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2020 | OriginalPaper | Buchkapitel

3. Dynamics of Spray Granulation in Continuously Operated Horizontal Fluidized Beds

verfasst von : C. Neugebauer, E. Diez, L. Mielke, S. Palis, A. Bück, E. Tsotsas, A. Kienle, S. Heinrich

Erschienen in: Dynamic Flowsheet Simulation of Solids Processes

Verlag: Springer International Publishing

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Abstract

This chapter presents new findings on process and product design in continuous spray layering granulation in horizontal fluidized beds. The results are achieved by a multi-scale approach, combining single-particle characterization of the influence of drying conditions on layer formation and properties with meso-scale information of particle flow and recirculation between process chambers separated by weirs. On the macro-scale, population balance modeling is used to describe the overall process dynamics taking into account apparatus design and process conditions. New process regime maps are presented along with control concepts to guarantee stable and safe operation as well as desired particle properties.

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Literatur
1.
Zurück zum Zitat Diez, E., Meyer, K., Bück, A., Tsotsas, E., Heinrich, S.: Influence of process conditions on the product properties in a continuous fluidized bed spray granulation process. Chem. Eng. Res. Des. 139, 104–115 (2018) Diez, E., Meyer, K., Bück, A., Tsotsas, E., Heinrich, S.: Influence of process conditions on the product properties in a continuous fluidized bed spray granulation process. Chem. Eng. Res. Des. 139, 104–115 (2018)
2.
Zurück zum Zitat Ramkrishna, D.: Population Balances: Theory and Applications to Particulate Systems in Engineering. Academic Press, San Diego, CA (2000) Ramkrishna, D.: Population Balances: Theory and Applications to Particulate Systems in Engineering. Academic Press, San Diego, CA (2000)
3.
Zurück zum Zitat Bück, A., Peglow, M., Naumann, M., Tsotsas, E.: Population balance model for drying of droplets containing aggregating nanoparticles. AIChE J. 58(11), 3318–3328 (2012) Bück, A., Peglow, M., Naumann, M., Tsotsas, E.: Population balance model for drying of droplets containing aggregating nanoparticles. AIChE J. 58(11), 3318–3328 (2012)
4.
Zurück zum Zitat Burgschweiger, J., Tsotsas, E.: Experimental investigation and modelling of continuous fluidized bed drying under steady-state and dynamic conditions. Chem. Eng. Sci. 57(24), 5021–5038 (2002) Burgschweiger, J., Tsotsas, E.: Experimental investigation and modelling of continuous fluidized bed drying under steady-state and dynamic conditions. Chem. Eng. Sci. 57(24), 5021–5038 (2002)
5.
Zurück zum Zitat Peglow, M., Kumar, J., Heinrich, S., Warnecke, G., Tsotsas, E., Mörl, L., Wolf, B.: A generic population balance model for simultaneous agglomeration and drying in fluidized beds. Chem. Eng. Sci. 62(1–2), 513–532 (2007) Peglow, M., Kumar, J., Heinrich, S., Warnecke, G., Tsotsas, E., Mörl, L., Wolf, B.: A generic population balance model for simultaneous agglomeration and drying in fluidized beds. Chem. Eng. Sci. 62(1–2), 513–532 (2007)
6.
Zurück zum Zitat Seydel, P., Blömer, J., Bertling, J.: Modeling particle formation at spray drying using population balances. Drying Technol. 24(2), 137–146 (2006) Seydel, P., Blömer, J., Bertling, J.: Modeling particle formation at spray drying using population balances. Drying Technol. 24(2), 137–146 (2006)
7.
Zurück zum Zitat Vreman, A., van Lare, C., Hounslow, M.: A basic population balance model for fluidized bed spray granulation. Chem. Eng. Sci. 64, 4389–4398 (2009) Vreman, A., van Lare, C., Hounslow, M.: A basic population balance model for fluidized bed spray granulation. Chem. Eng. Sci. 64, 4389–4398 (2009)
8.
Zurück zum Zitat Maronga, S.J., Wnukowski, P.: Modelling of the three-domain fluidized-bed particulate coating process. Chem. Eng. Sci. 52(17), 2915–2925 (1997) Maronga, S.J., Wnukowski, P.: Modelling of the three-domain fluidized-bed particulate coating process. Chem. Eng. Sci. 52(17), 2915–2925 (1997)
9.
Zurück zum Zitat Sherony, D.F.: A model of surface renewal with application to fluid bed coating of particles. Chem. Eng. Sci. 36(5), 845–848 (1981) Sherony, D.F.: A model of surface renewal with application to fluid bed coating of particles. Chem. Eng. Sci. 36(5), 845–848 (1981)
10.
Zurück zum Zitat Wnukowski, P., Setterwall, F.: The coating of particles in a fluidized bed (residence time distribution in a system of two coupled perfect mixers). Chem. Eng. Sci. 44(3), 493–505 (1989) Wnukowski, P., Setterwall, F.: The coating of particles in a fluidized bed (residence time distribution in a system of two coupled perfect mixers). Chem. Eng. Sci. 44(3), 493–505 (1989)
11.
Zurück zum Zitat Bück, A., Neugebauer, C., Meyer, K., Palis, S., Diez, E., Kienle, A., Heinrich, S., Tsotsas, E.: Influence of operation parameters on process stability in continuous fluidized bed layering with external classification. Powder Technol. 300, 37–45 (2016) Bück, A., Neugebauer, C., Meyer, K., Palis, S., Diez, E., Kienle, A., Heinrich, S., Tsotsas, E.: Influence of operation parameters on process stability in continuous fluidized bed layering with external classification. Powder Technol. 300, 37–45 (2016)
12.
Zurück zum Zitat Dreyschultze, C., Neugebauer, C., Palis, S., Bück, A., Tsotsas, E., Heinrich, S., Kienle, A.: Influence of zone formation on stability of continuous fluidized bed spray granulation with external product classification. Particuology 23, 1–7 (2015) Dreyschultze, C., Neugebauer, C., Palis, S., Bück, A., Tsotsas, E., Heinrich, S., Kienle, A.: Influence of zone formation on stability of continuous fluidized bed spray granulation with external product classification. Particuology 23, 1–7 (2015)
13.
Zurück zum Zitat Hampel, N., Bück, A., Peglow, M., Tsotsas, E.: Continuous pellet coating in a Wurster fluidized bed process. Chem. Eng. Sci. 86, 87–98 (2013) Hampel, N., Bück, A., Peglow, M., Tsotsas, E.: Continuous pellet coating in a Wurster fluidized bed process. Chem. Eng. Sci. 86, 87–98 (2013)
14.
Zurück zum Zitat Neugebauer, C., Palis, S., Bück, A., Tsotsas, E., Heinrich, S., Kienle, A.: A dynamic two zone model of continuous fluidized bed layering granulation with internal product classification. Particuology 31, 8–14 (2017) Neugebauer, C., Palis, S., Bück, A., Tsotsas, E., Heinrich, S., Kienle, A.: A dynamic two zone model of continuous fluidized bed layering granulation with internal product classification. Particuology 31, 8–14 (2017)
15.
Zurück zum Zitat Mörl, L., Heinrich, S., Peglow, M.: Fluidized bed spray granulation. In: Granulation, Handbook of Powder Technology (Chap. 2), vol. 11, pp 21–188. Elsevier, Amsterdam (2007) Mörl, L., Heinrich, S., Peglow, M.: Fluidized bed spray granulation. In: Granulation, Handbook of Powder Technology (Chap. 2), vol. 11, pp 21–188. Elsevier, Amsterdam (2007)
16.
Zurück zum Zitat Rieck, C., Hoffmann, T., Bück, A., Peglow, M., Tsotsas, E.: Influence of drying conditions on layer porosity in fluidized bed spray granulation. Powder Technol. 272, 120–131 (2015) Rieck, C., Hoffmann, T., Bück, A., Peglow, M., Tsotsas, E.: Influence of drying conditions on layer porosity in fluidized bed spray granulation. Powder Technol. 272, 120–131 (2015)
17.
Zurück zum Zitat Meyer, K., Bück, A., Tsotsas, E.: Determination of particle exchange rates at over-flow weirs in horizontal fluidised beds by particle tracking velocimetry. Particuology 32, 1–9 (2017) Meyer, K., Bück, A., Tsotsas, E.: Determination of particle exchange rates at over-flow weirs in horizontal fluidised beds by particle tracking velocimetry. Particuology 32, 1–9 (2017)
18.
Zurück zum Zitat Boucher, D., Deng, Z., Leadbeater, T., Langlois, R., Renaud, M., Waters, K.: PEPT studies of heavy particle flow within a spiral concentrator. Miner. Eng. 62, 120–128 (2014) Boucher, D., Deng, Z., Leadbeater, T., Langlois, R., Renaud, M., Waters, K.: PEPT studies of heavy particle flow within a spiral concentrator. Miner. Eng. 62, 120–128 (2014)
19.
Zurück zum Zitat Nilsson, L., Wimmerstedt, R.: Residence time distribution and particle dispersion in a longitudinal-flow fluidised bed. Chem. Eng. Sci. 43, 1153–1160 (1988) Nilsson, L., Wimmerstedt, R.: Residence time distribution and particle dispersion in a longitudinal-flow fluidised bed. Chem. Eng. Sci. 43, 1153–1160 (1988)
20.
Zurück zum Zitat Satija, S., Zucker, I.: Hydrodynamics of vibro-fluidized beds. Drying Technol. 4, 19–43 (1986) Satija, S., Zucker, I.: Hydrodynamics of vibro-fluidized beds. Drying Technol. 4, 19–43 (1986)
21.
Zurück zum Zitat de Velden, M.V., Baeyens, J., Seville, J., Fan, X.: The solids flow in the riser of a circulating fluidised bed (CFB) viewed by positron emission particle tracking (PEPT). Powder Technol. 183, 290–296 (2008) de Velden, M.V., Baeyens, J., Seville, J., Fan, X.: The solids flow in the riser of a circulating fluidised bed (CFB) viewed by positron emission particle tracking (PEPT). Powder Technol. 183, 290–296 (2008)
22.
Zurück zum Zitat Börner, M., Peglow, M., Tsotsas, E.: Derivation of parameters for a two compartment population balance model of Wurster fluidized bed granulation. Powder Technol. 238, 122–131 (2013) Börner, M., Peglow, M., Tsotsas, E.: Derivation of parameters for a two compartment population balance model of Wurster fluidized bed granulation. Powder Technol. 238, 122–131 (2013)
23.
Zurück zum Zitat Hagemeier, T., Börner, M., Bück, A., Tsotsas, E.: A comparative study on optical techniques for the estimation of granular flow velocities. Chem. Eng. Sci. 131, 63–75 (2015a) Hagemeier, T., Börner, M., Bück, A., Tsotsas, E.: A comparative study on optical techniques for the estimation of granular flow velocities. Chem. Eng. Sci. 131, 63–75 (2015a)
24.
Zurück zum Zitat Hagemeier, T., Roloff, C., Bück, A., Tsotsas, E.: Estimation of particle dynamics in 2-D fluidized beds using particle tracking velocimetry. Particuology 22, 39–51 (2015b) Hagemeier, T., Roloff, C., Bück, A., Tsotsas, E.: Estimation of particle dynamics in 2-D fluidized beds using particle tracking velocimetry. Particuology 22, 39–51 (2015b)
25.
Zurück zum Zitat Bendicks, C., Tarlet, D., Roloff, C., Bordas, R., Wunderlich, B., Michaelis, B., Thevenin, D.: Improved 3-D particle tracking velocimetry with colored particles. J. Sign. Inf. Process. 2, 59–71 (2011) Bendicks, C., Tarlet, D., Roloff, C., Bordas, R., Wunderlich, B., Michaelis, B., Thevenin, D.: Improved 3-D particle tracking velocimetry with colored particles. J. Sign. Inf. Process. 2, 59–71 (2011)
26.
Zurück zum Zitat Capart, H., Young, D., Zech, Y.: Voronoi imaging methods for the measurement of granular flows. Exp. Fluids 32, 121–135 (2002) Capart, H., Young, D., Zech, Y.: Voronoi imaging methods for the measurement of granular flows. Exp. Fluids 32, 121–135 (2002)
27.
Zurück zum Zitat You, C., Zhao, H., Cai, Y., Qi, H., Xu, X.: Experimental investigation of interparticle collision rate in particulate flow. Int. J. Multiph. Flow 30, 1121–1138 (2004) You, C., Zhao, H., Cai, Y., Qi, H., Xu, X.: Experimental investigation of interparticle collision rate in particulate flow. Int. J. Multiph. Flow 30, 1121–1138 (2004)
28.
Zurück zum Zitat Charlou, C., Sauceau, M., Milhe, M., Arlabosse, P.: Application of Markov chains to the modeling of sludge flow in an agitated indirect continuous dryer. In: Proceedings of European Symposium on Drying (EuroDrying 2013), Paris (2013) Charlou, C., Sauceau, M., Milhe, M., Arlabosse, P.: Application of Markov chains to the modeling of sludge flow in an agitated indirect continuous dryer. In: Proceedings of European Symposium on Drying (EuroDrying 2013), Paris (2013)
29.
Zurück zum Zitat Bachmann, P., Bück, A., Tsotsas, E.: Investigation of the residence time behavior of particulate products and correlation for Bodenstein number in horizontal fluidized beds. Powder Technol. 301, 1067–1076 (2017a) Bachmann, P., Bück, A., Tsotsas, E.: Investigation of the residence time behavior of particulate products and correlation for Bodenstein number in horizontal fluidized beds. Powder Technol. 301, 1067–1076 (2017a)
30.
Zurück zum Zitat Bachmann, P., Bück, A., Tsotsas, E.: Investigation of the residence time behavior of particulate products and correlation for Bodenstein number in horizontal fluidized beds with internal weirs. Powder Technol. 308, 378–387 (2017b) Bachmann, P., Bück, A., Tsotsas, E.: Investigation of the residence time behavior of particulate products and correlation for Bodenstein number in horizontal fluidized beds with internal weirs. Powder Technol. 308, 378–387 (2017b)
31.
Zurück zum Zitat Deen, N., van Sint, A.M., van der Hoef, M., Kuipers, J.: Review of discrete particle modeling of fluidized beds. J. Chem. Eng. Sci. 62, 28–44 (2007) Deen, N., van Sint, A.M., van der Hoef, M., Kuipers, J.: Review of discrete particle modeling of fluidized beds. J. Chem. Eng. Sci. 62, 28–44 (2007)
32.
Zurück zum Zitat Pietsch, S., Kieckhefen, P., Heinrich, S., Müller, M., Schönherr, M., Kleine Jäger, F.: CFD-DEM modelling of circulation frequencies and residence times in a prismatic spouted bed. Chem. Eng. Res. Des. 132, 1105–1116 (2018) Pietsch, S., Kieckhefen, P., Heinrich, S., Müller, M., Schönherr, M., Kleine Jäger, F.: CFD-DEM modelling of circulation frequencies and residence times in a prismatic spouted bed. Chem. Eng. Res. Des. 132, 1105–1116 (2018)
33.
Zurück zum Zitat Kieckhefen, P., Lichtenegger, T., Pietsch, S., Pirker, S., Heinrich, S.: Simulation of spray coating in a spouted bed using recurrence CFD. Particuology 42, 92–103 (2019) Kieckhefen, P., Lichtenegger, T., Pietsch, S., Pirker, S., Heinrich, S.: Simulation of spray coating in a spouted bed using recurrence CFD. Particuology 42, 92–103 (2019)
34.
Zurück zum Zitat Fang, M., Luo, K., Yang, S., Zhang, K., Fan, J.: Computational fluid dynamics-discrete element method investigation of solid mixing characteristics in an internally circulating fluidized bed. Ind. Eng. Chem. Res. 52, 7556–7568 (2013) Fang, M., Luo, K., Yang, S., Zhang, K., Fan, J.: Computational fluid dynamics-discrete element method investigation of solid mixing characteristics in an internally circulating fluidized bed. Ind. Eng. Chem. Res. 52, 7556–7568 (2013)
35.
Zurück zum Zitat Wang, S., Luo, K., Hu, C., Fan, J.: CFD-DEM study of the effect of ring baffles on system performance of a full-loop circulating fluidized bed. Chem. Eng. Sci. 196, 130–144 (2019) Wang, S., Luo, K., Hu, C., Fan, J.: CFD-DEM study of the effect of ring baffles on system performance of a full-loop circulating fluidized bed. Chem. Eng. Sci. 196, 130–144 (2019)
36.
Zurück zum Zitat Yang, S., Cahyadi, A.: CFD-DEM investigation into the scaling up of spout-fluid beds via two interconnected chambers. AIChE J. 62, 1898–1916 (2016) Yang, S., Cahyadi, A.: CFD-DEM investigation into the scaling up of spout-fluid beds via two interconnected chambers. AIChE J. 62, 1898–1916 (2016)
37.
Zurück zum Zitat Yang, S., Zhang, L., Sun, Y., Chew, J.: Improving the operational stability of the multi-chamber spout-fluid bed via the insertion of a submerged partition. AIChE J. 63, 485–500 (2017) Yang, S., Zhang, L., Sun, Y., Chew, J.: Improving the operational stability of the multi-chamber spout-fluid bed via the insertion of a submerged partition. AIChE J. 63, 485–500 (2017)
38.
Zurück zum Zitat Weller, H., Tabor, G., Jasak, H., Fureby, C.: A tensorial approach to computational continuum mechanics using object-oriented techniques. Comput. Phys. 12, 620–631 (1998) Weller, H., Tabor, G., Jasak, H., Fureby, C.: A tensorial approach to computational continuum mechanics using object-oriented techniques. Comput. Phys. 12, 620–631 (1998)
39.
Zurück zum Zitat Zhou, Z., Kuang, S., Chu, K., Yu, A.: Discrete particle simulation of particle-fluid flow: model formulations and their applicability. J. Fluid Mech. 661, 482–510 (2010) Zhou, Z., Kuang, S., Chu, K., Yu, A.: Discrete particle simulation of particle-fluid flow: model formulations and their applicability. J. Fluid Mech. 661, 482–510 (2010)
40.
Zurück zum Zitat Goniva, C., Kloss, C., Deen, N., Kuipers, J., Pirker, S.: Influence of rolling friction on single spout fluidized bed simulation. Particuology 10, 582–591 (2012) Goniva, C., Kloss, C., Deen, N., Kuipers, J., Pirker, S.: Influence of rolling friction on single spout fluidized bed simulation. Particuology 10, 582–591 (2012)
41.
Zurück zum Zitat Kloss, C., Goniva, C., Hager, A., Amberger, S., Pirker, S.: Models, algorithms and validation for open source DEM and CFD-DEM. Prog. Comput. Fluid Dyn. 12, 140–152 (2012) Kloss, C., Goniva, C., Hager, A., Amberger, S., Pirker, S.: Models, algorithms and validation for open source DEM and CFD-DEM. Prog. Comput. Fluid Dyn. 12, 140–152 (2012)
42.
Zurück zum Zitat Diez, E., Kieckhefen, P., Meyer, K., Bück, A., Tsotsas, E., Heinrich, S.: Particle dynamics in a multi-staged fluidized bed: particle transport behavior on micro-scale by discrete particle modelling. Adv. Powder Technol. 30, 2014–2031 (2019) Diez, E., Kieckhefen, P., Meyer, K., Bück, A., Tsotsas, E., Heinrich, S.: Particle dynamics in a multi-staged fluidized bed: particle transport behavior on micro-scale by discrete particle modelling. Adv. Powder Technol. 30, 2014–2031 (2019)
43.
Zurück zum Zitat Hoffmann, T., Rieck, C., Bück, A., Tsotsas, E.: Influence of granule porosity during fluidized bed spray granulation. Proc. Eng. 102, 458–467 (2015) Hoffmann, T., Rieck, C., Bück, A., Tsotsas, E.: Influence of granule porosity during fluidized bed spray granulation. Proc. Eng. 102, 458–467 (2015)
44.
Zurück zum Zitat Wagner, W.: New vapour pressure measurements for argon and nitrogen and a new method for establishing rational vapour pressure equations. Cryogenics 13, 470–482 (1973) Wagner, W.: New vapour pressure measurements for argon and nitrogen and a new method for establishing rational vapour pressure equations. Cryogenics 13, 470–482 (1973)
45.
Zurück zum Zitat Tzika, M., Alexandridou, S., Kiparissides, C.: Evaluation of the morphological and release characteristics of coated fertilizer granules produced in a Wurster fluidized bed. Powder Technol. 132, 16–24 (2003) Tzika, M., Alexandridou, S., Kiparissides, C.: Evaluation of the morphological and release characteristics of coated fertilizer granules produced in a Wurster fluidized bed. Powder Technol. 132, 16–24 (2003)
46.
Zurück zum Zitat Whitehouse, D.: Surfaces and Their Measurement, pp. 16–95. Butterworth-Heinemann, Boston (2002) Whitehouse, D.: Surfaces and Their Measurement, pp. 16–95. Butterworth-Heinemann, Boston (2002)
47.
Zurück zum Zitat DIN EN ISO 25178-2 (2012) Geometrical product specifications (GPS)—Surface texture: Areal—Part 2: Terms, definitions and surface texture parameters. International Standards Organization DIN EN ISO 25178-2 (2012) Geometrical product specifications (GPS)—Surface texture: Areal—Part 2: Terms, definitions and surface texture parameters. International Standards Organization
48.
Zurück zum Zitat Dadkhah, M., Peglow, M., Tsotsas, E.: Characterization of the internal morphology of agglomerates produced in a spray fluidized bed by X-ray tomography. Powder Technol. 228, 349–358 (2012) Dadkhah, M., Peglow, M., Tsotsas, E.: Characterization of the internal morphology of agglomerates produced in a spray fluidized bed by X-ray tomography. Powder Technol. 228, 349–358 (2012)
49.
Zurück zum Zitat Sondej, F., Bück, A., Koslowsky, K., Bachmann, P., Jacob, M., Tsotsas, E.: Investigation of coating layer morphology by micro-computed X-ray tomography. Powder Technol. 273, 165–175 (2015) Sondej, F., Bück, A., Koslowsky, K., Bachmann, P., Jacob, M., Tsotsas, E.: Investigation of coating layer morphology by micro-computed X-ray tomography. Powder Technol. 273, 165–175 (2015)
50.
Zurück zum Zitat Antonyuk, S., Tomas, J., Heinrich, S., Mörl, L.: Breakage behaviour of spherical granulates by compression. Chem. Eng. Sci. 60, 4031–4044 (2005) Antonyuk, S., Tomas, J., Heinrich, S., Mörl, L.: Breakage behaviour of spherical granulates by compression. Chem. Eng. Sci. 60, 4031–4044 (2005)
51.
Zurück zum Zitat Litster, J., Ennis, B.: The Science and Engineering of Granulation Processes. Springer, New York (2004) Litster, J., Ennis, B.: The Science and Engineering of Granulation Processes. Springer, New York (2004)
52.
Zurück zum Zitat Neugebauer, C., Bück, A., Palis, S., Mielke, L., Tsotsas, E., Kienle, A.: Influence of thermal conditions on particle properties in fluidized bed layering granulation. Processes 6(12), 235 (2018) Neugebauer, C., Bück, A., Palis, S., Mielke, L., Tsotsas, E., Kienle, A.: Influence of thermal conditions on particle properties in fluidized bed layering granulation. Processes 6(12), 235 (2018)
53.
Zurück zum Zitat Schmidt, M., Bück, A., Tsotsas, E.: Experimental investigation of the influence of drying conditions on process stability of continuous spray fluidized bed layering granulation with external product separation. Powder Technol. 320, 474–482 (2017) Schmidt, M., Bück, A., Tsotsas, E.: Experimental investigation of the influence of drying conditions on process stability of continuous spray fluidized bed layering granulation with external product separation. Powder Technol. 320, 474–482 (2017)
54.
Zurück zum Zitat Neugebauer, C., Bück, A., Kienle, A.: Control of particle size and porosity in continuous fluidized bed layering granulation processes with sieve mill cycle. Chem. Eng. Technol. 43(5), 813–818 (2020) Neugebauer, C., Bück, A., Kienle, A.: Control of particle size and porosity in continuous fluidized bed layering granulation processes with sieve mill cycle. Chem. Eng. Technol. 43(5), 813–818 (2020)
55.
Zurück zum Zitat Heinrich, S., Peglow, M., Ihlow, M., Henneberg, M., Mörl, L.: Analysis of start-up process in continuous fluidized bed spray granulation by population balance modeling. Chem. Eng. Sci. 57, 4369–4390 (2002) Heinrich, S., Peglow, M., Ihlow, M., Henneberg, M., Mörl, L.: Analysis of start-up process in continuous fluidized bed spray granulation by population balance modeling. Chem. Eng. Sci. 57, 4369–4390 (2002)
56.
Zurück zum Zitat Radichkov, R., Müller, T., Kienle, A., Heinrich, S., Peglow, M., Mörl, L.: A numerical bifurcation analysis of fluidized bed spray granulation with external classification. Chem. Eng. Process. 45, 826–837 (2006) Radichkov, R., Müller, T., Kienle, A., Heinrich, S., Peglow, M., Mörl, L.: A numerical bifurcation analysis of fluidized bed spray granulation with external classification. Chem. Eng. Process. 45, 826–837 (2006)
57.
Zurück zum Zitat Schmidt, M., Bück, A., Tsotsas, E.: Experimental investigation of process stability of continuous spray fludized bed layering granulation with internal separation. Chem. Eng. Sci. 126, 55–66 (2015a) Schmidt, M., Bück, A., Tsotsas, E.: Experimental investigation of process stability of continuous spray fludized bed layering granulation with internal separation. Chem. Eng. Sci. 126, 55–66 (2015a)
58.
Zurück zum Zitat Schmidt, M., Rieck, C., Bück, A., Tsotsas, E.: Experimental investigation of process stability of continuous spray fludized bed layering granulation with external product separation. Chem. Eng. Sci. 137, 466–475 (2015b) Schmidt, M., Rieck, C., Bück, A., Tsotsas, E.: Experimental investigation of process stability of continuous spray fludized bed layering granulation with external product separation. Chem. Eng. Sci. 137, 466–475 (2015b)
59.
Zurück zum Zitat Neugebauer, C., Palis, S., Bück, A., Diez, E., Heinrich, S., Tsotsas, E., Kienle, A.: Influence of mill characteristics on stability of continuous layering granulation with external product classification. Comput. Aided Chem. Eng. 38, 1275–1280 (2016) Neugebauer, C., Palis, S., Bück, A., Diez, E., Heinrich, S., Tsotsas, E., Kienle, A.: Influence of mill characteristics on stability of continuous layering granulation with external product classification. Comput. Aided Chem. Eng. 38, 1275–1280 (2016)
60.
Zurück zum Zitat Palis, S., Dreyschultze, C., Neugebauer, C., Kienle, A.: Auto-tuning control systems for improved operation of continuous fluidized bed spray granulation processes with external product classifcation. Proc. Eng. 102, 133–141 (2015) Palis, S., Dreyschultze, C., Neugebauer, C., Kienle, A.: Auto-tuning control systems for improved operation of continuous fluidized bed spray granulation processes with external product classifcation. Proc. Eng. 102, 133–141 (2015)
61.
Zurück zum Zitat Palis, S., Dreyschultze, C., Kienle, A.: A methodology for experimental determination of stability boundaries with application to fluidized bed spray granulation. In: Computer Aided Chemical Engineering, vol. 33, pp 625–630. Elsevier, Amsterdam (2014) Palis, S., Dreyschultze, C., Kienle, A.: A methodology for experimental determination of stability boundaries with application to fluidized bed spray granulation. In: Computer Aided Chemical Engineering, vol. 33, pp 625–630. Elsevier, Amsterdam (2014)
62.
Zurück zum Zitat Palis, S., Neugebauer, C., Bück, A., Heinrich, S., Tsotsas, E., Kienle, A.: Control of multi-chamber continuous fluidized bed spray granulation. In: Proceedings of PARTEC 2016: International Congress on Particle Technology: Nürnberg, Germany, April 19–21 (2016) Palis, S., Neugebauer, C., Bück, A., Heinrich, S., Tsotsas, E., Kienle, A.: Control of multi-chamber continuous fluidized bed spray granulation. In: Proceedings of PARTEC 2016: International Congress on Particle Technology: Nürnberg, Germany, April 19–21 (2016)
63.
Zurück zum Zitat Palis, S.: Control of multi-chamber continuous fluidized bed spray granulation. In: Proceedings of the 12th IFAC Symposium on Dynamics and Control of Process Systems—DYCOPS 2019, Florianopolis/Brazil, 23-26 April, iFAC-PapersOnLine, vol. 52(1), pp. 406–411 (2019) Palis, S.: Control of multi-chamber continuous fluidized bed spray granulation. In: Proceedings of the 12th IFAC Symposium on Dynamics and Control of Process Systems—DYCOPS 2019, Florianopolis/Brazil, 23-26 April, iFAC-PapersOnLine, vol. 52(1), pp. 406–411 (2019)
64.
Zurück zum Zitat Palis, S.: Non-identifier-based adaptive control of continuous fluidized bed spray granulation with external sieve-mill cycle. J. Process Control 71, 46–51 (2019b) Palis, S.: Non-identifier-based adaptive control of continuous fluidized bed spray granulation with external sieve-mill cycle. J. Process Control 71, 46–51 (2019b)
65.
Zurück zum Zitat Neugebauer, C., Diez, E., Bück, A., Palis, S., Heinrich, S., Kienle, A.: Dynamics and control of continuous fluidized bed layering granulation with screen-mill-cycle. Powder Technol. 354, 765–778 (2019b) Neugebauer, C., Diez, E., Bück, A., Palis, S., Heinrich, S., Kienle, A.: Dynamics and control of continuous fluidized bed layering granulation with screen-mill-cycle. Powder Technol. 354, 765–778 (2019b)
66.
Zurück zum Zitat Bück, A., Palis, S., Tsotsas, E.: Model-based control of particle properties in fluidised bed spray granulation. Powder Technol. 270, 575–583 (2015) Bück, A., Palis, S., Tsotsas, E.: Model-based control of particle properties in fluidised bed spray granulation. Powder Technol. 270, 575–583 (2015)
67.
Zurück zum Zitat Palis, S., Kienle, A.: Stabilization of continuous fluidized bed spray granulation with external product classification. Chem. Eng. Sci. 70, 200–209 (2012) Palis, S., Kienle, A.: Stabilization of continuous fluidized bed spray granulation with external product classification. Chem. Eng. Sci. 70, 200–209 (2012)
68.
Zurück zum Zitat Palis, S., Kienle, A.: H\(_{\infty }\) loop shaping control for continuous fluidized bed spray granulation with internal product classification. Ind. Eng. Chem. Res. 52, 408–420 (2013) Palis, S., Kienle, A.: H\(_{\infty }\) loop shaping control for continuous fluidized bed spray granulation with internal product classification. Ind. Eng. Chem. Res. 52, 408–420 (2013)
69.
Zurück zum Zitat Palis, S., Kienle, A.: Discrepancy based control of particulate processes. J. Process Control 24, 33–46 (2014) Palis, S., Kienle, A.: Discrepancy based control of particulate processes. J. Process Control 24, 33–46 (2014)
Metadaten
Titel
Dynamics of Spray Granulation in Continuously Operated Horizontal Fluidized Beds
verfasst von
C. Neugebauer
E. Diez
L. Mielke
S. Palis
A. Bück
E. Tsotsas
A. Kienle
S. Heinrich
Copyright-Jahr
2020
DOI
https://doi.org/10.1007/978-3-030-45168-4_3