Skip to main content
Erschienen in: Physics of Metals and Metallography 10/2018

01.10.2018 | STRUCTURE, PHASE TRANSFORMATIONS, AND DIFFUSION

Structure and Microtexture of Niobium Recrystallized after Cryogenic Deformation by Shear under Pressure

verfasst von: L. M. Voronova, T. I. Chashchukhina, M. V. Degtyarev

Erschienen in: Physics of Metals and Metallography | Ausgabe 10/2018

Einloggen

Aktivieren Sie unsere intelligente Suche, um passende Fachinhalte oder Patente zu finden.

search-config
loading …

Abstract

Annealing of the submicrocrystalline (SMC) structure of niobium obtained by high pressure torsion to e = 7 at the temperature of liquid nitrogen was carried out. The influence of the annealing temperature in the range of 100–1100°C on the recrystallization of the SMC structure and the formation of texture was investigated. This paper discusses the role of static recovery and thermoactivated formation of recrystallization nuclei. The submicrograined recrystallized structure characterized by an average grain size of 0.8 μm, by a high homogeneity, and by the lack of the texture has been obtained. The sharpest recrystallization texture is formed as a result of annealing at 900°C; the average grain size is 10 μm in this case.

Sie haben noch keine Lizenz? Dann Informieren Sie sich jetzt über unsere Produkte:

Springer Professional "Wirtschaft+Technik"

Online-Abonnement

Mit Springer Professional "Wirtschaft+Technik" erhalten Sie Zugriff auf:

  • über 102.000 Bücher
  • über 537 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Finance + Banking
  • Management + Führung
  • Marketing + Vertrieb
  • Maschinenbau + Werkstoffe
  • Versicherung + Risiko

Jetzt Wissensvorsprung sichern!

Springer Professional "Wirtschaft"

Online-Abonnement

Mit Springer Professional "Wirtschaft" erhalten Sie Zugriff auf:

  • über 67.000 Bücher
  • über 340 Zeitschriften

aus folgenden Fachgebieten:

  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Finance + Banking
  • Management + Führung
  • Marketing + Vertrieb
  • Versicherung + Risiko




Jetzt Wissensvorsprung sichern!

Springer Professional "Technik"

Online-Abonnement

Mit Springer Professional "Technik" erhalten Sie Zugriff auf:

  • über 67.000 Bücher
  • über 390 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Maschinenbau + Werkstoffe




 

Jetzt Wissensvorsprung sichern!

Literatur
1.
Zurück zum Zitat V. V. Popov, E. N. Popova, A. V. Stolbovskii, V. P. Pilyugin, and N. K. Arkhipova, “Nanostructurization of Nb by high-pressure torsion in liquid nitrogen and the thermal stability of the structure obtained,” Phys. Met. Metallogr. 113, 295–301 (2012).CrossRef V. V. Popov, E. N. Popova, A. V. Stolbovskii, V. P. Pilyugin, and N. K. Arkhipova, “Nanostructurization of Nb by high-pressure torsion in liquid nitrogen and the thermal stability of the structure obtained,” Phys. Met. Metallogr. 113, 295–301 (2012).CrossRef
2.
Zurück zum Zitat V. V. Popov, E. N. Popova, V. P. Pilyugin, D. D. Kuznetsov, and A. V. Stolbovsky, “Nanostructuring of pure metals by severe plastic deformation at cryogenic temperatures,” IOP Conference on Materials Science and Engineering, 63, 012096 (2014). V. V. Popov, E. N. Popova, V. P. Pilyugin, D. D. Kuznetsov, and A. V. Stolbovsky, “Nanostructuring of pure metals by severe plastic deformation at cryogenic temperatures,” IOP Conference on Materials Science and Engineering, 63, 012096 (2014).
3.
Zurück zum Zitat G. S. D’yakonov, S. V. Zherebtsov, M. V. Klimova, and G. A. Salishchev, “Microstructure evolution of commercial-purity titanium during cryorolling,” Phys. Met. Metallogr. 116, 182–188 (2015).CrossRef G. S. D’yakonov, S. V. Zherebtsov, M. V. Klimova, and G. A. Salishchev, “Microstructure evolution of commercial-purity titanium during cryorolling,” Phys. Met. Metallogr. 116, 182–188 (2015).CrossRef
4.
Zurück zum Zitat V. P. Pilyugin, L. M. Voronova, M. V. Degtyarev, T. I. Chashchukhina, V. B. Vykhodets, and T. E. Kurennykh, “Structure evolution of pure iron upon low-temperature deformation under high pressure,” Phys. Met. Metallogr. 110, 564–573 (2010).CrossRef V. P. Pilyugin, L. M. Voronova, M. V. Degtyarev, T. I. Chashchukhina, V. B. Vykhodets, and T. E. Kurennykh, “Structure evolution of pure iron upon low-temperature deformation under high pressure,” Phys. Met. Metallogr. 110, 564–573 (2010).CrossRef
5.
Zurück zum Zitat M. A. Meyers, O. Vohringer, and V. A. Lubarda, “The onset of twinning in metals: A constitutive description,” Acta Mater. 49, 4025–4039 (2001).CrossRef M. A. Meyers, O. Vohringer, and V. A. Lubarda, “The onset of twinning in metals: A constitutive description,” Acta Mater. 49, 4025–4039 (2001).CrossRef
6.
Zurück zum Zitat Y. T. Zhu, X. Z. Liao, and X. L. Wu, “Deformation twinning in nanocrystalline materials,” Prog. Mater. Sci. 57, 1–62 (2012).CrossRef Y. T. Zhu, X. Z. Liao, and X. L. Wu, “Deformation twinning in nanocrystalline materials,” Prog. Mater. Sci. 57, 1–62 (2012).CrossRef
7.
Zurück zum Zitat T. M. Gapontseva, M. V. Degtyarev, V. P. Pilyugin, T. I. Chashchukhina, L. M. Voronova, and A. M. Patselov, “Effect of temperature of HPT deformation and the initial orientation on the structural evolution in single-crystal niobium,” Phys. Met. Metallogr. 117, 336–347 (2016).CrossRef T. M. Gapontseva, M. V. Degtyarev, V. P. Pilyugin, T. I. Chashchukhina, L. M. Voronova, and A. M. Patselov, “Effect of temperature of HPT deformation and the initial orientation on the structural evolution in single-crystal niobium,” Phys. Met. Metallogr. 117, 336–347 (2016).CrossRef
8.
Zurück zum Zitat N. A. Smirnova, V. I. Levit, V. P. Pilyugin, R. I. Kuznetsov, and M. V. Degtyarev, “Peculiarities of low-temperature recrystallization of nickel and copper,” Phys. Met. Metallogr. 62 (3), 140–144 (1986). N. A. Smirnova, V. I. Levit, V. P. Pilyugin, R. I. Kuznetsov, and M. V. Degtyarev, “Peculiarities of low-temperature recrystallization of nickel and copper,” Phys. Met. Metallogr. 62 (3), 140–144 (1986).
9.
Zurück zum Zitat M. V. Degtyarev, L. M. Voronova, T. I. Chashchukhina, D. V. Shinyavskii and V. I. Levit, “Recrystallization of submicrocrystalline niobium upon heating above and below the temperature of thermally activated nucleation,” Phys. Met. Metallogr. 117, 1111–1118 (2016).CrossRef M. V. Degtyarev, L. M. Voronova, T. I. Chashchukhina, D. V. Shinyavskii and V. I. Levit, “Recrystallization of submicrocrystalline niobium upon heating above and below the temperature of thermally activated nucleation,” Phys. Met. Metallogr. 117, 1111–1118 (2016).CrossRef
10.
Zurück zum Zitat H. H. Bernardi, H. R. Z. Sandim, K. D. Zilnyk, B. Verlinden, and D. Raabe, “Microstructural stability of a niobium single crystal deformed by equal channel angular pressing,” Mater. Res. 20, 1238–1247 (2017).CrossRef H. H. Bernardi, H. R. Z. Sandim, K. D. Zilnyk, B. Verlinden, and D. Raabe, “Microstructural stability of a niobium single crystal deformed by equal channel angular pressing,” Mater. Res. 20, 1238–1247 (2017).CrossRef
11.
Zurück zum Zitat Y. Yamaguchi, H. Doryo, M. Yuasa, H. Miyamoto, and M. Yamanaka, “Deformation and recrystallization behavior of super highpurity niobium for SRF cavity,” IOP Conf. Ser.: Mater. Sci. Eng. 194, 012029 (2017). Y. Yamaguchi, H. Doryo, M. Yuasa, H. Miyamoto, and M. Yamanaka, “Deformation and recrystallization behavior of super highpurity niobium for SRF cavity,” IOP Conf. Ser.: Mater. Sci. Eng. 194, 012029 (2017).
12.
Zurück zum Zitat L. M. Voronova, M. V. Degtyarev, T. I. Chashchukhina, D. V. Shinyavskii, and T. M. Gapontseva, “Effect of microcrystallites formed by deformation on the growth and orientation of grains during recrystallization of iron,” J. Mater. Sci. Lett. 7, 359–362 (2017). L. M. Voronova, M. V. Degtyarev, T. I. Chashchukhina, D. V. Shinyavskii, and T. M. Gapontseva, “Effect of microcrystallites formed by deformation on the growth and orientation of grains during recrystallization of iron,” J. Mater. Sci. Lett. 7, 359–362 (2017).
13.
Zurück zum Zitat L. M. Voronova, T. I. Chashchukhina, and M. V. Degtyarev, “Texture of recrystallization upon annealing of niobium with a sub-microcrystalline structure,” Phys. Met. Metallogr. 119 (2018) (in press). L. M. Voronova, T. I. Chashchukhina, and M. V. Degtyarev, “Texture of recrystallization upon annealing of niobium with a sub-microcrystalline structure,” Phys. Met. Metallogr. 119 (2018) (in press).
14.
Zurück zum Zitat M. V. Degtyarev, T. I. Chashchukhina, L. M. Voronova, A. M. Patselov, and V. P. Pilyugin, “Influence of the relaxation processes on the structure formation in pure metals and alloys under high-pressure deformation,” Acta Mater. 55, 6039–6050 (2007).CrossRef M. V. Degtyarev, T. I. Chashchukhina, L. M. Voronova, A. M. Patselov, and V. P. Pilyugin, “Influence of the relaxation processes on the structure formation in pure metals and alloys under high-pressure deformation,” Acta Mater. 55, 6039–6050 (2007).CrossRef
15.
Zurück zum Zitat V. N. Danilenko, S. Yu. Mironov, A. N. Belyakov, and A. P. Zhilyaev, “Application of EBSD analysis in physical materials science (review),” Zavod. Lab., Diagn. Mater. 78 (2), 28–46 (2012). V. N. Danilenko, S. Yu. Mironov, A. N. Belyakov, and A. P. Zhilyaev, “Application of EBSD analysis in physical materials science (review),” Zavod. Lab., Diagn. Mater. 78 (2), 28–46 (2012).
16.
Zurück zum Zitat F. J. Humphreys, “Quantitative metallography by electron backscattered diffraction,” J. Microsc. 195, 170–185 (1999).CrossRef F. J. Humphreys, “Quantitative metallography by electron backscattered diffraction,” J. Microsc. 195, 170–185 (1999).CrossRef
Metadaten
Titel
Structure and Microtexture of Niobium Recrystallized after Cryogenic Deformation by Shear under Pressure
verfasst von
L. M. Voronova
T. I. Chashchukhina
M. V. Degtyarev
Publikationsdatum
01.10.2018
Verlag
Pleiades Publishing
Erschienen in
Physics of Metals and Metallography / Ausgabe 10/2018
Print ISSN: 0031-918X
Elektronische ISSN: 1555-6190
DOI
https://doi.org/10.1134/S0031918X18100137

Weitere Artikel der Ausgabe 10/2018

Physics of Metals and Metallography 10/2018 Zur Ausgabe