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Erschienen in: Journal of Sol-Gel Science and Technology 2/2019

17.12.2018 | Original Paper: Sol–gel and hybrid materials for catalytic, photoelectrochemical and sensor applications

Facile synthesis of ZnO nanosheets as ultraviolet photocatalyst

verfasst von: H. Vahdat Vasei, S. M. Masoudpanah, M. Adeli, M. R. Aboutalebi

Erschienen in: Journal of Sol-Gel Science and Technology | Ausgabe 2/2019

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Abstract

ZnO powders were prepared by solution combustion synthesis method by means of sodium dodecyl sulfate (SDS) as fuel and SDS-citric acid mixed fuel at various fuel contents. Phase evolution studied by X-ray powder diffractometry showed single phase ZnO powders were directly formed by using mixed fuels, while the layered Zn4SO4(OH)6.nH2O impurity phase together with ZnO was formed by SDS fuel alone. The as-combusted ZnO powders using SDS fuel are composed of hexagonal nanosheets with the thickness of 70 nm, as observed by electron microscopy. However, the spongy powders with spherical particles achieved by mixture of fuels exhibited higher specific surface area on account of larger amounts of released gaseous products during combustion. The ZnO catalyst prepared by mixed fuel at ϕ = 0.75 showed the highest photodegradation (~96%) of methylene blue (MB), while about only 6% of MB was photodegraded by ZnO nanosheets under ultraviolet light irradiation.

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Metadaten
Titel
Facile synthesis of ZnO nanosheets as ultraviolet photocatalyst
verfasst von
H. Vahdat Vasei
S. M. Masoudpanah
M. Adeli
M. R. Aboutalebi
Publikationsdatum
17.12.2018
Verlag
Springer US
Erschienen in
Journal of Sol-Gel Science and Technology / Ausgabe 2/2019
Print ISSN: 0928-0707
Elektronische ISSN: 1573-4846
DOI
https://doi.org/10.1007/s10971-018-4902-9

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