Peng, G.E. Parris, B.A. Toseland, P.J. Battavio, Use of aluminum phosphate as the dehydration catalyst in single step dimethyl ether process, in Google Patents (1998)
34.
M.I. Prodromidis, A.B. Florou, S.M. Tzouwara-Karayanni, M.I. Karayannis, The importance of surface coverage in the electrochemical study of chemically modified electrodes. Electroanalysis 12, 1498–1501 (2000)CrossRef
35.
M. Bertotti, D. Pletcher, A study of nitrite oxidation at platinum microelectrodes. J. Braz. Chem. Soc. 8, 391–395 (1997)CrossRef
36.
A. Marlinda, A. Pandikumar, N. Yusoff, N. Huang, H. Lim, Electrochemical sensing of nitrite using a glassy carbon electrode modified with reduced functionalized graphene oxide decorated with flower-like zinc oxide. Microchim. Acta 182, 1113–1122 (2015)CrossRef
37.
M.A. Kamyabi, F. Aghajanloo, Electrocatalytic oxidation and determination of nitrite on carbon paste electrode modified with oxovanadium (IV)-4-methyl salophen. J. Electroanal. Chem. 614, 157–165 (2008)CrossRef
Metadata
Title
Synthesis of phosphate-modified zeolite as a modifier in carbon paste electrode for nitrite electrochemical detection
Authors
Adamu Idris
Tawfik Saleh
Oki Muraza
Mohammed Sanhoob
Md. Abdul Aziz
Abdul-Rahman Al-Betar
Publication date
02-01-2019
Publisher
Springer US
Published in
Journal of Materials Science: Materials in Electronics / Issue 4/2019
Print ISSN: 0957-4522
Electronic ISSN: 1573-482X
DOI
https://doi.org/10.1007/s10854-018-00601-5

Other articles of this Issue 4/2019

Journal of Materials Science: Materials in Electronics 4/2019 Go to the issue

OriginalPaper

MOVPE growth conditions optimization for AlGaN/GaN/Si heterostructures with SiN and LT-AlN interlayers designed for HEMT applications

OriginalPaper

The role of Zn substitution in P2-type Na0.67Ni0.23Zn0.1Mn0.67O2 cathode for inhibiting the phase transition at high potential and dissolution of manganese at low potential

OriginalPaper

Enhanced electrical and fatigue properties of La-modified (100)-oriented PZT thin films with various Zr/Ti ratio

OriginalPaper

Green synthesis of capacitive carbon derived from Platanus catkins with high energy density

OriginalPaper

Facile large-scale preparation of high-performance copper electrode materials for BaTiO3 ceramic capacitors

OriginalPaper

Synthesis of Bi2WO6 photocatalyst modified by SDBS and photocatalytic performance under visible light