Skip to main content
Erschienen in: Applied Composite Materials 5/2018

11.11.2017

Curing of Thick Thermoset Composite Laminates: Multiphysics Modeling and Experiments

verfasst von: S. Anandan, G. S. Dhaliwal, Z. Huo, K. Chandrashekhara, N. Apetre, N. Iyyer

Erschienen in: Applied Composite Materials | Ausgabe 5/2018

Einloggen

Aktivieren Sie unsere intelligente Suche, um passende Fachinhalte oder Patente zu finden.

search-config
loading …

Abstract

Fiber reinforced polymer composites are used in high-performance aerospace applications as they are resistant to fatigue, corrosion free and possess high specific strength. The mechanical properties of these composite components depend on the degree of cure and residual stresses developed during the curing process. While these parameters are difficult to determine experimentally in large and complex parts, they can be simulated using numerical models in a cost-effective manner. These simulations can be used to develop cure cycles and change processing parameters to obtain high-quality parts. In the current work, a numerical model was built in Comsol MultiPhysics to simulate the cure behavior of a carbon/epoxy prepreg system (IM7/Cycom 5320–1). A thermal spike was observed in thick laminates when the recommended cure cycle was used. The cure cycle was modified to reduce the thermal spike and maintain the degree of cure at the laminate center. A parametric study was performed to evaluate the effect of air flow in the oven, post cure cycles and cure temperatures on the thermal spike and the resultant degree of cure in the laminate.

Sie haben noch keine Lizenz? Dann Informieren Sie sich jetzt über unsere Produkte:

Springer Professional "Wirtschaft+Technik"

Online-Abonnement

Mit Springer Professional "Wirtschaft+Technik" erhalten Sie Zugriff auf:

  • über 102.000 Bücher
  • über 537 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Finance + Banking
  • Management + Führung
  • Marketing + Vertrieb
  • Maschinenbau + Werkstoffe
  • Versicherung + Risiko

Jetzt Wissensvorsprung sichern!

Springer Professional "Technik"

Online-Abonnement

Mit Springer Professional "Technik" erhalten Sie Zugriff auf:

  • über 67.000 Bücher
  • über 390 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Maschinenbau + Werkstoffe




 

Jetzt Wissensvorsprung sichern!

Literatur
1.
Zurück zum Zitat Khoun, L., Centea, T., Humert, P.: Characterization methodology of thermoset resins for the processing of composite materials - case study: CYCOM 890RTM epoxy resin. J. Compos. Mater. 44(11), 1397–1415 (2010)CrossRef Khoun, L., Centea, T., Humert, P.: Characterization methodology of thermoset resins for the processing of composite materials - case study: CYCOM 890RTM epoxy resin. J. Compos. Mater. 44(11), 1397–1415 (2010)CrossRef
2.
Zurück zum Zitat Balvers, J., Bersee, H., Beukers, A., Jansen, K.: Determination of cure depenent properties for curing simulation of thick-walled composites. Proceedings of 49th AIAA/ASME/ASCE/AHS/ASC Structures, pp. 1–12. Schaumburg, IL, 7–10 April 2008 Balvers, J., Bersee, H., Beukers, A., Jansen, K.: Determination of cure depenent properties for curing simulation of thick-walled composites. Proceedings of 49th AIAA/ASME/ASCE/AHS/ASC Structures, pp. 1–12. Schaumburg, IL, 7–10 April 2008
3.
Zurück zum Zitat Karkanas, P., Partridge, I., Attwood, D.: Modeling the cure of a commercial epoxy system for applications in resin transfer molding. Polym. Int. 41, 183–191 (1996)CrossRef Karkanas, P., Partridge, I., Attwood, D.: Modeling the cure of a commercial epoxy system for applications in resin transfer molding. Polym. Int. 41, 183–191 (1996)CrossRef
4.
Zurück zum Zitat Kratz, J., Hisao, K., Fernlund, G., Hubert, P.: Thermal models for MTM45-1 and Cycom 5320 out-of-autoclave prepreg resins. J. Compos. Mater. 47(3), 341–352 (2013)CrossRef Kratz, J., Hisao, K., Fernlund, G., Hubert, P.: Thermal models for MTM45-1 and Cycom 5320 out-of-autoclave prepreg resins. J. Compos. Mater. 47(3), 341–352 (2013)CrossRef
5.
Zurück zum Zitat Kim, D., Centea, T., Nutt, S.: Out-time effects on cure kinetics and viscosity for an out-of-autoclave (OOA) prepreg: modeling and monitoring. Compos. Sci. Technol. 100, 63–69 (2014)CrossRef Kim, D., Centea, T., Nutt, S.: Out-time effects on cure kinetics and viscosity for an out-of-autoclave (OOA) prepreg: modeling and monitoring. Compos. Sci. Technol. 100, 63–69 (2014)CrossRef
6.
Zurück zum Zitat Loos, A., Springer, G.: Curing of epoxy matrix composites. J. Compos. Mater. 17(2), 135–139 (1983)CrossRef Loos, A., Springer, G.: Curing of epoxy matrix composites. J. Compos. Mater. 17(2), 135–139 (1983)CrossRef
7.
Zurück zum Zitat Ciriscioli, P., Wang, Q., Springer, G.: Autoclave curing – comparison of model and test results. J. Compos. Mater. 26, 90–102 (1992)CrossRef Ciriscioli, P., Wang, Q., Springer, G.: Autoclave curing – comparison of model and test results. J. Compos. Mater. 26, 90–102 (1992)CrossRef
8.
Zurück zum Zitat Twardowski, T., Lin, S., Geil, P.: Curing in thick composite laminates: experiment and simulation. J. Compos. Mater. 27(3), 216–250 (1993)CrossRef Twardowski, T., Lin, S., Geil, P.: Curing in thick composite laminates: experiment and simulation. J. Compos. Mater. 27(3), 216–250 (1993)CrossRef
9.
Zurück zum Zitat Kim, J., Lee, D.: Development of an autoclave cure cycle with cooling and reheating steps for thick thermoset composite laminates. J. Compos. Mater. 31(22), 2264–2281 (1997)CrossRef Kim, J., Lee, D.: Development of an autoclave cure cycle with cooling and reheating steps for thick thermoset composite laminates. J. Compos. Mater. 31(22), 2264–2281 (1997)CrossRef
10.
Zurück zum Zitat Kim, C., Teng, H., Tucker, C., White, S.: The continuous curing process for thermoset polymer composites. part 1: modeling and demonstration. J. Compos. Mater. 29, 1222–1253 (1995)CrossRef Kim, C., Teng, H., Tucker, C., White, S.: The continuous curing process for thermoset polymer composites. part 1: modeling and demonstration. J. Compos. Mater. 29, 1222–1253 (1995)CrossRef
11.
Zurück zum Zitat Blest, D., Duffy, B., McKee, S., Zulkifle, A.: Curing simulation of thermoset composites. Compos. A: Appl. Sci. Manuf. 30(11), 1289–1309 (1999)CrossRef Blest, D., Duffy, B., McKee, S., Zulkifle, A.: Curing simulation of thermoset composites. Compos. A: Appl. Sci. Manuf. 30(11), 1289–1309 (1999)CrossRef
12.
Zurück zum Zitat Bogetti, T., Gillespie, J.J.: Two-dimensional cure simulation of thick thermosetting composites. J. Compos. Mater. 25(3), 239–273 (1991)CrossRef Bogetti, T., Gillespie, J.J.: Two-dimensional cure simulation of thick thermosetting composites. J. Compos. Mater. 25(3), 239–273 (1991)CrossRef
13.
Zurück zum Zitat Oh, J.H., Lee, D.G.: Cure cycle for thick glass/epoxy composite laminates. J. Compos. Mater. 36(1), 19–45 (2002)CrossRef Oh, J.H., Lee, D.G.: Cure cycle for thick glass/epoxy composite laminates. J. Compos. Mater. 36(1), 19–45 (2002)CrossRef
14.
Zurück zum Zitat Joshi, S., Liu, X., Lam, Y.: A numerical approach to the modeling of polymer curing in fibre-reinforced composites. Compos. Sci. Technol. 59(7), 1003–1013 (1999)CrossRef Joshi, S., Liu, X., Lam, Y.: A numerical approach to the modeling of polymer curing in fibre-reinforced composites. Compos. Sci. Technol. 59(7), 1003–1013 (1999)CrossRef
15.
Zurück zum Zitat Park, H., Lee, S.: Cure simulation of thick composite structures using the finite element method. J. Compos. Mater. 35(3), 188–201 (2001)CrossRef Park, H., Lee, S.: Cure simulation of thick composite structures using the finite element method. J. Compos. Mater. 35(3), 188–201 (2001)CrossRef
16.
Zurück zum Zitat Park, H., Goo, N., Min, K., Yoon, K.: Three-dimensional cure simulation of composite structures by the finite element method. Compos. Struct. 62(1), 51–57 (2003)CrossRef Park, H., Goo, N., Min, K., Yoon, K.: Three-dimensional cure simulation of composite structures by the finite element method. Compos. Struct. 62(1), 51–57 (2003)CrossRef
17.
Zurück zum Zitat Guo, Z., Du, S., Zhang, B.: Temperature field of thick thermoset composite laminates during cure process. Compos. Sci. Technol. 65, 517–523 (2005)CrossRef Guo, Z., Du, S., Zhang, B.: Temperature field of thick thermoset composite laminates during cure process. Compos. Sci. Technol. 65, 517–523 (2005)CrossRef
18.
Zurück zum Zitat Belov, D., Makarenko, I., Dunaev, A., Babkin, A., Solopchenko, A., Yablokova, M., Kepman, A., Tretyakov, A., Ulyanov, A., Gromashev, A.: Curing processes simulation of complex shape carbon fiber reinforced composite components produced by vacuum infusion. Polym. Compos. 37(7), 2252–2259 (2016)CrossRef Belov, D., Makarenko, I., Dunaev, A., Babkin, A., Solopchenko, A., Yablokova, M., Kepman, A., Tretyakov, A., Ulyanov, A., Gromashev, A.: Curing processes simulation of complex shape carbon fiber reinforced composite components produced by vacuum infusion. Polym. Compos. 37(7), 2252–2259 (2016)CrossRef
19.
Zurück zum Zitat Shevtsov, S., Zhilyaev, I., Soloviev, A., Parinov, I., Dubrov, V.: Optimization of the composite cure process based on the thermo-kinetic model. Adv. Mater. Res. 185-192, 569 (2012) Shevtsov, S., Zhilyaev, I., Soloviev, A., Parinov, I., Dubrov, V.: Optimization of the composite cure process based on the thermo-kinetic model. Adv. Mater. Res. 185-192, 569 (2012)
20.
Zurück zum Zitat Bheemreddy, V., Huo, Z., Chandrashekhara, K., Brack, R.: Process modeling of cavity molded composite flex beams. Finite Elem. Anal. Des. 78, 8–15 (2014)CrossRef Bheemreddy, V., Huo, Z., Chandrashekhara, K., Brack, R.: Process modeling of cavity molded composite flex beams. Finite Elem. Anal. Des. 78, 8–15 (2014)CrossRef
21.
Zurück zum Zitat Chang, M., Chen, C., Young, W.: Optimal design of the cure cycle for consolidation of thick composite laminates. Polym. Compos. 17(5), 743–751 (1996)CrossRef Chang, M., Chen, C., Young, W.: Optimal design of the cure cycle for consolidation of thick composite laminates. Polym. Compos. 17(5), 743–751 (1996)CrossRef
22.
Zurück zum Zitat Michaud, D., Beris, A., Dhurjati, P.: Thick-sectioned RTM composite manufacturing, part 2. robust cure cycle optimization and control. J. Compos. Mater. 36, 1201–1231 (2002)CrossRef Michaud, D., Beris, A., Dhurjati, P.: Thick-sectioned RTM composite manufacturing, part 2. robust cure cycle optimization and control. J. Compos. Mater. 36, 1201–1231 (2002)CrossRef
23.
Zurück zum Zitat Yousefi, A., Lafleur, P.: Kinetic studies of thermoset cure Reactions-a review. Polym. Compos. 18(2), 157–168 (1997)CrossRef Yousefi, A., Lafleur, P.: Kinetic studies of thermoset cure Reactions-a review. Polym. Compos. 18(2), 157–168 (1997)CrossRef
24.
Zurück zum Zitat Shin, D., Hahn, H.: A consistent cure kinetic model for AS4/3502 graphite/epoxy. Compos. A: Appl. Sci. Manuf. 31(9), 991–999 (2000)CrossRef Shin, D., Hahn, H.: A consistent cure kinetic model for AS4/3502 graphite/epoxy. Compos. A: Appl. Sci. Manuf. 31(9), 991–999 (2000)CrossRef
25.
Zurück zum Zitat HexTow IM7 Carbon Fiber Datasheet, 2016, Hexcel Corporation HexTow IM7 Carbon Fiber Datasheet, 2016, Hexcel Corporation
26.
Zurück zum Zitat Springer, G., Tsai, S.: Thermal conductivities of unidirectional materials. J. Compos. Mater. 1, 166–173 (1967)CrossRef Springer, G., Tsai, S.: Thermal conductivities of unidirectional materials. J. Compos. Mater. 1, 166–173 (1967)CrossRef
27.
Zurück zum Zitat Kluge, N., Lundstrom, T., Westerberg, L., Nyman, T.: Modelling heat transfer inside an antoclave: effect of radiation. J. Reinf. Plast. Compos. 35(14), 1126–1142 (2016)CrossRef Kluge, N., Lundstrom, T., Westerberg, L., Nyman, T.: Modelling heat transfer inside an antoclave: effect of radiation. J. Reinf. Plast. Compos. 35(14), 1126–1142 (2016)CrossRef
Metadaten
Titel
Curing of Thick Thermoset Composite Laminates: Multiphysics Modeling and Experiments
verfasst von
S. Anandan
G. S. Dhaliwal
Z. Huo
K. Chandrashekhara
N. Apetre
N. Iyyer
Publikationsdatum
11.11.2017
Verlag
Springer Netherlands
Erschienen in
Applied Composite Materials / Ausgabe 5/2018
Print ISSN: 0929-189X
Elektronische ISSN: 1573-4897
DOI
https://doi.org/10.1007/s10443-017-9658-9

Weitere Artikel der Ausgabe 5/2018

Applied Composite Materials 5/2018 Zur Ausgabe

    Marktübersichten

    Die im Laufe eines Jahres in der „adhäsion“ veröffentlichten Marktübersichten helfen Anwendern verschiedenster Branchen, sich einen gezielten Überblick über Lieferantenangebote zu verschaffen.