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Journal of Electronic Materials
Published in: Journal of Electronic Materials 1/2023

27-10-2022 | Original Research Article

Novel Synthesis of a PANI/ZnO Nanohybrid for Enhanced NO2 Gas Sensing Performance at Low Temperatures

Authors: To Thi Nguyet, Lai Van Duy, Quan Thi Minh Nguyet, Chu Thi Xuan, Dang Thi Thanh Le, Chu Manh Hung, Nguyen Van Duy, Nguyen Duc Hoa

Published in: Journal of Electronic Materials | Issue 1/2023

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Abstract

Nanohybrids, which comprise organic and inorganic materials, have gained increasing interest in the application for enhanced sensing response to both reducing and oxidation gases. In this study, we prepared nanohybrids of polyaniline (PANI) and ZnO nanoplates through a hydrothermal route for high-performance nitrogen dioxide gas sensing at low temperatures. The structure, morphology, and surface composition of as-synthesized samples were, respectively, examined via x-ray diffraction, scanning electron microscopy, transmission electron microscopy, and Fourier transform infrared spectroscopy. The results indicated that the resistive sensor based on the PANI/ZnO hybrid showed the highest response toward NO2 at 150°C with a response value Rg/Ra = 601 to 5 ppm NO2. We also investigated the sensing properties of volatile organic compounds including methanol, ethanol, triethylamine, toluene, and isopropanol. Indeed, the heterojunction reflects the characteristics of the n-type ZnO semiconductor. Characterization and gas sensing measurements exhibited protonation and deprotonation of the PANI/ZnO heterojunction, which contributes to the nitrogen dioxide sensing mechanism. Overall, the obtained findings demonstrated that the PANI/ZnO nanoplates are promising materials for sensing applications in food analysis and environmental monitoring.

Graphical Abstract

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Metadata
Title
Novel Synthesis of a PANI/ZnO Nanohybrid for Enhanced NO2 Gas Sensing Performance at Low Temperatures
Authors
To Thi Nguyet
Lai Van Duy
Quan Thi Minh Nguyet
Chu Thi Xuan
Dang Thi Thanh Le
Chu Manh Hung
Nguyen Van Duy
Nguyen Duc Hoa
Publication date
27-10-2022
Publisher
Springer US
Published in
Journal of Electronic Materials / Issue 1/2023
Print ISSN: 0361-5235
Electronic ISSN: 1543-186X
DOI
https://doi.org/10.1007/s11664-022-09990-0

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