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Journal of Polymer Research
Erschienen in: Journal of Polymer Research 5/2021

01.05.2021 | ORIGINAL PAPER

Controllable synthesis of ZnFe2O4 sub-microparticles by poly (diallyldimethylammonium chloride)-assisted solvothermal method

verfasst von: Manijeh Shaterian, Alireza Rezvani, Ahmad Reza Abbasian

Erschienen in: Journal of Polymer Research | Ausgabe 5/2021

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Abstract

Magnetic zinc ferrite (ZnFe2O4) sub-microparticles were synthesized using a facile poly (diallyldimethylammonium chloride) (PDDA)-assisted solvothermal method. X-ray diffraction (XRD) results confirm the formation of spinel structure of ZnFe2O4 with crystallite size from 11 to 41 nm. Scanning electronic microscope (SEM) images show that the samples exhibit a spherical-like morphology self-assembled by primary nanoparticles with sizes about 95–345 nm that are changed with reaction conditions. The zeta potential is increased by the addition PDDA, which indicates the colloidal stability of the sub-microparticles. Dynamic light scattering measurement shows that the presence of PDDA significantly decreased the average hydrodynamic size of the sub-microparticles from 349 nm without PDDA to 117.6 nm with 6 mL of PDDA. Vibrating sample magnetometer (VSM) measurements reveal that the samples synthesized with 0 and 2 mL of PDDA exhibit superparamagnetic properties while those synthesized with 4, 6 and 8 mL of PDDA show a ferromagnetic behavior. The reaction time and different amounts of PDDA influence the crystallinity, size, magnetic property and surface area of the ZnFe2O4 sub-microparticles.
Vorheriger Artikel Functionalization of polyhydromethylsiloxane with nitrogen-containing organic compounds
Nächster Artikel Enhanced mechanical and adhesive properties of PDMS based on novel PDMS-epoxy IPN structure

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Metadaten
Titel
Controllable synthesis of ZnFe2O4 sub-microparticles by poly (diallyldimethylammonium chloride)-assisted solvothermal method
verfasst von
Manijeh Shaterian
Alireza Rezvani
Ahmad Reza Abbasian
Publikationsdatum
01.05.2021
Verlag
Springer Netherlands
Erschienen in
Journal of Polymer Research / Ausgabe 5/2021
Print ISSN: 1022-9760
Elektronische ISSN: 1572-8935
DOI
https://doi.org/10.1007/s10965-021-02416-1

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