Skip to main content
Fachgebiete
Automobil + Motoren Bauwesen + Immobilien Business IT + Informatik Elektrotechnik + Elektronik Energie + Nachhaltigkeit Finance + Banking Management + Führung Marketing + Vertrieb Maschinenbau + Werkstoffe Versicherung + Risiko
DE
EN
Bücher
Zeitschriften
Themenseiten
Organisationspsychologie Projektmanagement Marketing Smart Manufacturing
Weitere Formate
Podcasts Webinare Technik Webinare Wirtschaft Kongresse Veranstaltungskalender Awards
Jetzt Einzelzugang starten
Zugang für Unternehmen
Referenzkunden
SLX-Digitalkonferenz: Zukunftswerkstatt 2024

Mehr Umsatz mit Top-Kontakten

Am 7. Mai erfahren Sie, wie Vertriebsteams Leadgenerierung, Leadnurturing und Leadstrategien effizient steuern können.
Erweiterte Suche
Anmelden
nach oben
Journal of Materials Science
Erschienen in: Journal of Materials Science 15/2015

01.08.2015 | Original Paper

Digital image correlation measurement of resin chemical and thermal shrinkage after gelation

verfasst von: Oleksandr G. Kravchenko, Segii G. Kravchenko, Aaron Casares, R. Byron Pipes

Erschienen in: Journal of Materials Science | Ausgabe 15/2015

Einloggen

Aktivieren Sie unsere intelligente Suche, um passende Fachinhalte oder Patente zu finden.

search-config
loading …

Abstract

A method for measuring chemical shrinkage and coefficient of thermal expansion during cure and post-gelation is presented based on digital image correlation to record the in situ stress-free strain field in a thermosetting polymer. An independent determination of the resin cure kinetics was required to relate the chemical shrinkage strain and coefficient of thermal expansion to the degree of cure. The changes in the coefficient of thermal expansion were observed from the initial heating to final cooling of the sample. The results obtained are shown to compare favorably with results previously found by other techniques. The proposed method provides a simple and reliable procedure to measure the evolution of thermo-chemical shrinkage properties of the resin during the cure cycle.
Vorheriger Artikel Metastable microstructures containing zero valent iron for fast degradation of azo dyes
Nächster Artikel Constitutive model parameters of concentrated bentonite suspensions modified with sodium pyrophosphate

Sie haben noch keine Lizenz? Dann Informieren Sie sich jetzt über unsere Produkte:

Springer Professional "Wirtschaft+Technik"

Online-Abonnement

Mit Springer Professional "Wirtschaft+Technik" erhalten Sie Zugriff auf:

  • über 102.000 Bücher
  • über 537 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Finance + Banking
  • Management + Führung
  • Marketing + Vertrieb
  • Maschinenbau + Werkstoffe
  • Versicherung + Risiko

Jetzt Wissensvorsprung sichern!

Jetzt informieren

Springer Professional "Technik"

Online-Abonnement

Mit Springer Professional "Technik" erhalten Sie Zugriff auf:

  • über 67.000 Bücher
  • über 390 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Maschinenbau + Werkstoffe




 

Jetzt Wissensvorsprung sichern!

Jetzt informieren
Literatur
1.
Madhukar MS, Genidy MS, Russell JD (2000) A new method to reduce cure-induced stresses in thermoset polymer composites, Part I: test method. J Compos Mater 34:1882–1904CrossRef
2.
Kravchenko OG, Li C, Strachan A, Kravchenko SG, Pipes RB (2014) Prediction of the chemical and thermal shrinkage in a thermoset polymer. Compos A Appl Sci Manuf 66:35–43CrossRef
3.
Snow AW, Armistead JP (1994) A simple dilatometer for thermoset cure shrinkage and thermal expansion measurements. J Appl Polym Sci 52:401–411CrossRef
4.
Zarrelli M, Skordos AA, Partridge IK (2002) Investigation of cure induced shrinkage in unreinforced epoxy resin. Plast Rubber Compos 31:377–384CrossRef
5.
Nawab Y, Casari P, Boyard N, Jacquemin F (2013) Characterization of the cure shrinkage, reaction kinetics, bulk modulus and thermal conductivity of thermoset resin from a single experiment. J Mater Sci 48:2394–2403. doi:10.​1007/​s10853-012-7026-6 CrossRef
6.
Li C, Potter K, Wisnom MR, Stringer G (2004) In-situ measurement of chemical shrinkage of MY750 epoxy resin by a novel gravimetric method. Compos Sci Technol 64:55–64CrossRef
7.
Daniel IM, Wang T-M, Karalekas D, Gotro JT (1990) Determination of chemical cure shrinkage in composite laminates. J Compos Technol Res 12:172–176CrossRef
8.
Hoa SV, Ouellette P, Ngo TD (2009) Determination of shrinkage and modulus development of thermosetting resins. J Compos Mater 43:783–803CrossRef
9.
Lange J, Toll S, Månson J-AE, Hult A (1995) Residual stress build-up in thermoset films cured above their ultimate glass transition temperature. Polymer 36:3135–3141CrossRef
10.
Bucknall CB, Partridge IK, Phillips MJ (1991) Mechanism of shrinkage control in polyester resins containing low-profile additives. Polymer 32:636–640CrossRef
11.
Garstka T, Ersoy N, Potter KD, Wisnom MR (2007) In situ measurements of through-the-thickness strains during processing of AS4/8552 composite. Compos A Appl Sci Manuf 38:2517–2526CrossRef
12.
Khoun L, Hubert P (2010) Cure shrinkage characterization of an epoxy resin system by two in situ measurement methods. Polym Compos 31:1603–1610CrossRef
13.
14.
Sutton M, Wolters W, Peters W, Ranson W, McNeill S (1983) Determination of displacements using an improved digital correlation method. Image Vis Comput 1:133–139CrossRef
15.
Taher ST, Thomsen OT, Dulieu-Barton JM, Zhang S (2012) Determination of mechanical properties of PVC foam using a modified Arcan fixture. Compos A Appl Sci Manuf 43:1698–1708CrossRef
16.
Diaz JA, Wu X, Martini A, Youngblood JP, Moon RJ (2013) Thermal expansion of self-organized and shear-oriented cellulose nanocrystal films. Biomacromolecules 14:2900–2908CrossRef
17.
18.
Simon SL, Mckenna GB, Sindt O (2000) Modeling the evolution of the dynamic mechanical properties of a commercial epoxy during cure after gelation. J Appl Polym Sci 76:495–508CrossRef
19.
Karkanas PI, Partridge IK (2000) Cure modeling and monitoring of epoxy/amine resin systems. I. Cure kinetics modeling. J Appl Polym Sci 77:1419–1431CrossRef
20.
E37 Committee (2014) Test method for assignment of the glass transition temperatures by differential scanning calorimetry. ASTM International, West Conshohocken, PA. http://​www.​astm.​org/​
21.
Nielsen LE (1969) Cross-linking–effect on physical properties of polymers. J Macromol Sci C 3:69–103CrossRef
22.
Li C, Medvedev GA, Lee E-W, Kim J, Caruthers JM, Strachan A (2012) Molecular dynamics simulations and experimental studies of the thermomechanical response of an epoxy thermoset polymer. Polymer 53:4222–4230CrossRef
23.
Kasapis S, Al-Marhoobi IM, Mitchell JR (2003) Testing the validity of comparisons between the rheological and the calorimetric glass transition temperatures. Carbohydr Res 338:787–794CrossRef
24.
Deszczynski M, Kasapis S, MacNaughton W, Mitchell JR (2002) High sugar/polysaccharide glasses: resolving the role of water molecules in structure formation. Int J Biol Macromol 30:279–282CrossRef
Metadaten
Titel
Digital image correlation measurement of resin chemical and thermal shrinkage after gelation
verfasst von
Oleksandr G. Kravchenko
Segii G. Kravchenko
Aaron Casares
R. Byron Pipes
Publikationsdatum
01.08.2015
Verlag
Springer US
Erschienen in
Journal of Materials Science / Ausgabe 15/2015
Print ISSN: 0022-2461
Elektronische ISSN: 1573-4803
DOI
https://doi.org/10.1007/s10853-015-9072-3

Weitere Artikel der Ausgabe 15/2015

Journal of Materials Science 15/2015 Zur Ausgabe

Original Paper

Local octahedral rotations and octahedral connectivity in epitaxially strained LaNiO3/LaGaO3 superlattices

Original Paper

Cycling performance and morphological evolution of pulsed laser-deposited FeF2 thin film cathodes for Li-ion batteries

Original Paper

Preparation of hollow core/shell CeO2@TiO2 with enhanced photocatalytic performance

Original Paper

Elasto-capillary collapse of circular tubes as a model for cellulosic wood fibres

Original Paper

Synthesis of TiO2-doped mesoporous nanobioactive glass particles and their cytocompatibility against osteoblast cell line

Original Paper

Superhydrophobic and superoleophilic “sponge-like” aerogels for oil/water separation

Premium Partner

    Marktübersichten

    Die im Laufe eines Jahres in der „adhäsion“ veröffentlichten Marktübersichten helfen Anwendern verschiedenster Branchen, sich einen gezielten Überblick über Lieferantenangebote zu verschaffen. 

    Zur Marktübersicht
    Bildnachweise