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Erschienen in: Journal of Nanoparticle Research 7/2022

01.07.2022 | Research paper

Magnesium oxide nanofabrication from magnesium chloride salt by thermal plasma method: effects of quenching and concentration

verfasst von: Pedram Nasiri, Shahrooz Saviz, Davoud Dorranian, Amir Hossein Sari

Erschienen in: Journal of Nanoparticle Research | Ausgabe 7/2022

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Abstract

Fabrication of magnesium oxide nanostructures from aqueous solution of magnesium chloride salt, by thermal plasma method, has been investigated and effects of cooling temperature as well as concentration of salt in the aqueous solution on the properties of synthesized nanostructures were studied experimentally. Three mechanisms of cooling include cooling with atmospheric air, argon flow in opposite directions, and water were examined to produce magnesium oxide nanoparticles at two concentrations of raw material. Results show that in any case, 95% purity rod shape and spherical magnesium oxide nanostructures may be produced by thermal plasma method. Cooling mechanism is a powerful tool to control the morphology of synthesized nanostructure. Furthermore, it was observed that sizes of nanostructures were decreased with decreasing the concentration of injected materials.

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Literatur
1.
Zurück zum Zitat Susanto SA, Yunarti RT, Widjaya RR, Maryati Y, Dwiatmoko AA, Aulia F, Rinaldi N (2021) Catalytic conversion of ethanol to butanol over magnesium oxide catalysts. IOP Conf Ser Mater Sci Eng 1011(1):012028CrossRef Susanto SA, Yunarti RT, Widjaya RR, Maryati Y, Dwiatmoko AA, Aulia F, Rinaldi N (2021) Catalytic conversion of ethanol to butanol over magnesium oxide catalysts. IOP Conf Ser Mater Sci Eng 1011(1):012028CrossRef
2.
Zurück zum Zitat Shen X, Nie X, Hu H (2014) Thermal conductivities of nanostructured magnesium oxide coatings deposited on magnesium alloys by plasma electrolytic oxidation. J Nanosci Nanotechnol 14(10):7933–7937CrossRef Shen X, Nie X, Hu H (2014) Thermal conductivities of nanostructured magnesium oxide coatings deposited on magnesium alloys by plasma electrolytic oxidation. J Nanosci Nanotechnol 14(10):7933–7937CrossRef
3.
Zurück zum Zitat Epstein JA (1976) Utilization of the Dead Sea minerals (a review). Hydrometallurgy 2(1):1–10CrossRef Epstein JA (1976) Utilization of the Dead Sea minerals (a review). Hydrometallurgy 2(1):1–10CrossRef
4.
Zurück zum Zitat Wang J, Li Z (2012) Crystallization and agglomeration kinetics of hydromagnesite in the reactive system MgCl2–Na2CO3–NaOH–H2O. Ind Eng Chem Res 51(23):7874–7883CrossRef Wang J, Li Z (2012) Crystallization and agglomeration kinetics of hydromagnesite in the reactive system MgCl2–Na2CO3–NaOH–H2O. Ind Eng Chem Res 51(23):7874–7883CrossRef
5.
Zurück zum Zitat Wahab R, Ansari SG, Dar MA, Kim YS, Shin HS (2007) Synthesis of magnesium oxide nanoparticles by sol-gel process. Mater Sci Forum 558:983–986CrossRef Wahab R, Ansari SG, Dar MA, Kim YS, Shin HS (2007) Synthesis of magnesium oxide nanoparticles by sol-gel process. Mater Sci Forum 558:983–986CrossRef
6.
Zurück zum Zitat Rao KG, Ashok CH, Rao KV, Chakra CS (2014) Structural properties of MgO nanoparticles: synthesized by co-precipitation technique. Int J Sci Res 3(12):43–46 Rao KG, Ashok CH, Rao KV, Chakra CS (2014) Structural properties of MgO nanoparticles: synthesized by co-precipitation technique. Int J Sci Res 3(12):43–46
7.
Zurück zum Zitat Cui H, Wu X, Chen Y, Boughton RI (2014) Synthesis and characterization of mesoporous MgO by template-free hydrothermal method. Mater Res Bull 50:307–311CrossRef Cui H, Wu X, Chen Y, Boughton RI (2014) Synthesis and characterization of mesoporous MgO by template-free hydrothermal method. Mater Res Bull 50:307–311CrossRef
8.
Zurück zum Zitat Pereira H, Moura CG, Miranda G, Silva FS (2021) Influence of liquid media and laser energy on the production of MgO nanoparticles by laser ablation. Opt Laser Technol 142:107181CrossRef Pereira H, Moura CG, Miranda G, Silva FS (2021) Influence of liquid media and laser energy on the production of MgO nanoparticles by laser ablation. Opt Laser Technol 142:107181CrossRef
9.
Zurück zum Zitat Tharani K, Christy AJ, Sagadevan S, Nehru LC (2021) Fabrication of Magnesium oxide nanoparticles using combustion method for a biological and environmental cause. Chem Phys Lett 763:138216CrossRef Tharani K, Christy AJ, Sagadevan S, Nehru LC (2021) Fabrication of Magnesium oxide nanoparticles using combustion method for a biological and environmental cause. Chem Phys Lett 763:138216CrossRef
10.
Zurück zum Zitat Liu WJ, Jiang H, Tian K, Ding YW, Yu HQ (2013) Mesoporous carbon stabilized MgO nanoparticles synthesized by pyrolysis of MgCl2 preloaded waste biomass for highly efficient CO2 capture. Environ Sci Technol 47(16):9397–9403CrossRef Liu WJ, Jiang H, Tian K, Ding YW, Yu HQ (2013) Mesoporous carbon stabilized MgO nanoparticles synthesized by pyrolysis of MgCl2 preloaded waste biomass for highly efficient CO2 capture. Environ Sci Technol 47(16):9397–9403CrossRef
11.
Zurück zum Zitat Heimann RB (2008) Plasma-spray coating: principles and applications. Wiley, New York Heimann RB (2008) Plasma-spray coating: principles and applications. Wiley, New York
12.
Zurück zum Zitat Byun Y, Namkung W, Cho M, Chung JW, Kim YS, Lee JH, Lee CR, Hwang SM (2010) Demonstration of thermal plasma gasification/vitrification for municipal solid waste treatment. Environ Sci Technol 44(17):6680–6684CrossRef Byun Y, Namkung W, Cho M, Chung JW, Kim YS, Lee JH, Lee CR, Hwang SM (2010) Demonstration of thermal plasma gasification/vitrification for municipal solid waste treatment. Environ Sci Technol 44(17):6680–6684CrossRef
13.
Zurück zum Zitat Khandanjou S, Ghoranneviss M, Saviz S, Afshar MR (2018) Influences of substrate temperature on microstructure and corrosion behavior of APS Ni50Ti25Al25 inter-metallic coating. Chin Phys B 27(2):028104CrossRef Khandanjou S, Ghoranneviss M, Saviz S, Afshar MR (2018) Influences of substrate temperature on microstructure and corrosion behavior of APS Ni50Ti25Al25 inter-metallic coating. Chin Phys B 27(2):028104CrossRef
14.
Zurück zum Zitat Hessel V, Cravotto G, Fitzpatrick P, Patil BS, Lang J, Bonrath W (2013) Industrial applications of plasma, microwave and ultrasound techniques: nitrogen-fixation and hydrogenation reactions. Chem Eng Process 71:19–30CrossRef Hessel V, Cravotto G, Fitzpatrick P, Patil BS, Lang J, Bonrath W (2013) Industrial applications of plasma, microwave and ultrasound techniques: nitrogen-fixation and hydrogenation reactions. Chem Eng Process 71:19–30CrossRef
15.
Zurück zum Zitat Shigeta M, Murphy AB (2011) Thermal plasmas for nanofabrication. J Phys D Appl Phys 44(17):174025CrossRef Shigeta M, Murphy AB (2011) Thermal plasmas for nanofabrication. J Phys D Appl Phys 44(17):174025CrossRef
16.
Zurück zum Zitat Li M, Wang X, Li H, Di H, Wu X, Fang C, Yang B (2013) Preparation of photoluminescent single crystalline MgO nanobelts by DC arc plasma jet CVD. Appl Surf Sci 274:188–194CrossRef Li M, Wang X, Li H, Di H, Wu X, Fang C, Yang B (2013) Preparation of photoluminescent single crystalline MgO nanobelts by DC arc plasma jet CVD. Appl Surf Sci 274:188–194CrossRef
17.
Zurück zum Zitat Zhang H, Cao T, Cheng Y (2014) Synthesis of nanostructured MgO powders with photoluminescence by plasma-intensified pyrohydrolysis process of bischofite from brine. Green Proc Synth 3(3):215–222 CrossRef Zhang H, Cao T, Cheng Y (2014) Synthesis of nanostructured MgO powders with photoluminescence by plasma-intensified pyrohydrolysis process of bischofite from brine. Green Proc Synth 3(3):215–222 CrossRef
18.
Zurück zum Zitat Sirota V, Selemenev V, Kovaleva M, Pavlenko I, Mamunin K, Dokalov V, Prozorova M (2016) Synthesis of magnesium oxide nanopowder by thermal plasma using magnesium nitrate hexahydrate. Phys Res Int 2016:1–4CrossRef Sirota V, Selemenev V, Kovaleva M, Pavlenko I, Mamunin K, Dokalov V, Prozorova M (2016) Synthesis of magnesium oxide nanopowder by thermal plasma using magnesium nitrate hexahydrate. Phys Res Int 2016:1–4CrossRef
19.
Zurück zum Zitat Dash S, Sahoo RK, Singh SK, Chauhan DS (2018) Synthesis of magnesium oxide nanopowder via plasma processing route. Int J Nano Biomater 7(3):210–218CrossRef Dash S, Sahoo RK, Singh SK, Chauhan DS (2018) Synthesis of magnesium oxide nanopowder via plasma processing route. Int J Nano Biomater 7(3):210–218CrossRef
20.
Zurück zum Zitat Yoshida T, Kawasaki A, Nakagawa K, Akashi K (1979) The synthesis of ultrafine titanium nitride in an rf plasma. J Mater Sci 14(7):1624–1630CrossRef Yoshida T, Kawasaki A, Nakagawa K, Akashi K (1979) The synthesis of ultrafine titanium nitride in an rf plasma. J Mater Sci 14(7):1624–1630CrossRef
21.
Zurück zum Zitat Yoshida T, Akashi K (1981) Preparation of ultrafine iron particles using an RF plasma. Trans Japan Instit Metals 22(6):371–378CrossRef Yoshida T, Akashi K (1981) Preparation of ultrafine iron particles using an RF plasma. Trans Japan Instit Metals 22(6):371–378CrossRef
22.
Zurück zum Zitat Lee HJ, Eguchi K, Yoshida T (1990) Preparation of ultrafine silicon nitride, and silicon nitride and silicon carbide mixed powders in a hybrid plasma. J Am Ceram Soc 73(11):3356–3362CrossRef Lee HJ, Eguchi K, Yoshida T (1990) Preparation of ultrafine silicon nitride, and silicon nitride and silicon carbide mixed powders in a hybrid plasma. J Am Ceram Soc 73(11):3356–3362CrossRef
23.
Zurück zum Zitat Ostrikov K, Murphy AB (2007) Plasma-aided nanofabrication: where is the cutting edge? J Phys D Appl Phys 40(8):2223CrossRef Ostrikov K, Murphy AB (2007) Plasma-aided nanofabrication: where is the cutting edge? J Phys D Appl Phys 40(8):2223CrossRef
24.
Zurück zum Zitat Li JG, Kamiyama H, Wang XH, Moriyoshi Y, Ishigaki T (2006) TiO2 nanopowders via radio-frequency thermal plasma oxidation of organic liquid precursors: synthesis and characterization. J Eur Ceram Soc 26(4–5):423–428CrossRef Li JG, Kamiyama H, Wang XH, Moriyoshi Y, Ishigaki T (2006) TiO2 nanopowders via radio-frequency thermal plasma oxidation of organic liquid precursors: synthesis and characterization. J Eur Ceram Soc 26(4–5):423–428CrossRef
25.
Zurück zum Zitat Gupta A, Swihart MT, Wiggers H (2009) Luminescent colloidal dispersion of silicon quantum dots from microwave plasma synthesis: exploring the photoluminescence behavior across the visible spectrum. Adv Func Mater 19(5):696–703CrossRef Gupta A, Swihart MT, Wiggers H (2009) Luminescent colloidal dispersion of silicon quantum dots from microwave plasma synthesis: exploring the photoluminescence behavior across the visible spectrum. Adv Func Mater 19(5):696–703CrossRef
26.
Zurück zum Zitat Jiayin G, Xiaobao F, Dolbec R, Siwen X, Jurewicz J, Boulos M (2010) Development of nanopowder synthesis using induction plasma. Plasma Sci Technol 12(2):188CrossRef Jiayin G, Xiaobao F, Dolbec R, Siwen X, Jurewicz J, Boulos M (2010) Development of nanopowder synthesis using induction plasma. Plasma Sci Technol 12(2):188CrossRef
27.
Zurück zum Zitat Shomate CH, Huffman EH (1943) Heats of formation of MgO, MgCl2, MgCl2· H2O, MgCl2· 2H2O, MgCl2· 4H2O, and MgCl2· 6H2O1. J Am Chem Soc 65(8):1625–1629CrossRef Shomate CH, Huffman EH (1943) Heats of formation of MgO, MgCl2, MgCl2· H2O, MgCl2· 2H2O, MgCl2· 4H2O, and MgCl2· 6H2O1. J Am Chem Soc 65(8):1625–1629CrossRef
Metadaten
Titel
Magnesium oxide nanofabrication from magnesium chloride salt by thermal plasma method: effects of quenching and concentration
verfasst von
Pedram Nasiri
Shahrooz Saviz
Davoud Dorranian
Amir Hossein Sari
Publikationsdatum
01.07.2022
Verlag
Springer Netherlands
Erschienen in
Journal of Nanoparticle Research / Ausgabe 7/2022
Print ISSN: 1388-0764
Elektronische ISSN: 1572-896X
DOI
https://doi.org/10.1007/s11051-022-05533-0

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