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Journal of Materials Engineering and Performance

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01-08-2014

Effects of Grit Blasting and Annealing on the High-Temperature Oxidation Behavior of Austenitic and Ferritic Fe-Cr Alloys

Authors: M. Proy, M. V. Utrilla, E. Otero, B. Bouchaud, F. Pedraza

Published in: Journal of Materials Engineering and Performance | Issue 8/2014

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Abstract

Grit blasting (corundum) of an austenitic AISI 304 stainless steel (18Cr-8Ni) and of a low-alloy SA213 T22 ferritic steel (2.25Cr-1Mo) followed by annealing in argon resulted in enhanced outward diffusion of Cr, Mn, and Fe. Whereas 3 bar of blasting pressure allowed to grow more Cr₂O₃ and Mn_xCr_3−xO₄ spinel-rich scales, higher pressures gave rise to Fe₂O₃-enriched layers and were therefore disregarded. The effect of annealing pre-oxidation treatment on the isothermal oxidation resistance was subsequently evaluated for 48 h for both steels and the results were compared with their polished counterparts. The change of oxidation kinetics of the pre-oxidized 18Cr-8Ni samples at 850 °C was ascribed to the growth of a duplex Cr₂O₃/Mn_xCr_3−xO₄ scale that remained adherent to the substrate. Such a positive effect was less marked when considering the oxidation kinetics of the 2.25Cr-1Mo steel but a more compact and thinner Fe_xCr_3−xO₄ subscale grew at 650 °C compared to that of the polished samples. It appeared that the beneficial effect is very sensitive to the experimental blasting conditions. The input of Raman micro-spectroscopy was shown to be of ground importance in the precise identification of multiple oxide phases grown under the different conditions investigated in this study.

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Title: Effects of Grit Blasting and Annealing on the High-Temperature Oxidation Behavior of Austenitic and Ferritic Fe-Cr Alloys
Authors: M. Proy
M. V. Utrilla
E. Otero
B. Bouchaud
F. Pedraza
Publication date: 01-08-2014
Publisher: Springer US
Published in: Journal of Materials Engineering and Performance / Issue 8/2014
Print ISSN: 1059-9495
Electronic ISSN: 1544-1024
DOI: https://doi.org/10.1007/s11665-014-1073-x

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