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2020 | OriginalPaper | Buchkapitel

Base Transesterification of Ineffectual Soybean Oil Using Lab Scale Synthesized CaO Catalyst

verfasst von : Rakesh Singh Ningthoujam, Ronaldo Singh Naorem, Denin Singh Langpokpam, Thokchom Subhaschandra Singh, Tikendra Nath Verma

Erschienen in: Advances in Applied Mechanical Engineering

Verlag: Springer Singapore

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Abstract

The present study involves the transesterification of ineffectual soybean oil using synthesized calcinated (duck eggshell) calcium oxide (CaO) as heterogeneous base catalyst. The catalyst was first prepared by exposing at a muffle furnace for about 180 min 800 °C and then characterized using X-ray diffraction (XRD), Fourier transform infrared spectrometry (FT-IR), scanning electron microscopy (SEM) and energy-dispersive x-ray spectroscopy (EDX). There is characterization of uncooked, ineffectual and transesterified ineffectual soybean oil using FT-IR spectrometry. The yield was obtained to be 94.55% when transesterified at 3% (wt%) catalyst loading, 10:1 alcohol to oil ratio, a reaction temperature of 70 °C and a reaction time of 60 min. The methyl ester underwent gas chromatography–mass spectrometer (GC-MS) test to check the contents of the yield oil. It was found that the cheap and ready to be discarded ineffectual soybean oil can be effectively used for producing biodiesel.

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Metadaten
Titel
Base Transesterification of Ineffectual Soybean Oil Using Lab Scale Synthesized CaO Catalyst
verfasst von
Rakesh Singh Ningthoujam
Ronaldo Singh Naorem
Denin Singh Langpokpam
Thokchom Subhaschandra Singh
Tikendra Nath Verma
Copyright-Jahr
2020
Verlag
Springer Singapore
DOI
https://doi.org/10.1007/978-981-15-1201-8_79

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