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2020 | OriginalPaper | Buchkapitel

14. Recent Advances in Micro-extraction Based Analytical Approaches for Pesticides Analysis in Environmental Samples

verfasst von : Anshuman Srivastava, Minu Singh, Shiv Singh, Sheelendra Pratap Singh

Erschienen in: Measurement, Analysis and Remediation of Environmental Pollutants

Verlag: Springer Singapore

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Abstract

Pesticides are auxiliary input to induce the quality and production of food. It is also considerate to minimize the postharvest losses of crops and to fulfill the increasing demand. Although pesticides are useful in food production, their versatile use had resulted in the occurrence of contamination and residues in all necessities of our life, i.e., food, water, and air. Nowadays, consumer perception about food safety and quality leads to transparency and traceability in various agricultural practices. The pesticide had a diverse meaning, it encompasses many hundreds of toxic chemicals, exhibiting enormously diverse chemical and physical properties. Thus to determine the level of pesticide residue in different commodities, a simple, effective and robust sample preparation and analytical determination technique is required. Further, technique includes both identification and quantification of analytes in food commodities, which strictly fulfill the international regulation on maximum residue limits. This chapter briefly discusses the modern analytical approaches, including different sample preparation technique followed by chromatography and mass spectrometry techniques.

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Literatur
Zurück zum Zitat Anastassiades M, Lehotay SJ, Štajnbaher D, Schenck FJ (2003a) Fast and easy multiresidue method employing acetonitrile extraction/partitioning and “dispersive solid-phase extraction” for the determination of pesticide residues in produce. J AOAC Int 86(2):412–431 Anastassiades M, Lehotay SJ, Štajnbaher D, Schenck FJ (2003a) Fast and easy multiresidue method employing acetonitrile extraction/partitioning and “dispersive solid-phase extraction” for the determination of pesticide residues in produce. J AOAC Int 86(2):412–431
Zurück zum Zitat Anastassiades M, Lehotay S, štajnbaher D, Schenck F (2003) Fast and easy multiresidue method employing acetonitrile extraction/partitioning and “dispersive solid-phase extraction” for the determination of pesticide residues in produce, vol 86 Anastassiades M, Lehotay S, štajnbaher D, Schenck F (2003) Fast and easy multiresidue method employing acetonitrile extraction/partitioning and “dispersive solid-phase extraction” for the determination of pesticide residues in produce, vol 86
Zurück zum Zitat Barriada-Pereira M, Concha-Graña E, González-Castro MJ, Muniategui-Lorenzo S, López-Mahı́a P, Prada-Rodrı́guez D, Fernández-Fernández E (2003) Microwave-assisted extraction versus Soxhlet extraction in the analysis of 21 organochlorine pesticides in plants. J Chromatogr A 1008(1):115–122. https://doi.org/10.1016/S0021-9673(03)01061-6CrossRef Barriada-Pereira M, Concha-Graña E, González-Castro MJ, Muniategui-Lorenzo S, López-Mahı́a P, Prada-Rodrı́guez D, Fernández-Fernández E (2003) Microwave-assisted extraction versus Soxhlet extraction in the analysis of 21 organochlorine pesticides in plants. J Chromatogr A 1008(1):115–122. https://​doi.​org/​10.​1016/​S0021-9673(03)01061-6CrossRef
Zurück zum Zitat Codex Alimentarius. Accessed on July 2012 Codex Alimentarius. Accessed on July 2012
Zurück zum Zitat de la Guardia M, Garrigues S (2012) Handbook of green analytical chemistry. Wiley, ChichesterCrossRef de la Guardia M, Garrigues S (2012) Handbook of green analytical chemistry. Wiley, ChichesterCrossRef
Zurück zum Zitat Farajzadeh MA, Mogaddam MRA (2012) Air-assisted liquid–liquid microextraction method as a novel microextraction technique; application in extraction and preconcentration of phthalate esters in aqueous sample followed by gas chromatography–flame ionization detection. Anal Chim Acta 728:31–38. https://doi.org/10.1016/j.aca.2012.03.031CrossRef Farajzadeh MA, Mogaddam MRA (2012) Air-assisted liquid–liquid microextraction method as a novel microextraction technique; application in extraction and preconcentration of phthalate esters in aqueous sample followed by gas chromatography–flame ionization detection. Anal Chim Acta 728:31–38. https://​doi.​org/​10.​1016/​j.​aca.​2012.​03.​031CrossRef
Zurück zum Zitat Farajzadeh M, Feriduni B, Afshar mogaddam M (2015) Development of a new extraction method based on counter current salting-out homogenous liquid–liquid extraction followed by dispersive liquid–liquid microextraction: application for the extraction and preconcentration of widely used pesticides from fruit juices, vol 367. https://doi.org/10.1016/j.talanta.2015.06.024CrossRef Farajzadeh M, Feriduni B, Afshar mogaddam M (2015) Development of a new extraction method based on counter current salting-out homogenous liquid–liquid extraction followed by dispersive liquid–liquid microextraction: application for the extraction and preconcentration of widely used pesticides from fruit juices, vol 367. https://​doi.​org/​10.​1016/​j.​talanta.​2015.​06.​024CrossRef
Zurück zum Zitat Farajzadeh MA, Feriduni B, Afshar Mogaddam MR (2016) Development of a new extraction method based on counter current salting-out homogenous liquid–liquid extraction followed by dispersive liquid–liquid microextraction: Application for the extraction and preconcentration of widely used pesticides from fruit juices. Talanta 146:772–779. https://doi.org/10.1016/j.talanta.2015.06.024CrossRef Farajzadeh MA, Feriduni B, Afshar Mogaddam MR (2016) Development of a new extraction method based on counter current salting-out homogenous liquid–liquid extraction followed by dispersive liquid–liquid microextraction: Application for the extraction and preconcentration of widely used pesticides from fruit juices. Talanta 146:772–779. https://​doi.​org/​10.​1016/​j.​talanta.​2015.​06.​024CrossRef
Zurück zum Zitat Fatoki OS, Awofolu RO (2003) Methods for selective determination of persistent organochlorine pesticide residues in water and sediments by capillary gas chromatography and electron-capture detection. J Chromatogr A 983(1–2):225–236CrossRef Fatoki OS, Awofolu RO (2003) Methods for selective determination of persistent organochlorine pesticide residues in water and sediments by capillary gas chromatography and electron-capture detection. J Chromatogr A 983(1–2):225–236CrossRef
Zurück zum Zitat González-Curbelo M, Socas-Rodríguez B, Herrera-Herrera A, González-Sálamo J, Hernández-Borges J, Rodríguez-Delgado M (2015) Evolution and applications of the QuEChERS method. TrAC Trends Anal Chem 71:169–185CrossRef González-Curbelo M, Socas-Rodríguez B, Herrera-Herrera A, González-Sálamo J, Hernández-Borges J, Rodríguez-Delgado M (2015) Evolution and applications of the QuEChERS method. TrAC Trends Anal Chem 71:169–185CrossRef
Zurück zum Zitat Gonzalez-Rodriguez RM, Cancho-Grande B, Simal-Gandara J (2009) Multiresidue determination of 11 new fungicides in grapes and wines by liquid-liquid extraction/clean-up and programmable temperature vaporization injection with analyte protectants/gas chromatography/ion trap mass spectrometry. J Chromatogr A 1216(32):6033–6042. https://doi.org/10.1016/j.chroma.2009.06.046CrossRef Gonzalez-Rodriguez RM, Cancho-Grande B, Simal-Gandara J (2009) Multiresidue determination of 11 new fungicides in grapes and wines by liquid-liquid extraction/clean-up and programmable temperature vaporization injection with analyte protectants/gas chromatography/ion trap mass spectrometry. J Chromatogr A 1216(32):6033–6042. https://​doi.​org/​10.​1016/​j.​chroma.​2009.​06.​046CrossRef
Zurück zum Zitat Jiang Y, Li X, Xu J, Pan C, Zhang J, Niu W (2009) Multiresidue method for the determination of 77 pesticides in wine using QuEChERS sample preparation and gas chromatography with mass spectrometry. Food Addit Contam Part A: Chem Anal Control Expo Risk Assess 26(6):859–866. https://doi.org/10.1080/02652030902822794CrossRef Jiang Y, Li X, Xu J, Pan C, Zhang J, Niu W (2009) Multiresidue method for the determination of 77 pesticides in wine using QuEChERS sample preparation and gas chromatography with mass spectrometry. Food Addit Contam Part A: Chem Anal Control Expo Risk Assess 26(6):859–866. https://​doi.​org/​10.​1080/​0265203090282279​4CrossRef
Zurück zum Zitat Kaczyński P, Łozowicka B (2017) One-step QuEChERS-based approach to extraction and cleanup in multiresidue analysis of sulfonylurea herbicides in cereals by liquid chromatography–tandem mass spectrometry. Food Anal Methods 10(1):147–160CrossRef Kaczyński P, Łozowicka B (2017) One-step QuEChERS-based approach to extraction and cleanup in multiresidue analysis of sulfonylurea herbicides in cereals by liquid chromatography–tandem mass spectrometry. Food Anal Methods 10(1):147–160CrossRef
Zurück zum Zitat Lee J, Kim L, Shin Y, Lee J, Lee J, Kim E, Moon J-K, Kim J-H (2017) Rapid and simultaneous analysis of 360 pesticides in brown rice, spinach, orange, and potato using microbore GC-MS/MS. J Agric Food Chem 65(16):3387–3395CrossRef Lee J, Kim L, Shin Y, Lee J, Lee J, Kim E, Moon J-K, Kim J-H (2017) Rapid and simultaneous analysis of 360 pesticides in brown rice, spinach, orange, and potato using microbore GC-MS/MS. J Agric Food Chem 65(16):3387–3395CrossRef
Zurück zum Zitat Luo Y-B, Zheng H-B, Jiang X-Y, Li X, Zhang H-F, Zhu F-P, Pang Y-Q, Feng Y-Q (2015) Determination of pesticide residues in tobacco using modified QuEChERS procedure coupled to on-line gel permeation chromatography-gas chromatography/tandem mass spectrometry. Chin J Anal Chem 43(10):1538–1544. https://doi.org/10.1016/S1872-2040(15)60870-2CrossRef Luo Y-B, Zheng H-B, Jiang X-Y, Li X, Zhang H-F, Zhu F-P, Pang Y-Q, Feng Y-Q (2015) Determination of pesticide residues in tobacco using modified QuEChERS procedure coupled to on-line gel permeation chromatography-gas chromatography/tandem mass spectrometry. Chin J Anal Chem 43(10):1538–1544. https://​doi.​org/​10.​1016/​S1872-2040(15)60870-2CrossRef
Zurück zum Zitat Pawliszyn J, Pedersen-Bjergaard S (2006) Analytical microextraction: current status and future trends. J Chromatogr Sci 44(6):291–307CrossRef Pawliszyn J, Pedersen-Bjergaard S (2006) Analytical microextraction: current status and future trends. J Chromatogr Sci 44(6):291–307CrossRef
Zurück zum Zitat Poole CF (2000) Solid-phase extraction, encyclopedia of separation science, vol 3. Academic Press, p 1405 Poole CF (2000) Solid-phase extraction, encyclopedia of separation science, vol 3. Academic Press, p 1405
Zurück zum Zitat Sharma BK (2006) Environmental chemistry. Goel Publication House, New Delhi Sharma BK (2006) Environmental chemistry. Goel Publication House, New Delhi
Zurück zum Zitat Specht W, Pelz S, Gilsbach W (1995) Gas-chromatographic determination of pesticide residues after clean-up by gel-permeation chromatography and mini-silica gel-column chromatography6. Communication(*): Replacement of dichloromethane by ethyl acetate/cyclohexane in liquid-liquid partition and simplified conditions for extraction and liquid-liquid partition, vol 353. https://doi.org/10.1007/s0021653530183CrossRef Specht W, Pelz S, Gilsbach W (1995) Gas-chromatographic determination of pesticide residues after clean-up by gel-permeation chromatography and mini-silica gel-column chromatography6. Communication(*): Replacement of dichloromethane by ethyl acetate/cyclohexane in liquid-liquid partition and simplified conditions for extraction and liquid-liquid partition, vol 353. https://​doi.​org/​10.​1007/​s0021653530183CrossRef
Zurück zum Zitat Stalling D, Tindle RC, Johnson JL (1972) Cleanup of pesticide and polychlorinated biphenyl residues in fish extracts by gel permeation chromatography, vol 55 Stalling D, Tindle RC, Johnson JL (1972) Cleanup of pesticide and polychlorinated biphenyl residues in fish extracts by gel permeation chromatography, vol 55
Zurück zum Zitat Wang P, Zhang Q, Wang Y, Wang T, Li X, Ding L, Jiang G (2010) Evaluation of Soxhlet extraction, accelerated solvent extraction and microwave-assisted extraction for the determination of polychlorinated biphenyls and polybrominated diphenyl ethers in soil and fish samples. Anal Chim Acta 663(1):43–48. https://doi.org/10.1016/j.aca.2010.01.035CrossRef Wang P, Zhang Q, Wang Y, Wang T, Li X, Ding L, Jiang G (2010) Evaluation of Soxhlet extraction, accelerated solvent extraction and microwave-assisted extraction for the determination of polychlorinated biphenyls and polybrominated diphenyl ethers in soil and fish samples. Anal Chim Acta 663(1):43–48. https://​doi.​org/​10.​1016/​j.​aca.​2010.​01.​035CrossRef
Zurück zum Zitat Zhang J, Rodila R, Gage E, Hautman M, Fan L, King LL, Wu H, El-Shourbagy TA (2010) High-throughput salting-out assisted liquid/liquid extraction with acetonitrile for the simultaneous determination of simvastatin and simvastatin acid in human plasma with liquid chromatography. Anal Chim Acta 661(2):167–172. https://doi.org/10.1016/j.aca.2009.12.023CrossRef Zhang J, Rodila R, Gage E, Hautman M, Fan L, King LL, Wu H, El-Shourbagy TA (2010) High-throughput salting-out assisted liquid/liquid extraction with acetonitrile for the simultaneous determination of simvastatin and simvastatin acid in human plasma with liquid chromatography. Anal Chim Acta 661(2):167–172. https://​doi.​org/​10.​1016/​j.​aca.​2009.​12.​023CrossRef
Zurück zum Zitat Zheng G, Han C, Liu Y, Wang J, Zhu M, Wang C, Shen Y (2014) Multiresidue analysis of 30 organochlorine pesticides in milk and milk powder by gel permeation chromatography-solid phase extraction-gas chromatography-tandem mass spectrometry. J Dairy Sci 97(10):6016–6026. https://doi.org/10.3168/jds.2014-8192CrossRef Zheng G, Han C, Liu Y, Wang J, Zhu M, Wang C, Shen Y (2014) Multiresidue analysis of 30 organochlorine pesticides in milk and milk powder by gel permeation chromatography-solid phase extraction-gas chromatography-tandem mass spectrometry. J Dairy Sci 97(10):6016–6026. https://​doi.​org/​10.​3168/​jds.​2014-8192CrossRef
Zurück zum Zitat Zheng W, Yoo K-H, Choi J-M, Park D-H, Kim S-K, Kang Y-S, El-Aty AA, Hacımüftüoğlu A, Jeong JH, Bekhit AE-D (2019) A modified QuEChERS method coupled with liquid chromatography-tandem mass spectrometry for the simultaneous detection and quantification of scopolamine, L-hyoscyamine, and sparteine residues in animal-derived food products. J Adv Res 15:95–102CrossRef Zheng W, Yoo K-H, Choi J-M, Park D-H, Kim S-K, Kang Y-S, El-Aty AA, Hacımüftüoğlu A, Jeong JH, Bekhit AE-D (2019) A modified QuEChERS method coupled with liquid chromatography-tandem mass spectrometry for the simultaneous detection and quantification of scopolamine, L-hyoscyamine, and sparteine residues in animal-derived food products. J Adv Res 15:95–102CrossRef
Metadaten
Titel
Recent Advances in Micro-extraction Based Analytical Approaches for Pesticides Analysis in Environmental Samples
verfasst von
Anshuman Srivastava
Minu Singh
Shiv Singh
Sheelendra Pratap Singh
Copyright-Jahr
2020
Verlag
Springer Singapore
DOI
https://doi.org/10.1007/978-981-15-0540-9_14