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2012 | OriginalPaper | Buchkapitel

Application of 1H NMR to the Hydration Monitoring of Lime-Pozzolan Mortars

verfasst von : Maria Tziotziou, Eleni Karakosta, Ioannis Karatasios, Michalis Fardis, Pagona Maravelaki-Kalaitzaki, Georgios Papavassiliou, Vassilis Kilikoglou

Erschienen in: Historic Mortars

Verlag: Springer Netherlands

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Abstract

The micro-structural evolution of a lime-pozzolan system, during hydration, was studied by 1H Nuclear Magnetic Resonance (NMR). The hydration process was monitored for a period of 1 year by 1H NMR spin-lattice relaxation measurements, performed in a portable magnet. The development of the hydration was also examined by scanning electron microscopy (SEM), X-ray diffraction (XRD), mercury intrusion porosimetry (MIP), infrared spectroscopy (FT-IR) and thermal analysis (DTA/TG) and compared with the NMR results. The results indicated that 1H NMR provides valuable information on the hydration process of lime-pozzolan mortars in a non-invasive way, as it was possible to monitor the development of the hydration phases through the resulted microstructure, in real-time.

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Metadaten
Titel
Application of 1H NMR to the Hydration Monitoring of Lime-Pozzolan Mortars
verfasst von
Maria Tziotziou
Eleni Karakosta
Ioannis Karatasios
Michalis Fardis
Pagona Maravelaki-Kalaitzaki
Georgios Papavassiliou
Vassilis Kilikoglou
Copyright-Jahr
2012
Verlag
Springer Netherlands
DOI
https://doi.org/10.1007/978-94-007-4635-0_34