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Journal of Materials Science

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14-05-2018 | Mechanochemical Synthesis

Mechanochemical syntheses of LiFeGe₂O₆-based nanocomposite and novel nanoglassy LiFeTi₂O₆

Authors: Erika Tóthová, Ralf Witte, Michal Hegedüs, Mamoru Senna, Horst Hahn, Paul Heitjans, Vladimír Šepelák

Published in: Journal of Materials Science | Issue 19/2018

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Abstract

Two members of the pyroxene family, the germanate-type LiFeGe₂O₆ and the titanate-type LiFeTi₂O₆, are prepared for the first time via non-conventional one-step mechanosynthesis. The evolution of the as-prepared materials in the course of mechanosynthesis and their structural state on the long-range and local atomic scales are characterized by X-ray diffraction and ⁵⁷Fe Mössbauer spectroscopy, respectively. Both, the nanocrystalline nature of LiFeGe₂O₆ and the nanoglassy state of LiFeTi₂O₆ are revealed.

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Title: Mechanochemical syntheses of LiFeGe2O6-based nanocomposite and novel nanoglassy LiFeTi2O6
Authors: Erika Tóthová
Ralf Witte
Michal Hegedüs
Mamoru Senna
Horst Hahn
Paul Heitjans
Vladimír Šepelák
Publication date: 14-05-2018
Publisher: Springer US
Published in: Journal of Materials Science / Issue 19/2018
Print ISSN: 0022-2461
Electronic ISSN: 1573-4803
DOI: https://doi.org/10.1007/s10853-018-2405-2

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