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Erschienen in: Journal of Sol-Gel Science and Technology 3/2020

18.01.2020 | Original Paper: Sol–gel and hybrid materials with surface modification for applications

Flame-retardant and water-repellent coating on cotton fabric by titania–boron sol–gel method

verfasst von: Aziz Bentis, Aicha Boukhriss, Said Gmouh

Erschienen in: Journal of Sol-Gel Science and Technology | Ausgabe 3/2020

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Abstract

This work aims to prepare a series of sols based on Titanium (IV) butoxide (TBT) and using boric acid as a functional additive. The sols were applied onto the cotton fabric by the pad-pry-cure process. The as-obtained cotton fabrics were characterized using Fourier-transform infrared (FTIR) spectroscopy and scanning electron microscopy (SEM) analysis in order to determine their chemical composition and their surface morphology, respectively. The results indicate the formation of TiO2–boron-based coating over the surface of coated cotton fabric. X-ray diffraction (XRD) patterns showed that the coating did not affect the crystallographic structure of the cellulosic fabric. The functional properties of the treated samples were measured from thermo-oxidative stability and burning behavior performance, drop absorption and water uptake measurements. The results showed that the coated cotton fabrics by the sol–gel approach through the application of TiO2–boron-based coating with 2.5 molar ratio of boric acid possessed high thermal stability and flame retardancy. Most importantly, a total burning time of 2 s and a residue of more than 90% were obtained after 10 s of flame application, indicating that the functionalized cotton fabric self-extinguished the fire rapidly. The water-repellent properties were also enhanced and the obtained results mentioned that the drop time and the water uptake were improved compared with untreated cotton fabric. The effect of the application of TiO2–boron-based coatings on the mechanical properties of cotton samples, as well as their washing fastness were studied.

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Metadaten
Titel
Flame-retardant and water-repellent coating on cotton fabric by titania–boron sol–gel method
verfasst von
Aziz Bentis
Aicha Boukhriss
Said Gmouh
Publikationsdatum
18.01.2020
Verlag
Springer US
Erschienen in
Journal of Sol-Gel Science and Technology / Ausgabe 3/2020
Print ISSN: 0928-0707
Elektronische ISSN: 1573-4846
DOI
https://doi.org/10.1007/s10971-020-05224-z

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