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2020 | OriginalPaper | Buchkapitel

6. Characterization of Lead Halide Perovskites Using Synchrotron X-ray Techniques

verfasst von : Lijia Liu, Zhaohui Dong

Erschienen in: Perovskite Quantum Dots

Verlag: Springer Singapore

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Abstract

In this chapter, we are going to introduce several characterization methods that utilize synchrotron X-rays as the probing source for understanding electronic structure, crystal structure, and optical properties of lead halide perovskite materials. We will show how X-ray absorption fine structure (XAFS) can be used to understand the dissociation mechanism, to identify the presence of defect, and to analyze the influence of dopant introduction on structural modification. We will demonstrate that an X-ray excited optical luminescence (XEOL) in combination with XAFS analysis helps to understand the luminescence mechanism of doped perovskite. We will also present the use of synchrotron X-ray diffraction (XRD) to study the creation of new crystal phases induced by high pressure and the phase transformation of perovskite in situ. The working principle of each technique will be introduced, followed by examples from recently published research articles.

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Nächstes Kapitel Perovskite Quantum Dot Photodetectors

I. Chung, B. Lee, J. He, R.P. Chang, M.G. Kanatzidis, Nature 485, 486–489 (2012)

H.S. Jung, N.G. Park, Small 11, 10–25 (2015)

Q. Zhang, Y. Yin, ACS Central Sci. 4, 668–679 (2018)

L. Protesescu, S. Yakunin, M.I. Bodnarchuk, F. Krieg, R. Caputo, C.H. Hendon, R.X. Yang, A. Walsh, M.V. Kovalenko, Nano Lett. 15, 3692–3696 (2015)

A. Kojima, K. Teshima, Y. Shirai, T. Miyasaka, J. Am. Chem. Soc. 131, 6050–6051 (2009)

D. Shi, V. Adinolfi, R. Comin, M. Yuan, E. Alarousu, A. Buin, Y. Chen, S. Hoogland, A. Rothenberger, K. Katsiev, Y. Losovyj, X. Zhang, P.A. Dowben, O.F. Mohammed, E.H. Sargent, O.M. Bakr, Science 347, 519–522 (2015)

M.A. Green, A. Ho-Baillie, H.J. Snaith, Nat. Photonics 8, 506–514 (2014)

C. Bi, S. Wang, Q. Li, S.V. Kershaw, J. Tian, A.L. Rogach, J. Phys. Chem. Lett. 10, 943–952 (2019)

J.S. Yao, J. Ge, B.N. Han, K.H. Wang, H.B. Yao, H.L. Yu, J.H. Li, B.S. Zhu, J.Z. Song, C. Chen, Q. Zhang, H.B. Zeng, Y. Luo, S.H. Yu, J. Am. Chem. Soc. 140, 3626–3634 (2018)

10.

W. Liu, Q. Lin, H. Li, K. Wu, I. Robel, J.M. Pietryga, V.I. Klimov, J. Am. Chem. Soc. 138, 14954–14961 (2016)

11.

P.J.S. Rana, T. Swetha, H. Mandal, A. Saeki, P.R. Bangal, S.P. Singh, J. Phys. Chem. C 123, 17026–17034 (2019)

12.

D. Bryant, N. Aristidou, S. Pont, I. Sanchez-Molina, T. Chotchunangatchaval, S. Wheeler, J.R. Durrant, S.A. Haque, Energy Environ. Sci. 9, 1655–1660 (2016)

13.

B. Conings, J. Drijkoningen, N. Gauquelin, A. Babayigit, J. D’Haen, L. D’Olieslaeger, A. Ethirajan, J. Verbeeck, J. Manca, E. Mosconi, F. De Angelis, H.G. Boyen, Adv. Energy Mater. 5, 1500477 (2015)

14.

B. Salhi, Y.S. Wudil, M.K. Hossain, A. Al-Ahmed, F.A. Al-Sulaiman, Renew. Sustain. Energy Rev. 90, 210–222 (2018)

15.

S. Huang, Z. Li, B. Wang, N. Zhu, C. Zhang, L. Kong, Q. Zhang, A. Shan, L. Li, A.C.S. Appl, Mater. Interfaces 9, 7249–7258 (2017)

16.

J. Pan, S.P. Sarmah, B. Murali, I. Dursun, W. Peng, M.R. Parida, J. Liu, L. Sinatra, N. Alyami, C. Zhao, E. Alarousu, T.K. Ng, B.S. Ooi, O.M. Bakr, O.F. Mohammed, J. Phys. Chem. Lett. 6, 5027–5033 (2015)

17.

Z. Shi, J. Guo, Y. Chen, Q. Li, Y. Pan, H. Zhang, Y. Xia, W. Huang, Adv. Mater. 29, 1605005 (2017)

18.

L. Liang, P. Gao, Adv. Sci. 5, 1700331 (2018)

19.

W. Xu, L. Liu, L. Yang, P. Shen, B. Sun, J.A. McLeod, Nano Lett. 16, 4720–4725 (2016)

20.

M.-C. Jung, Y.M. Lee, H.-K. Lee, J. Park, S.R. Raga, L.K. Ono, S. Wang, M.R. Leyden, B.D. Yu, S. Hong, Y. Qi, Appl. Phys. Lett. 108, 073901 (2016)

21.

J.A. McLeod, Z. Wu, B. Sun, L. Liu, Nanoscale 8, 6361–6368 (2016)

22.

J. Ma, Q. Yao, J.A. McLeod, L.Y. Chang, C.W. Pao, J. Chen, T.K. Sham, L. Liu, Nanoscale 11, 6182–6191 (2019)

23.

Y. Wang, X. Lu, W. Yang, T. Wen, L. Yang, X. Ren, L. Wang, Z. Lin, Y. Zhao, J. Am. Chem. Soc. 137, 11144–11149 (2015)

24.

M. Liu, J. Zhao, Z. Luo, Z. Sun, N. Pan, H. Ding, X. Wang, Chem. Mater. 30, 5846–5852 (2018)

25.

B. Philippe, B.-W. Park, R. Lindblad, J. Oscarsson, S. Ahmadi, E.M.J. Johansson, H. Rensmo, Chem. Mater. 27, 1720–1731 (2015)

26.

V.K. Ravi, P.K. Santra, N. Joshi, J. Chugh, S.K. Singh, H. Rensmo, P. Ghosh, A. Nag, J. Phys. Chem. Lett. 8, 4988–4994 (2017)

27.

W. Huang, F. Huang, E. Gann, Y.-B. Cheng, C. McNeill, Adv. Funct. Mater. 25, 5529–5536 (2015)

28.

C.Y. Chang, Y.C. Huang, C.S. Tsao, W.F. Su, A.C.S. Appl, Mater. Interfaces 8, 26712–26721 (2016)

29.

G. Bunker, Introduction to XAFS: A Practical Guide to X-Ray Absorption Fine Structure Spectroscopy (Cambridge University Press, New York, 2010)

30.

P. Willmott, Spectroscopic Techniques, An Introduction to Synchrotron Radiation: Techniques And Applications (John Wiley & Sons Ltd, UK, 2019)

31.

An online version of the booklet is available at: https://xdb.lbl.gov/

32.

E.A. Stern, D.E. Sayers, F.W. Lytle, Phys. Rev. B 11, 4836–4846 (1975)

33.

J.J. Rehr, R.C. Albers, Rev. Mod. Phys. 72 (2000)

34.

Z. Sun, Q. Liu, T. Yao, W. Yan, S. Wei, Sci. Chin. Mater. 58, 313–341 (2015)

35.

J.A. McLeod, Z. Wu, P. Shen, B. Sun, L. Liu, J. Phys. Chem. Lett. 5, 2863–2867 (2014)

36.

Y. Wang, Z. Xia, L. Liu, W. Xu, Z. Yuan, Y. Zhang, H. Sirringhaus, Y. Lifshitz, S.T. Lee, Q. Bao, B. Sun, Adv. Mater. 29, 1606370 (2017)

37.

P. Shen, K. Nie, X. Sun, L. Liu, J.A. McLeod, Phys. Stat. Sol. RRL 10, 677–681 (2016)

38.

L. Etgar, P. Gao, Z. Xue, Q. Peng, A.K. Chandiran, B. Liu, M.K. Nazeeruddin, M. Gratzel, J. Am. Chem. Soc. 134, 17396–17399 (2012)

39.

S.D. Stranks, G.E. Eperon, G. Grancini, C. Menelaou, M.J. Alcocer, T. Leijtens, L.M. Herz, A. Petrozza, H.J. Snaith, Science 342, 341–344 (2013)

40.

J.M. Frost, K.T. Butler, F. Brivio, C.H. Hendon, M. van Schilfgaarde, A. Walsh, Nano Lett. 14, 2584–2590 (2014)

41.

G. Niu, X. Guo, L. Wang, J. Mater. Chem. A 3, 8970–8980 (2015)

42.

Q. Wang, R. Wang, P. Shen, C. Li, Y. Li, L. Liu, S. Duhm, J. Tang, Adv. Mater. Interfaces (2015)

43.

S.R. Raga, M.-C. Jung, M.V. Lee, M.R. Leyden, Y. Kato, Y. Qi, Chem. Mater. 27, 1597–1603 (2015)

44.

T.-W. Ng, C.-Y. Chan, M.-F. Lo, Z.Q. Guan, C.-S. Lee, J. Mater. Chem. A (2015)

45.

R. Wang, C. Wu, Y. Hu, J. Li, P. Shen, Q. Wang, L. Liao, L. Liu, S. Duhm, A.C.S. Appl, Mater. Interfaces 9, 7859–7865 (2017)

46.

N.K. Kim, Y.H. Min, S. Noh, E. Cho, G. Jeong, M. Joo, S.W. Ahn, J.S. Lee, S. Kim, K. Ihm, H. Ahn, Y. Kang, H.S. Lee, D. Kim, Sci. Rep. 7, 4645 (2017)

47.

G. Grancini, A.R. Srimath Kandada, J.M. Frost, A.J. Barker, M. De Bastiani, M. Gandini, S. Marras, G. Lanzani, A. Walsh, A. Petrozza, Nat. Photonics, 9, 695–701 (2015)

48.

E.J. Juarez-Perez, Z. Hawash, S.R. Raga, L.K. Ono, Y. Qi, Energy Environ. Sci. 9, 3406–3410 (2016)

49.

G. Abdelmageed, L. Jewell, K. Hellier, L. Seymour, b. Luo, F. Bridges, J.Z. Zhang, S. Carter, Appl. Phys. Lett. 109, 233905 (2016)

50.

G. Abdelmageed, C. Mackeen, K. Hellier, L. Jewell, L. Seymour, M. Tingwald, F. Bridges, J.Z. Zhang, S. Carter, Sol. Energy Mater. Sol. Cells 174, 566–571 (2018)

51.

J. Kim, S.-H. Lee, J.H. Lee, K.-H. Hong, J. Phys. Chem. Lett. 5, 1312–1317 (2014)

52.

W.-J. Yin, T. Shi, Y. Yan, Appl. Phys. Lett. 104, 063903 (2014)

53.

C.-C. Chueh, C.-Y. Liao, F. Zuo, S.T. Williams, P.-W. Liang, A.K.Y. Jen, J. Mater. Chem. A 3, 9058–9062 (2015)

54.

Q. Chen, H. Zhou, Y. Fang, A.Z. Stieg, T.B. Song, H.H. Wang, X. Xu, Y. Liu, S. Lu, J. You, P. Sun, J. McKay, M.S. Goorsky, Y. Yang, Nature Commun. 6, 7269 (2015)

55.

S. Das Adhikari, S.K. Dutta, A. Dutta, A.K. Guria, N. Pradhan, Angew. Chem. 56, 8746–8750 (2017)

56.

A. Ishii, T. Miyasaka, Adv. Sci. 7, 1903142 (2020)

57.

H. Shao, X. Bai, H. Cui, G. Pan, P. Jing, S. Qu, J. Zhu, Y. Zhai, B. Dong, H. Song, Nanoscale 10, 1023–1029 (2018)

58.

Z.J. Yong, S.Q. Guo, J.P. Ma, J.Y. Zhang, Z.Y. Li, Y.M. Chen, B.B. Zhang, Y. Zhou, J. Shu, J.L. Gu, L.R. Zheng, O.M. Bakr, H.T. Sun, J. Am. Chem. Soc. 140, 9942–9951 (2018)

59.

G.H. Ahmed, J.K. El-Demellawi, J. Yin, J. Pan, D.B. Velusamy, M.N. Hedhili, E. Alarousu, O.M. Bakr, H.N. Alshareef, O.F. Mohammed, ACS Energy Lett. 3, 2301–2307 (2018)

60.

J.-P. Ma, Y.-M. Chen, L.-M. Zhang, S.-Q. Guo, J.-D. Liu, H. Li, B.-J. Ye, Z.-Y. Li, Y. Zhou, B.-B. Zhang, O.M. Bakr, J.-Y. Zhang, H.-T. Sun, J. Mater. Chem. C 7, 3037–3048 (2019)

61.

T.K. Sham, D.T. Jiang, I. Coulthard, J.W. Lorimer, X.H. Feng, K.H. Tan, S.P. Frigo, R.A. Rosenberg, D.C. Houghton, B. Bryskiewicz, Nature, 363, 331–334 (1993)

62.

L. Armelao, F. Heigl, A. Jurgensen, R.I.R. Blyth, T. Regier, X.T. Zhou, T.K. Sham, J. Phys. Chem. C 111, 10194–10200 (2007)

63.

Y. Hu, A. Mcaclennan, T.K. Sham, J. Luminescence 166, 143–147 (2015)

64.

L. Liu, T.K. Sham, in Titanium Dioxide: Material for a Sustainable Environment, ed. by D. Yang, Luminescence from TiO2 Nanotubes And Related Nanostructures Investigated using Synchrotron X-Ray Absorption Near-Edge Structure and X-ray Excited Optical Luminescence (IntechOpen, 2017)

65.

L. Liu, J. Li, T.-K. Sham, Can. J. Chem. 93, 106–112 (2015)

66.

A.K. Guria, S.K. Dutta, S.D. Adhikari, N. Pradhan, ACS Energy Lett. 2, 1014–1021 (2017)

67.

A.P. Hammersley, S.O. Svensson, M. Hanfland, A.N. Fitch, D. Hausermann, High Pressure Research 14, 235–248 (1996)

68.

L.B. McCusker, R.B. von Dreele, D.E. Cox, D. Louer, P. Scardi, J. Appl. Cryst. 32, 36–50 (1999)

69.

A.C. Larson, R.B. Von Dreele, Los Alamos National Laboratory Report, Los Alamos National Laboratory (2000)

70.

B.H. Toby, J. Appl. Cryst. 34, 210–213 (2001)

71.

J. Yang, B.D. Siempelkamp, D. Liu, T.L. Kelly, ACS Nano 9, 1955–1963 (2015)

72.

J. Zhao, B. Cai, Z. Luo, Y. Dong, Y. Zhang, H. Xu, B. Hong, Y. Yang, L. Li, W. Zhang, C. Gao, Sci. Rep. 6, 21976 (2016)

73.

L. Zhang, Q. Zeng, K. Wang, J. Phys. Chem. Lett. 8, 3752–3758 (2017)

74.

P. Wang, J. Guan, D.T.K. Galeschuk, Y. Yao, C.F. He, S. Jiang, S. Zhang, Y. Liu, M. Jin, C. Jin, Y. Song, J. Phys. Chem. Lett. 8, 2119–2125 (2017)

75.

M. Szafranski, A. Katrusiak, J. Phys. Chem. Lett. 7, 3458–3466 (2016)

76.

P. Postorino, L. Malavasi, J. Phys. Chem. Lett. 8, 2613–2622 (2017)

77.

G. Liu, L. Kong, J. Gong, W. Yang, H.-K. Mao, Q. Hu, Z. Liu, R.D. Schaller, D. Zhang, T. Xu, Adv. Funct. Mater. 27, 1604208 (2017)

78.

A. Jaffe, Y. Lin, W.L. Mao, H.I. Karunadasa, J. Am. Chem. Soc. 139, 4330–4333 (2017)

79.

L. Wang, K. Wang, B. Zou, J. Phys. Chem. Lett. 7, 2556–2562 (2016)

80.

L. Wang, K. Wang, G. Xiao, Q. Zeng, B. Zou, J. Phys. Chem. Lett. 7, 5273–5279 (2016)

81.

M. Szafranski, A. Katrusiak, J. Phys. Chem. Lett. 8, 2496–2506 (2017)

82.

X. Lu, Y. Wang, C.C. Stoumpos, Q. Hu, X. Guo, H. Chen, L. Yang, J.S. Smith, W. Yang, Y. Zhao, H. Xu, M.G. Kanatzidis, Q. Jia, Adv. Mater. 28, 8663–8668 (2016)

83.

S. Jiang, Y. Fang, R. Li, H. Xiao, J. Crowley, C. Wang, T.J. White, W.A. Goddard 3rd., Z. Wang, T. Baikie, J. Fang, Angew. Chem. 55, 6540–6544 (2016)

84.

A. Jaffe, Y. Lin, C.M. Beavers, J. Voss, W.L. Mao, H.I. Karunadasa, ACS Central Sci. 2, 201–209 (2016)

85.

A. Jaffe, Y. Lin, W.L. Mao, H.I. Karunadasa, J. Am. Chem. Soc. 137, 1673–1678 (2015)

86.

Y. Lee, D. Mitzi, P. Barnes, T. Vogt. Phys. Rev. B, 68 (2003)

87.

K. Gesi, Ferroelectrics 203, 249–268 (1997)

88.

K. Matsuishi, T. Ishihara, S. Onari, Y.H. Chang, C.H. Park, Phys. Stat. Sol. (b) 241, 3328–3333 (2004)

89.

I.P. Swainson, M.G. Tucker, D.J. Wilson, B. Winkler, V. Milman, Chem. Mater. 19, 2401–2405 (2007)

90.

A.D. Chijioke, W.J. Nellis, A. Soldatov, I.F. Silvera, J. Appl. Phys. 98, 114905 (2005)

91.

A.R. Milosavljevic, D.K. Bozanic, S. Sadhu, N. Vukmirovic, R. Dojcilovic, P. Sapkota, W. Huang, J. Bozek, C. Nicolas, L. Nahon, S. Ptasinska, J. Phys. Chem. Lett. 9, 3604–3611 (2018)

92.

L. Oesinghaus, J. Schlipf, N. Giesbrecht, L. Song, Y. Hu, T. Bein, P. Docampo, P. Müller-Buschbaum, Adv. Mater. Interfaces 3, 1600403 (2016)

93.

M. Kodur, R.E. Kumar, Y. Luo, D.N. Cakan, X. Li, M. Stuckelberger, D.P. Fenning. Adv. Energy Mater. 1903170 (2020)

Titel: Characterization of Lead Halide Perovskites Using Synchrotron X-ray Techniques
verfasst von: Lijia Liu
Zhaohui Dong
Verlag: Springer Singapore
Buch: Perovskite Quantum Dots
Print ISBN: 978-981-15-6636-3

Electronic ISBN: 978-981-15-6637-0

Copyright-Jahr: 2020
DOI: https://doi.org/10.1007/978-981-15-6637-0_6