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2017 | OriginalPaper | Buchkapitel

Effect of Extrusion Ratio on Microstructure and Resulting Mechanical Properties of Mg Alloys with LPSO Phase

verfasst von : Klaudia Horváth, Daria Drozdenko, Gerardo Garcés, Kristián Máthis, Patrik Dobroň

Erschienen in: Magnesium Technology 2017

Verlag: Springer International Publishing

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Abstract

The WZ21 (Mg + 1.8 wt% Y + 0.7 wt% Zn) magnesium alloy having an addition of 0.5 wt% of CaO was extruded with different extrusion ratios (4:1, 10:1, 18:1) at 350 °C. In all alloys, a long-period stacking-ordered (LPSO) phase composed of Zn and Y is formed. The microstructure was analyzed by electron backscatter diffraction (EBSD) mapping. The WZ21 alloy after extrusion with the extrusion ratio of 4:1 contains large grains. The fraction of recrystallized grains increases with increasing extrusion ratio. All samples have basal planes oriented parallel to the extrusion direction (ED) and this texture weaken with increasing extrusion ratio. Mechanical properties of the samples were investigated during compression along ED at room temperature and at a constant strain rate of 10−3 s−1. Concurrently, with the deformation tests, the acoustic emission (AE) response of the specimens was recorded. The maximum of the AE count rate in all cases corresponds to the macroscopic yield point.

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Literatur
1.
Zurück zum Zitat M.M. Avedesian, H. Baker: Magnesium and Magnesium Alloys (ASM Specialty Handbook). ASM International (1999) (ISBN 0-87170-657-1) M.M. Avedesian, H. Baker: Magnesium and Magnesium Alloys (ASM Specialty Handbook). ASM International (1999) (ISBN 0-87170-657-1)
2.
Zurück zum Zitat E. Abe, Y. Kawamura, K. Hayashi, A. Inoue, Long-period ordered structure in a high-strength nanocrystalline Mg-1 at% Zn-2 at% Y alloy studied by atomic-resolution Z-contrast STEM. Acta Mater. 50, 3845–3857 (2002)CrossRef E. Abe, Y. Kawamura, K. Hayashi, A. Inoue, Long-period ordered structure in a high-strength nanocrystalline Mg-1 at% Zn-2 at% Y alloy studied by atomic-resolution Z-contrast STEM. Acta Mater. 50, 3845–3857 (2002)CrossRef
3.
Zurück zum Zitat D. Egusa, E. Abe, The structure of long period stacking/order Mg–Zn–RE phases with extended non-stoichiometry ranges. Acta Mater. 60, 166–178 (2012)CrossRef D. Egusa, E. Abe, The structure of long period stacking/order Mg–Zn–RE phases with extended non-stoichiometry ranges. Acta Mater. 60, 166–178 (2012)CrossRef
4.
Zurück zum Zitat Y. Kawamura, M. Yamasaki, Formation and mechanical properties of Mg97Zn(1)Re(2) alloys with long-period stacking ordered structure. Mater. Trans. 48, 2986–2992 (2007)CrossRef Y. Kawamura, M. Yamasaki, Formation and mechanical properties of Mg97Zn(1)Re(2) alloys with long-period stacking ordered structure. Mater. Trans. 48, 2986–2992 (2007)CrossRef
5.
Zurück zum Zitat M. Yamasaki, K. Hashimoto, K. Hagihara, Y. Kawamura, Effect of multimodal microstructure on mechanical properties of Mg-Zn-Y extruded alloy. Acta Mater. 59, 3646–3658 (2011)CrossRef M. Yamasaki, K. Hashimoto, K. Hagihara, Y. Kawamura, Effect of multimodal microstructure on mechanical properties of Mg-Zn-Y extruded alloy. Acta Mater. 59, 3646–3658 (2011)CrossRef
6.
Zurück zum Zitat Y. Kawamura, T. Kasahara, S. Izumi, M. Yamasaki, Elevated temperature Mg97Z2Cu1 alloy with long period ordered structure. Scr. Mater 55, 453–456 (2006)CrossRef Y. Kawamura, T. Kasahara, S. Izumi, M. Yamasaki, Elevated temperature Mg97Z2Cu1 alloy with long period ordered structure. Scr. Mater 55, 453–456 (2006)CrossRef
7.
Zurück zum Zitat K. Hagihara, N. Yokotami, Y. Umakoshi, Plastic deformation of Mg12YZn with 18R long-period stacking ordered structure. Intermetallics 18, 267–276 (2010)CrossRef K. Hagihara, N. Yokotami, Y. Umakoshi, Plastic deformation of Mg12YZn with 18R long-period stacking ordered structure. Intermetallics 18, 267–276 (2010)CrossRef
8.
Zurück zum Zitat K. Hagihara, Y. Sugino, Y. Fukusumi, Y. Umakoshi, T. Nakano, Plastuc deformation behavior of Mg12ZnY LPSO-phase with 14H-typed structure. Mater. Trans. 52, 1096–1103 (2011)CrossRef K. Hagihara, Y. Sugino, Y. Fukusumi, Y. Umakoshi, T. Nakano, Plastuc deformation behavior of Mg12ZnY LPSO-phase with 14H-typed structure. Mater. Trans. 52, 1096–1103 (2011)CrossRef
9.
Zurück zum Zitat J.K. Kim, S. Sandlöbes, D. Raabe, On the room temperature deformation mechanisms of a Mg-Y-Zn alloy with long-period-stacking-ordered structures. Acta Mater. 82, 414–423 (2015)CrossRef J.K. Kim, S. Sandlöbes, D. Raabe, On the room temperature deformation mechanisms of a Mg-Y-Zn alloy with long-period-stacking-ordered structures. Acta Mater. 82, 414–423 (2015)CrossRef
10.
Zurück zum Zitat G. Garcés, D.G. Morris, M.A. Muňoz-Morris, P. Perez, D. Tolnai, C. Mendis, A. Stark, H.K. Lim, S. Kim, N. Shell, P. Adva, Plasticity analysis by synchrotron radiation in a Mg97Y2Zn1 alloy with bimodal grain structure and containing LPSO phase. Acta Mater. 94, 78–86 (2015)CrossRef G. Garcés, D.G. Morris, M.A. Muňoz-Morris, P. Perez, D. Tolnai, C. Mendis, A. Stark, H.K. Lim, S. Kim, N. Shell, P. Adva, Plasticity analysis by synchrotron radiation in a Mg97Y2Zn1 alloy with bimodal grain structure and containing LPSO phase. Acta Mater. 94, 78–86 (2015)CrossRef
11.
Zurück zum Zitat X.P. Yhang, S. Castagne, X.F. Luo, C.F. Gu, Effects of extrusion ratio on the ratcheting behavior of extruded AZ31B magnesium alloy under asymmetrical uniaxial cyclic loading. Mat. Sci. Eng. A 528, 838–845 (2011)CrossRef X.P. Yhang, S. Castagne, X.F. Luo, C.F. Gu, Effects of extrusion ratio on the ratcheting behavior of extruded AZ31B magnesium alloy under asymmetrical uniaxial cyclic loading. Mat. Sci. Eng. A 528, 838–845 (2011)CrossRef
12.
Zurück zum Zitat X. Zhang, G. Yuan, J. Niu, P. Fu, W. Ding, Microstructure, mechanical properties, biocorrosion behavior and cytotoxicity of as/extruded Mg-Nd-Yn-Yr alloy with different extrusion ratios. J. Mech. Behav. Biomed 9, 153–162 (2012)CrossRef X. Zhang, G. Yuan, J. Niu, P. Fu, W. Ding, Microstructure, mechanical properties, biocorrosion behavior and cytotoxicity of as/extruded Mg-Nd-Yn-Yr alloy with different extrusion ratios. J. Mech. Behav. Biomed 9, 153–162 (2012)CrossRef
13.
Zurück zum Zitat J. Bohlen, S.B. Yi, D. Letzig, K.U. Kainer, Effect of rare earths elements on the microstructure and texture development in magnesium-manganese alloys during extrusion. Mater. Sci. Eng. A 527, 7092–7098 (2010)CrossRef J. Bohlen, S.B. Yi, D. Letzig, K.U. Kainer, Effect of rare earths elements on the microstructure and texture development in magnesium-manganese alloys during extrusion. Mater. Sci. Eng. A 527, 7092–7098 (2010)CrossRef
14.
Zurück zum Zitat P. Dobroň, F. Chmelík, S. Yi, K. Parfenenko, D. Letzig, J. Bohlen, Grain size effects on deformation twinning in an extruded magnesium alloy tested in compression. Scr. Mater. 65, 424–427 (2011)CrossRef P. Dobroň, F. Chmelík, S. Yi, K. Parfenenko, D. Letzig, J. Bohlen, Grain size effects on deformation twinning in an extruded magnesium alloy tested in compression. Scr. Mater. 65, 424–427 (2011)CrossRef
15.
Zurück zum Zitat P. Dobroň, F. Chmelík, K. Parfenenko, D. Letzig, J. Bohlen, On the Effect of the Extrusion Speed on Microstructure and Plastic Deformation of ZE10 and ZEK100 Magnesium Alloys - an Acoustic Emission Study. Acta Phys. Pol. A 122(3), 593–596 (2012)CrossRef P. Dobroň, F. Chmelík, K. Parfenenko, D. Letzig, J. Bohlen, On the Effect of the Extrusion Speed on Microstructure and Plastic Deformation of ZE10 and ZEK100 Magnesium Alloys - an Acoustic Emission Study. Acta Phys. Pol. A 122(3), 593–596 (2012)CrossRef
16.
Zurück zum Zitat J. Čapek, K. Máthis, B. Clausen, J. Stráská, P. Beran, P. Lukáš, Study of the loading mode dependence of the twinning in random textured cast magnesium by acoustic emission and neutron diffraction methods. Mater. Sci. Eng. A 602, 25–32 (2014)CrossRef J. Čapek, K. Máthis, B. Clausen, J. Stráská, P. Beran, P. Lukáš, Study of the loading mode dependence of the twinning in random textured cast magnesium by acoustic emission and neutron diffraction methods. Mater. Sci. Eng. A 602, 25–32 (2014)CrossRef
17.
Zurück zum Zitat A. Vinogradov, D. Orlov, A. Danyuk, Y. Estrin, Effect of grain size on the mechanisms of plastic deformation in wrought Mg-Zn-Zr alloy revealed by acoustic emission technique. Acta Mater. 61, 20144–22056 (2013) A. Vinogradov, D. Orlov, A. Danyuk, Y. Estrin, Effect of grain size on the mechanisms of plastic deformation in wrought Mg-Zn-Zr alloy revealed by acoustic emission technique. Acta Mater. 61, 20144–22056 (2013)
18.
Zurück zum Zitat D.L. Yin, J.T. Wang, J.Q. Liu, X. Zhao, On tension–compression yield asymmetry in an extruded Mg–3Al–1Zn alloy. J. Alloys Compd. 478, 789–795 (2009)CrossRef D.L. Yin, J.T. Wang, J.Q. Liu, X. Zhao, On tension–compression yield asymmetry in an extruded Mg–3Al–1Zn alloy. J. Alloys Compd. 478, 789–795 (2009)CrossRef
19.
Zurück zum Zitat W.F. Hosford, The Mechanics of Crystals and Textured Polycrystals (Oxford University Press, Oxford, 1993) W.F. Hosford, The Mechanics of Crystals and Textured Polycrystals (Oxford University Press, Oxford, 1993)
20.
Zurück zum Zitat C.R. Heiple, S.H. Carpenter, Acoustic emission produced by deformation of metals and alloys—a review: Part I. J. Acoust. Emission 6, 177 (1987) C.R. Heiple, S.H. Carpenter, Acoustic emission produced by deformation of metals and alloys—a review: Part I. J. Acoust. Emission 6, 177 (1987)
21.
Zurück zum Zitat G. Garcés, P. Perez, S. Cabeza, H.K. Lin, S. Kim, W. Gan, P. Adeva, Reverse tension/compression asymmetry of a Mg-Y-Zn alloys containing LPSO phase. Mat. Sci. Eng. A 647, 287–293 (2015)CrossRef G. Garcés, P. Perez, S. Cabeza, H.K. Lin, S. Kim, W. Gan, P. Adeva, Reverse tension/compression asymmetry of a Mg-Y-Zn alloys containing LPSO phase. Mat. Sci. Eng. A 647, 287–293 (2015)CrossRef
22.
Zurück zum Zitat J. Bohlen, F. Chmelík, P. Dobroň, D. Letzig, P. Lukáč, K.U. Kainer, Acoustic emission during tensile testing of magnesium AZ alloys. J. Alloys Comp. 378, 214–219 (2004)CrossRef J. Bohlen, F. Chmelík, P. Dobroň, D. Letzig, P. Lukáč, K.U. Kainer, Acoustic emission during tensile testing of magnesium AZ alloys. J. Alloys Comp. 378, 214–219 (2004)CrossRef
Metadaten
Titel
Effect of Extrusion Ratio on Microstructure and Resulting Mechanical Properties of Mg Alloys with LPSO Phase
verfasst von
Klaudia Horváth
Daria Drozdenko
Gerardo Garcés
Kristián Máthis
Patrik Dobroň
Copyright-Jahr
2017
DOI
https://doi.org/10.1007/978-3-319-52392-7_8

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