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Historischer Abriss zur Entstehung und Entwicklung der Chemischen Reaktionstechnik Kapitel lesen Erstes Kapitel lesen

2020 | OriginalPaper | Buchkapitel

37. Spezielle labortechnische Reaktoren: Hochdurchsatz-Reaktionstechnik

verfasst von : Klaus Stöwe

Erschienen in: Handbuch Chemische Reaktoren

Verlag: Springer Berlin Heidelberg

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Zusammenfassung

In diesem Kapitel des Handbuchs Chemischer Reaktoren werden Ansätze zur Parallelisierung von Reaktoren mit dem Ziel der Erhöhung der Effizienz der Testverfahren, Reduktion des zeitlichen und finanziellen Aufwandes für die Testung, die Erhöhung der Reproduzierbarkeit der Ergebnisse und Wissensgenerierung beschrieben. Wie jedes experimentelle Vorgehen bedarf auch die Hochdurchsatz-Experimentation einer sehr sorgfältigen Planung der Versuche im Sinne eines Design of Experiment (DoE). Im Hochdurchsatz-Workflow werden anschließend die Phasen Primär- und Sekundärscreening solange durchlaufen, bis ein entsprechendes Entwicklungsziel erreicht worden ist. Parallelisiert werden können praktisch alle konventionellen Reaktortypen. Oberster Grundsatz bei der Planung und Entwicklung von Multireaktorsystemen ist ein völlig gleichartiges Verhalten aller Reaktoren des Parallelsystems, damit eine Vergleichbarkeit der Ergebnisse gegeben ist. Im Stadium der Realisierung eines Parallelisierungskonzeptes muss daher das Reaktorsystem immer gegen konventionelle Anlagen validiert werden. Vorgestellt werden Beispiele für Parallelreaktorkonzepte aus den Bereichen der mikrostrukturierten Hochdurchsatzreaktoren, der parallelen Strömungsrohrreaktoren, der parallelen Satzreaktoren und der photochemischen Parallelreaktoren.

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Metadaten
Titel
Spezielle labortechnische Reaktoren: Hochdurchsatz-Reaktionstechnik
verfasst von
Klaus Stöwe
Copyright-Jahr
2020
Verlag
Springer Berlin Heidelberg
Buch
Handbuch Chemische Reaktoren

Print ISBN: 978-3-662-56433-2

Electronic ISBN: 978-3-662-56434-9

Copyright-Jahr: 2020

DOI
https://doi.org/10.1007/978-3-662-56434-9_45