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Journal of Materials Engineering and Performance

Erschienen in:

01.08.2014

Effects of Grit Blasting and Annealing on the High-Temperature Oxidation Behavior of Austenitic and Ferritic Fe-Cr Alloys

verfasst von: M. Proy, M. V. Utrilla, E. Otero, B. Bouchaud, F. Pedraza

Erschienen in: Journal of Materials Engineering and Performance | Ausgabe 8/2014

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Abstract

Grit blasting (corundum) of an austenitic AISI 304 stainless steel (18Cr-8Ni) and of a low-alloy SA213 T22 ferritic steel (2.25Cr-1Mo) followed by annealing in argon resulted in enhanced outward diffusion of Cr, Mn, and Fe. Whereas 3 bar of blasting pressure allowed to grow more Cr₂O₃ and Mn_xCr_3−xO₄ spinel-rich scales, higher pressures gave rise to Fe₂O₃-enriched layers and were therefore disregarded. The effect of annealing pre-oxidation treatment on the isothermal oxidation resistance was subsequently evaluated for 48 h for both steels and the results were compared with their polished counterparts. The change of oxidation kinetics of the pre-oxidized 18Cr-8Ni samples at 850 °C was ascribed to the growth of a duplex Cr₂O₃/Mn_xCr_3−xO₄ scale that remained adherent to the substrate. Such a positive effect was less marked when considering the oxidation kinetics of the 2.25Cr-1Mo steel but a more compact and thinner Fe_xCr_3−xO₄ subscale grew at 650 °C compared to that of the polished samples. It appeared that the beneficial effect is very sensitive to the experimental blasting conditions. The input of Raman micro-spectroscopy was shown to be of ground importance in the precise identification of multiple oxide phases grown under the different conditions investigated in this study.

Vorheriger Artikel Microstructural Characterization of Thermomechanical and Heat-Affected Zones of an Inertia Friction Welded Astroloy

Nächster Artikel Material Parameters for Creep Rupture of Austenitic Stainless Steel Foils

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Titel: Effects of Grit Blasting and Annealing on the High-Temperature Oxidation Behavior of Austenitic and Ferritic Fe-Cr Alloys
verfasst von: M. Proy
M. V. Utrilla
E. Otero
B. Bouchaud
F. Pedraza
Publikationsdatum: 01.08.2014
Verlag: Springer US
Erschienen in: Journal of Materials Engineering and Performance / Ausgabe 8/2014
Print ISSN: 1059-9495
Elektronische ISSN: 1544-1024
DOI: https://doi.org/10.1007/s11665-014-1073-x

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