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Published in: Journal of Materials Engineering and Performance 10/2018

13-08-2018

The Application of Centrifugal Atomization Method for Preparation of Rapidly Solidified Nd-Fe-B Flakes Used for Production of Permanent Magnets

Authors: Mihael Brunčko, Žiga Erman, Peter Kirbiš, Ivan Anžel

Published in: Journal of Materials Engineering and Performance | Issue 10/2018

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Abstract

Nd-Fe-B-type permanent magnets are used in applications that require a high-energy product/volume ratio in order to reduce weight. Automotive industry, hard drives, or wind turbines are just examples of an application where their use can be found. Conventional casting techniques reveal the formation of a high quantity of α-Fe and large Nd-rich regions. On the other hand, new techniques, like strip casting, melt-spinning and centrifugal atomization, produce homogeneous and fine-scaled microstructures. This paper discusses the application of rapid solidification by means of the centrifugal atomization method for preparation of Nd-Fe-B flakes. The effect of alloy composition and various process parameters of centrifugal atomization on the microstructure of rapidly solidified Nd-Fe-B alloy were investigated. The microstructures and the phase composition were examined by metallographic techniques, namely optical and scanning electron microscopy. Additionally, the influence of the processing parameters on the microstructures of as-cast flakes and subsequent magnetic properties of the prepared magnets will be discussed.

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Literature
1.
go back to reference W. Kurz and D.J. Fisher, Fundaments of Solidification, Trans Tech Publications, Brookfield, 1989 W. Kurz and D.J. Fisher, Fundaments of Solidification, Trans Tech Publications, Brookfield, 1989
2.
go back to reference H. Jones, Rapid Solidification of Metals and Alloys, Monograph No. 8, The institution of metallurgists, London, 1982 H. Jones, Rapid Solidification of Metals and Alloys, Monograph No. 8, The institution of metallurgists, London, 1982
3.
4.
go back to reference E.I. Anderson, W. Tang, and R.W. Mccallum, Particulate Processing and Properties of High-Performance Permanent Magnets, Int. J. Powder Metal., 2004, 40(6), p 37–60 E.I. Anderson, W. Tang, and R.W. Mccallum, Particulate Processing and Properties of High-Performance Permanent Magnets, Int. J. Powder Metal., 2004, 40(6), p 37–60
5.
go back to reference J.M.D. Coey, Magnetism and magnetic materials, Cambridge University Press, Cambridge, 2010, p 614CrossRef J.M.D. Coey, Magnetism and magnetic materials, Cambridge University Press, Cambridge, 2010, p 614CrossRef
6.
go back to reference O. Gutfleisch, Rare Earth Magnets: Materials, V: Encyclopedia of Materials: Science and Technology, 2nd ed., Elsevier, Oxford, 2001, p 8022–8025 O. Gutfleisch, Rare Earth Magnets: Materials, V: Encyclopedia of Materials: Science and Technology, 2nd ed., Elsevier, Oxford, 2001, p 8022–8025
7.
go back to reference B.E. Davies, R.S. Mottram, and I.R. Harris, Recent Developments in the Sintering of NdFeB, Mater. Chem. Phys., 2001, 67(1–3), p 272–281CrossRef B.E. Davies, R.S. Mottram, and I.R. Harris, Recent Developments in the Sintering of NdFeB, Mater. Chem. Phys., 2001, 67(1–3), p 272–281CrossRef
8.
go back to reference P. Tenaud, H. Lemaire, and F. Vial, Recent Improvements in NdFeB Sintered Magnets, J. Magn. Magn. Mater., 1991, 101, p 328–332CrossRef P. Tenaud, H. Lemaire, and F. Vial, Recent Improvements in NdFeB Sintered Magnets, J. Magn. Magn. Mater., 1991, 101, p 328–332CrossRef
9.
go back to reference S. Guo, Q.Y. Zhou, R.J. Chen, D. Lee, and A.R. Yan, Microstructure and Magnetic Properties of Sintered Nd-Fe-B Magnets with High Hydrogen Content, J. Appl. Phys., 2011, 109, p 07A734CrossRef S. Guo, Q.Y. Zhou, R.J. Chen, D. Lee, and A.R. Yan, Microstructure and Magnetic Properties of Sintered Nd-Fe-B Magnets with High Hydrogen Content, J. Appl. Phys., 2011, 109, p 07A734CrossRef
10.
go back to reference G. Bai, R.W. Gao, Y. Sun, G.B. Han, and B. Wang, Study of High-Coercivity Sintered NdFeB Magnets, J. Magn. Magn. Mater., 2007, 308, p 20–23CrossRef G. Bai, R.W. Gao, Y. Sun, G.B. Han, and B. Wang, Study of High-Coercivity Sintered NdFeB Magnets, J. Magn. Magn. Mater., 2007, 308, p 20–23CrossRef
11.
go back to reference W. Rodewald, B. Wall, M. Katter, and K. Ustuner, Top NdFeB Magnets with Greater than 56 MGOe Energy Density and 9.8 kOe Coercivity, IEEE Trans. Magn., 2002, 38, p 2955–2957CrossRef W. Rodewald, B. Wall, M. Katter, and K. Ustuner, Top NdFeB Magnets with Greater than 56 MGOe Energy Density and 9.8 kOe Coercivity, IEEE Trans. Magn., 2002, 38, p 2955–2957CrossRef
12.
go back to reference R.S. Sheridan, A.J. Williams, I. Harris, and A. Walton, Improved HDDR Processing Route for Production of Anisotropic Powder from Sintered NdFeB Magnets, J. Magn. Magn. Mater., 2014, 350, p 114–118CrossRef R.S. Sheridan, A.J. Williams, I. Harris, and A. Walton, Improved HDDR Processing Route for Production of Anisotropic Powder from Sintered NdFeB Magnets, J. Magn. Magn. Mater., 2014, 350, p 114–118CrossRef
13.
go back to reference D. Brown, B.M. Ma, and Z. Chen, Developments in the Processing and Properties of Nd-Fe-N-Type Permanent Magnets, J. Magn. Magn. Mater., 2002, 248, p 432–440CrossRef D. Brown, B.M. Ma, and Z. Chen, Developments in the Processing and Properties of Nd-Fe-N-Type Permanent Magnets, J. Magn. Magn. Mater., 2002, 248, p 432–440CrossRef
14.
go back to reference S. Ozawa, T. Saito, and T. Motegi, Effects of Cooling Rate on Microstructures and Magnetic Properties of Nd-Fe-B Alloys, J. Alloy. Compd., 2004, 363(1–2), p 268–275CrossRef S. Ozawa, T. Saito, and T. Motegi, Effects of Cooling Rate on Microstructures and Magnetic Properties of Nd-Fe-B Alloys, J. Alloy. Compd., 2004, 363(1–2), p 268–275CrossRef
15.
go back to reference J. Bernardi, J. Fidler, M. Sagawa, and Y. Hirose, Microstructural Analysis of Strip-Cast Nd-Fe-B Alloys for High (BH)max Magnets, J. Appl. Phys., 1998, 83, p 6396CrossRef J. Bernardi, J. Fidler, M. Sagawa, and Y. Hirose, Microstructural Analysis of Strip-Cast Nd-Fe-B Alloys for High (BH)max Magnets, J. Appl. Phys., 1998, 83, p 6396CrossRef
16.
go back to reference L.Q. Yu, M. Yan, J.M. Wu, W. Luo, X.G. Cui, and H.G. Ying, On the Cooling Rate of Strip Cast Ingots for Sintered NdFeB Magnets, Phys. B, 2007, 393, p 1–5CrossRef L.Q. Yu, M. Yan, J.M. Wu, W. Luo, X.G. Cui, and H.G. Ying, On the Cooling Rate of Strip Cast Ingots for Sintered NdFeB Magnets, Phys. B, 2007, 393, p 1–5CrossRef
17.
go back to reference Z. Tian, S. Li, K. Peng, B. Gu, and Y. Du, The Microstructure and Magnetic Properties of NdFeB Magnets Directly Solidified at a Low Cooling Rate, Mater. Sci. Eng. A, 2004, 380, p 143–146CrossRef Z. Tian, S. Li, K. Peng, B. Gu, and Y. Du, The Microstructure and Magnetic Properties of NdFeB Magnets Directly Solidified at a Low Cooling Rate, Mater. Sci. Eng. A, 2004, 380, p 143–146CrossRef
18.
go back to reference G. Binglin, L. Bo, W. Dongling, Y. Xiaojun, and H. Jifan, Influence of Cooling Rate on Microstructure of NdFeB Strip Casting Flakes, Mater. Sci. Forum, 2005, 475–479, p 2169–2172 G. Binglin, L. Bo, W. Dongling, Y. Xiaojun, and H. Jifan, Influence of Cooling Rate on Microstructure of NdFeB Strip Casting Flakes, Mater. Sci. Forum, 2005, 475–479, p 2169–2172
19.
go back to reference X. Jing, Y. Shihong, Y. Dunbo, L. Zongan, L. Shipeng, and L. Hongwei, Influence of Solidification Rate on Microstructures of Cast Strips and Corresponding Sintered NdFeB Magnets, J. Rare Earths, 2006, 24(1), p 306–309CrossRef X. Jing, Y. Shihong, Y. Dunbo, L. Zongan, L. Shipeng, and L. Hongwei, Influence of Solidification Rate on Microstructures of Cast Strips and Corresponding Sintered NdFeB Magnets, J. Rare Earths, 2006, 24(1), p 306–309CrossRef
20.
go back to reference D. Goll, S. Schweizer, C. Wegierski, and G. Schneider, Towards a Better Understanding of Intergranular Phases in Fe-Nd-B Sintered Magnets, Phys. Status Solidi RRL, 2012, 6(9–10), p 388–390CrossRef D. Goll, S. Schweizer, C. Wegierski, and G. Schneider, Towards a Better Understanding of Intergranular Phases in Fe-Nd-B Sintered Magnets, Phys. Status Solidi RRL, 2012, 6(9–10), p 388–390CrossRef
Metadata
Title
The Application of Centrifugal Atomization Method for Preparation of Rapidly Solidified Nd-Fe-B Flakes Used for Production of Permanent Magnets
Authors
Mihael Brunčko
Žiga Erman
Peter Kirbiš
Ivan Anžel
Publication date
13-08-2018
Publisher
Springer US
Published in
Journal of Materials Engineering and Performance / Issue 10/2018
Print ISSN: 1059-9495
Electronic ISSN: 1544-1024
DOI
https://doi.org/10.1007/s11665-018-3564-7

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