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Erschienen in: Measurement Techniques 8/2017

28.11.2017 | NANOMETROLOGY

A Dynamic Method of Nanoindentation

verfasst von: V. V. Meshcheryakov, V. V. Maslennikov, E. V. Melekesov

Erschienen in: Measurement Techniques | Ausgabe 8/2017

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Abstract

A new dynamic method of measuring the local value of hardness and contact stiffness at the nanoscale range using a probe in self-oscillation mode at resonant eigenfrequency is proposed. The possibility is shown of measuring the force of contact interaction of a probe with a sample in a range from ten to several hundred μN with shift of the probe’s resonant eigenfrequency, at a resolution up to one hundred nN. The advantage of this method is the absence of a drift component of the measuring signal during the time interval of a test cycle. This ensures operability of the method without special conditions of vibration insulation and thermal insulation that are necessary for instrumental indentation.

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Literatur
1.
Zurück zum Zitat W. C. Oliver and G. M. Pharr, “Measurement of hardness and elastic modulus by instrumented indentation: Advances in understanding and refinements to methodology,” J. Mater. Res., 19, No. 1, 3–20 (2004).ADSCrossRef W. C. Oliver and G. M. Pharr, “Measurement of hardness and elastic modulus by instrumented indentation: Advances in understanding and refinements to methodology,” J. Mater. Res., 19, No. 1, 3–20 (2004).ADSCrossRef
2.
Zurück zum Zitat GOST R 8.748-2011, Measurement of Hardness and Other Characteristics of Materials for Instrumental Indentation. GOST R 8.748-2011, Measurement of Hardness and Other Characteristics of Materials for Instrumental Indentation.
3.
Zurück zum Zitat Yu. I. Golovin, “Nanoindentation and mechanical properties of hard bodies in submicrovolumes, thin surface layers, and films (review),” Fiz. Tverd. Tela, 50, No. 12, 2113–2142 (2008). Yu. I. Golovin, “Nanoindentation and mechanical properties of hard bodies in submicrovolumes, thin surface layers, and films (review),” Fiz. Tverd. Tela, 50, No. 12, 2113–2142 (2008).
4.
Zurück zum Zitat S. A. S. Asif, K. J. Whal, R. J. Colton, and O. L. Warren, “Quantitative imaging of nanoscale mechanical properties using hybrid nanoindentation and force modulation,” J. Appl. Phys., 90, 1192 (2001).ADSCrossRef S. A. S. Asif, K. J. Whal, R. J. Colton, and O. L. Warren, “Quantitative imaging of nanoscale mechanical properties using hybrid nanoindentation and force modulation,” J. Appl. Phys., 90, 1192 (2001).ADSCrossRef
5.
Zurück zum Zitat F. J. Giessibl, F. Piemeier, T. Eguchi, et al., “Comparison of force sensors for atomic force microscopy based on quartz tuning forks and length-extensional resonators,” Phys. Rev. B, 84, 125409 (2011).ADSCrossRef F. J. Giessibl, F. Piemeier, T. Eguchi, et al., “Comparison of force sensors for atomic force microscopy based on quartz tuning forks and length-extensional resonators,” Phys. Rev. B, 84, 125409 (2011).ADSCrossRef
6.
Zurück zum Zitat H. Ooe, M. Fujii, M. Tomitori, and T. Arai, “Evaluation and optimization of quartz resonant-frequency retuned fork force sensors with high Q factors, and the associated electric circuits, for non-contact atomic force microscopy,” Rev. Sci. Instrum., 87, 023702 (2016), doi: https://doi.org/10.1063/1.4941065.ADSCrossRef H. Ooe, M. Fujii, M. Tomitori, and T. Arai, “Evaluation and optimization of quartz resonant-frequency retuned fork force sensors with high Q factors, and the associated electric circuits, for non-contact atomic force microscopy,” Rev. Sci. Instrum., 87, 023702 (2016), doi: https://​doi.​org/​10.​1063/​1.​4941065.ADSCrossRef
9.
Zurück zum Zitat K. V. Gogolinskii, V. N. Reshetov, and A. S. Useinov, “Hardness measurement in submicron and nanometer ranges of linear dimensions,” Mir Izmer., No. 8, 41–47 (2010). K. V. Gogolinskii, V. N. Reshetov, and A. S. Useinov, “Hardness measurement in submicron and nanometer ranges of linear dimensions,” Mir Izmer., No. 8, 41–47 (2010).
10.
Zurück zum Zitat V. V. Meshtcheryakov and A. V. Meshtcheryakov, “Scan speed control for tapping mode SPM,” Nanoscale Res. Lett., 7, No. 1, 121–125 (2012).ADSCrossRef V. V. Meshtcheryakov and A. V. Meshtcheryakov, “Scan speed control for tapping mode SPM,” Nanoscale Res. Lett., 7, No. 1, 121–125 (2012).ADSCrossRef
11.
Zurück zum Zitat D. V. Sivukhin, General Physics Course: Textbook, Vol. I, Mechanics, FIZMATLIT, Moscow (2005). D. V. Sivukhin, General Physics Course: Textbook, Vol. I, Mechanics, FIZMATLIT, Moscow (2005).
12.
Zurück zum Zitat N. M. Krylov and N. N. Bogolyubov, Introduction to Nonlinear Mechanics, Research Center for Regular and Chaotic Dynamics, Moscow, Izhevsk (2004). N. M. Krylov and N. N. Bogolyubov, Introduction to Nonlinear Mechanics, Research Center for Regular and Chaotic Dynamics, Moscow, Izhevsk (2004).
13.
Zurück zum Zitat V. A. Besekerskii and E. I. Popov, Theory of Automatic Control Systems, Izd. Professiya, St. Petersburg (2003). V. A. Besekerskii and E. I. Popov, Theory of Automatic Control Systems, Izd. Professiya, St. Petersburg (2003).
14.
Zurück zum Zitat V. V. Maslennikov, V. V. Meshcheryakov, and E. A. Dovgopolaya, “A method for analyzing ACSes described by a mathematical model with a cubic characteristic equation,” Avtomat. Telemekh., No. 12, 59–69 (2016). V. V. Maslennikov, V. V. Meshcheryakov, and E. A. Dovgopolaya, “A method for analyzing ACSes described by a mathematical model with a cubic characteristic equation,” Avtomat. Telemekh., No. 12, 59–69 (2016).
15.
Zurück zum Zitat Pal Jen Wei and Jen Fin Lin, “Modified method for continuous stiffness measurement,” J. Mater. Res., 24, No. 3, 599–606 (2009). Pal Jen Wei and Jen Fin Lin, “Modified method for continuous stiffness measurement,” J. Mater. Res., 24, No. 3, 599–606 (2009).
Metadaten
Titel
A Dynamic Method of Nanoindentation
verfasst von
V. V. Meshcheryakov
V. V. Maslennikov
E. V. Melekesov
Publikationsdatum
28.11.2017
Verlag
Springer US
Erschienen in
Measurement Techniques / Ausgabe 8/2017
Print ISSN: 0543-1972
Elektronische ISSN: 1573-8906
DOI
https://doi.org/10.1007/s11018-017-1269-1

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