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2020 | OriginalPaper | Buchkapitel

8. Characterization Techniques

verfasst von : Jose Martin Herrera Ramirez, Raul Perez Bustamante, Cesar Augusto Isaza Merino, Ana Maria Arizmendi Morquecho

Erschienen in: Unconventional Techniques for the Production of Light Alloys and Composites

Verlag: Springer International Publishing

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Abstract

This chapter focuses on the main characterization techniques used for the morphological, microstructural, and structural analysis, as well as for the mechanical behavior analysis of light alloys and composites. There are different characterization techniques available, ranging from the most common and accessible ones to the most sophisticated and, sometimes, not available to everyone. A brief description of all these techniques is provided, presenting some examples of each one to show their capabilities. Additionally, the chapter is intended to inform the reader about the nuances and limitations during the characterization of metal matrix composites. The understanding of the microstructural features, such as the distribution of the reinforcement within the matrix and the interfacial reaction between them, as well as of the mechanical, thermal, and corrosion behavior is necessary during the production of metal matrix composites.

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Literatur
1.
Zurück zum Zitat Armstrong, R., Adams, B. L., & Arnold, M. A. (2018). ASM handbook volume 10, materials characterization. Materials Park: ASM International. Armstrong, R., Adams, B. L., & Arnold, M. A. (2018). ASM handbook volume 10, materials characterization. Materials Park: ASM International.
2.
Zurück zum Zitat Cayless, R.B.C. (1990). ASM handbook volume 2, properties and selection: Nonferrous alloys and special purpose materials. Materials Park, OH: ASM International Cayless, R.B.C. (1990). ASM handbook volume 2, properties and selection: Nonferrous alloys and special purpose materials. Materials Park, OH: ASM International
3.
Zurück zum Zitat Hernandez Robles, F. C., Ramirez, J. M. H., & Mackay, R. (2017). Al-Si alloys: Automotive, aeronautical, and aerospace applications. Cham: Springer. Hernandez Robles, F. C., Ramirez, J. M. H., & Mackay, R. (2017). Al-Si alloys: Automotive, aeronautical, and aerospace applications. Cham: Springer.
4.
Zurück zum Zitat Spierings, A. B., Schneider, M., & Eggenberger, R. (2011). Comparison of density measurement techniques for additive manufactured metallic parts. Rapid Prototyping Journal, 17(5), 380–386. Spierings, A. B., Schneider, M., & Eggenberger, R. (2011). Comparison of density measurement techniques for additive manufactured metallic parts. Rapid Prototyping Journal, 17(5), 380–386.
6.
Zurück zum Zitat Sartorius YDK 01, YDK 01-0D, YDK 01 LP Density Determination Kit User’s Manual. 1998. Sartorius AG: Goettingen, Germany. Sartorius YDK 01, YDK 01-0D, YDK 01 LP Density Determination Kit User’s Manual. 1998. Sartorius AG: Goettingen, Germany.
7.
Zurück zum Zitat Latief, F., & Sherif, E.-S. M. (2012). Effects of sintering temperature and graphite addition on the mechanical properties of aluminum. Journal of Industrial and Engineering Chemistry, 18(6), 2129–2134. Latief, F., & Sherif, E.-S. M. (2012). Effects of sintering temperature and graphite addition on the mechanical properties of aluminum. Journal of Industrial and Engineering Chemistry, 18(6), 2129–2134.
9.
Zurück zum Zitat Du Plessis, A., et al. (2018). Standard method for microCT-based additive manufacturing quality control 2: Density measurement. MethodsX, 5, 1117–1123. Du Plessis, A., et al. (2018). Standard method for microCT-based additive manufacturing quality control 2: Density measurement. MethodsX, 5, 1117–1123.
10.
Zurück zum Zitat Guinebretière, R. (2013). X-ray diffraction by polycrystalline materials. Somerset: Wiley. Guinebretière, R. (2013). X-ray diffraction by polycrystalline materials. Somerset: Wiley.
11.
Zurück zum Zitat Cao, A., et al. (2001). X-ray diffraction characterization on the alignment degree of carbon nanotubes. Chemical Physics Letters, 344(1–2), 13–17. Cao, A., et al. (2001). X-ray diffraction characterization on the alignment degree of carbon nanotubes. Chemical Physics Letters, 344(1–2), 13–17.
12.
Zurück zum Zitat Rietveld, H. M. (2014). The Rietveld method. Physica Scripta, 89(9), 098002. Rietveld, H. M. (2014). The Rietveld method. Physica Scripta, 89(9), 098002.
13.
Zurück zum Zitat Dresselhaus, M. S., et al. (2010). Perspectives on carbon nanotubes and graphene raman spectroscopy. Nano Letters, 10(3), 751–758. Dresselhaus, M. S., et al. (2010). Perspectives on carbon nanotubes and graphene raman spectroscopy. Nano Letters, 10(3), 751–758.
14.
Zurück zum Zitat Dresselhaus, M. S., et al. (2005). Raman spectroscopy of carbon nanotubes. Physics Reports, 409(2), 47–99. Dresselhaus, M. S., et al. (2005). Raman spectroscopy of carbon nanotubes. Physics Reports, 409(2), 47–99.
15.
Zurück zum Zitat Heise, H. M., et al. (2011). Characterization of carbon nanotube filters and other carbonaceous materials by Raman spectroscopy—II: Study on dispersion and disorder parameters. Journal of Raman Spectroscopy, 42(3), 294–302. Heise, H. M., et al. (2011). Characterization of carbon nanotube filters and other carbonaceous materials by Raman spectroscopy—II: Study on dispersion and disorder parameters. Journal of Raman Spectroscopy, 42(3), 294–302.
16.
Zurück zum Zitat Jorio, A., et al. (2001). Structural (n, m) determination of isolated single-wall carbon nanotubes by resonant Raman scattering. Physical Review Letters, 86(6), 1118–1121. Jorio, A., et al. (2001). Structural (n, m) determination of isolated single-wall carbon nanotubes by resonant Raman scattering. Physical Review Letters, 86(6), 1118–1121.
17.
Zurück zum Zitat Lourie, O., & Wagner, H. (1998). Evaluation of Young’s modulus of carbon nanotubes by micro-Raman spectroscopy. Journal of Materials Research, 13(9), 2418–2422. Lourie, O., & Wagner, H. (1998). Evaluation of Young’s modulus of carbon nanotubes by micro-Raman spectroscopy. Journal of Materials Research, 13(9), 2418–2422.
18.
Zurück zum Zitat Goldstein, J. I., et al. (2017). Scanning electron microscopy and X-ray microanalysis. New York: Springer. Goldstein, J. I., et al. (2017). Scanning electron microscopy and X-ray microanalysis. New York: Springer.
19.
Zurück zum Zitat Girão, A. V., Caputo, G., & Ferro, M. C. (2017). Application of scanning electron microscopy–energy dispersive X-ray spectroscopy (SEM-EDS). Comprehensive Analytical Chemistry, 75, 153–168. Girão, A. V., Caputo, G., & Ferro, M. C. (2017). Application of scanning electron microscopy–energy dispersive X-ray spectroscopy (SEM-EDS). Comprehensive Analytical Chemistry, 75, 153–168.
20.
Zurück zum Zitat Abd Mutalib, M., et al. (2017). Chapter 9 – Scanning electron microscopy (SEM) and energy-dispersive X-ray (EDX) spectroscopy. In Membrane characterization (pp. 161–179). Amsterdam: Elsevier. Abd Mutalib, M., et al. (2017). Chapter 9 – Scanning electron microscopy (SEM) and energy-dispersive X-ray (EDX) spectroscopy. In Membrane characterization (pp. 161–179). Amsterdam: Elsevier.
21.
Zurück zum Zitat Lotnyk, A., et al. (2015). Focused high- and low-energy ion milling for TEM specimen preparation. Microelectronics Reliability, 55(9–10), 2119–2125. Lotnyk, A., et al. (2015). Focused high- and low-energy ion milling for TEM specimen preparation. Microelectronics Reliability, 55(9–10), 2119–2125.
22.
Zurück zum Zitat Ünlü, N. (2008). Preparation of high quality Al TEM specimens via a double-jet electropolishing technique. Materials Characterization, 59(5), 547–553. Ünlü, N. (2008). Preparation of high quality Al TEM specimens via a double-jet electropolishing technique. Materials Characterization, 59(5), 547–553.
23.
Zurück zum Zitat Darnbrough, J., Liu, D., & Flewitt, P. (2013). Micro-scale testing of ductile and brittle cantilever beam specimens in situ with a dual beam workstation. Measurement Science and Technology, 24(5), 055010. Darnbrough, J., Liu, D., & Flewitt, P. (2013). Micro-scale testing of ductile and brittle cantilever beam specimens in situ with a dual beam workstation. Measurement Science and Technology, 24(5), 055010.
24.
Zurück zum Zitat Mayer, J., et al. (2007). TEM sample preparation and FIB-induced damage. MRS Bulletin, 32(5), 400–407. Mayer, J., et al. (2007). TEM sample preparation and FIB-induced damage. MRS Bulletin, 32(5), 400–407.
25.
Zurück zum Zitat Williams, D. B., & Carter, C. B. (2009). Transmission electron microscopy: A textbook for materials science. Boston: Springer US. Williams, D. B., & Carter, C. B. (2009). Transmission electron microscopy: A textbook for materials science. Boston: Springer US.
26.
Zurück zum Zitat Liu, M., & Cowley, J. M. (1994). Structures of carbon nanotubes studied by HRTEM and nanodiffraction. Ultramicroscopy, 53(4), 333–342. Liu, M., & Cowley, J. M. (1994). Structures of carbon nanotubes studied by HRTEM and nanodiffraction. Ultramicroscopy, 53(4), 333–342.
27.
Zurück zum Zitat Hofer, F., et al. (2016). Fundamentals of electron energy-loss spectroscopy. In IOP conference series: Materials science and engineering. Bristol: IOP Publishing. Hofer, F., et al. (2016). Fundamentals of electron energy-loss spectroscopy. In IOP conference series: Materials science and engineering. Bristol: IOP Publishing.
28.
Zurück zum Zitat Demoncy, N., et al. (1998). Filling carbon nanotubes with metals by the arc-discharge method: The key role of sulfur. The European Physical Journal B-Condensed Matter and Complex Systems, 4(2), 147–157. Demoncy, N., et al. (1998). Filling carbon nanotubes with metals by the arc-discharge method: The key role of sulfur. The European Physical Journal B-Condensed Matter and Complex Systems, 4(2), 147–157.
29.
Zurück zum Zitat Van der Heide, P. (2011). X-ray photoelectron spectroscopy: An introduction to principles and practices. Hoboken: Wiley. Van der Heide, P. (2011). X-ray photoelectron spectroscopy: An introduction to principles and practices. Hoboken: Wiley.
30.
Zurück zum Zitat Haque, M. A., & Saif, T. (2008). Mechanical testing at the micro/nanoscale. In W. N. Sharpe (Ed.), Springer handbook of experimental solid mechanics. Boston: Springer US. Haque, M. A., & Saif, T. (2008). Mechanical testing at the micro/nanoscale. In W. N. Sharpe (Ed.), Springer handbook of experimental solid mechanics. Boston: Springer US.
31.
Zurück zum Zitat Cree, D., & Pugh, M. (2011). Dry wear and friction properties of an A356/SiC foam interpenetrating phase composite. Wear, 272(1), 88–96. Cree, D., & Pugh, M. (2011). Dry wear and friction properties of an A356/SiC foam interpenetrating phase composite. Wear, 272(1), 88–96.
32.
Zurück zum Zitat Suresh, K., et al. (2013). Sliding wear behavior of gas tunnel type plasma sprayed Ni-based metallic glass composite coatings. Vacuum, 88, 114–117. Suresh, K., et al. (2013). Sliding wear behavior of gas tunnel type plasma sprayed Ni-based metallic glass composite coatings. Vacuum, 88, 114–117.
33.
Zurück zum Zitat Abbas, A., et al. (2020). Tribological effects of carbon nanotubes on magnesium alloy AZ31 and analyzing aging effects on CNTs/AZ31 composites fabricated by stir casting process. Tribology International, 142, 105982. Abbas, A., et al. (2020). Tribological effects of carbon nanotubes on magnesium alloy AZ31 and analyzing aging effects on CNTs/AZ31 composites fabricated by stir casting process. Tribology International, 142, 105982.
34.
Zurück zum Zitat Huang, S. J., Abbas, A., & Ballóková, B. (2019). Effect of CNT on microstructure, dry sliding wear and compressive mechanical properties of AZ61 magnesium alloy. Journal of Materials Research and Technology, 8(5), 4273–4286. Huang, S. J., Abbas, A., & Ballóková, B. (2019). Effect of CNT on microstructure, dry sliding wear and compressive mechanical properties of AZ61 magnesium alloy. Journal of Materials Research and Technology, 8(5), 4273–4286.
35.
Zurück zum Zitat Lim, S., et al. (1999). The tribological properties of Al–Cu/SiCp metal–matrix composites fabricated using the rheocasting technique. Journal of Materials Processing Technology, 89, 591–596. Lim, S., et al. (1999). The tribological properties of Al–Cu/SiCp metal–matrix composites fabricated using the rheocasting technique. Journal of Materials Processing Technology, 89, 591–596.
36.
Zurück zum Zitat Rodrigo, P., et al. (2009). Microstructure and wear resistance of Al–SiC composites coatings on ZE41 magnesium alloy. Applied Surface Science, 255(22), 9174–9181. Rodrigo, P., et al. (2009). Microstructure and wear resistance of Al–SiC composites coatings on ZE41 magnesium alloy. Applied Surface Science, 255(22), 9174–9181.
37.
Zurück zum Zitat Lim, C., Lim, S., & Gupta, M. (2003). Wear behaviour of SiCp-reinforced magnesium matrix composites. Wear, 255(1–6), 629–637. Lim, C., Lim, S., & Gupta, M. (2003). Wear behaviour of SiCp-reinforced magnesium matrix composites. Wear, 255(1–6), 629–637.
38.
Zurück zum Zitat Narayanasamy, P., & Selvakumar, N. (2017). Tensile, compressive and wear behaviour of self-lubricating sintered magnesium based composites. Transactions of Nonferrous Metals Society of China, 27(2), 312–323. Narayanasamy, P., & Selvakumar, N. (2017). Tensile, compressive and wear behaviour of self-lubricating sintered magnesium based composites. Transactions of Nonferrous Metals Society of China, 27(2), 312–323.
39.
Zurück zum Zitat Dash, D., et al. (2020). Influence of TiC on microstructure, mechanical and wear properties of magnesium alloy (AZ91D) matrix composites. Journal of Scientific & Industrial Research, 29, 164–169. Dash, D., et al. (2020). Influence of TiC on microstructure, mechanical and wear properties of magnesium alloy (AZ91D) matrix composites. Journal of Scientific & Industrial Research, 29, 164–169.
40.
Zurück zum Zitat Thirugnanasambandham, T., et al. (2019). Experimental study of wear characteristics of Al2O3 reinforced magnesium based metal matrix composites. Materials Today: Proceedings, 14, 211–218. Thirugnanasambandham, T., et al. (2019). Experimental study of wear characteristics of Al2O3 reinforced magnesium based metal matrix composites. Materials Today: Proceedings, 14, 211–218.
41.
Zurück zum Zitat ASTM. (2017). G99-17 standard test method for wear testing with a pin-on-disk apparatus. West Conshohocken: ASTM International. ASTM. (2017). G99-17 standard test method for wear testing with a pin-on-disk apparatus. West Conshohocken: ASTM International.
42.
Zurück zum Zitat Oliver, W. C., & Pharr, G. M. (1992). An improved technique for determining hardness and elastic modulus using load and displacement sensing indentation experiments. Journal of Materials Research, 7(6), 1564–1586. Oliver, W. C., & Pharr, G. M. (1992). An improved technique for determining hardness and elastic modulus using load and displacement sensing indentation experiments. Journal of Materials Research, 7(6), 1564–1586.
43.
Zurück zum Zitat Laha, T., & Agarwal, A. (2008). Effect of sintering on thermally sprayed carbon nanotube reinforced aluminum nanocomposite. Materials Science and Engineering A, 480(1–2), 323–332. Laha, T., & Agarwal, A. (2008). Effect of sintering on thermally sprayed carbon nanotube reinforced aluminum nanocomposite. Materials Science and Engineering A, 480(1–2), 323–332.
44.
Zurück zum Zitat Duarte, M., et al. (2020). Nanomechanical characterization of a metal matrix composite reinforced with carbon nanotubes. AIMS Materials Science, 7(1), 33–45. Duarte, M., et al. (2020). Nanomechanical characterization of a metal matrix composite reinforced with carbon nanotubes. AIMS Materials Science, 7(1), 33–45.
45.
Zurück zum Zitat Chen, J., & Bull, S. (2006). On the relationship between plastic zone radius and maximum depth during nanoindentation. Surface and Coatings Technology, 201(7), 4289–4293. Chen, J., & Bull, S. (2006). On the relationship between plastic zone radius and maximum depth during nanoindentation. Surface and Coatings Technology, 201(7), 4289–4293.
46.
Zurück zum Zitat Chen, J. (2012). Indentation-based methods to assess fracture toughness for thin coatings. Journal of Physics D: Applied Physics, 45(20), 203001. Chen, J. (2012). Indentation-based methods to assess fracture toughness for thin coatings. Journal of Physics D: Applied Physics, 45(20), 203001.
47.
Zurück zum Zitat ASTM E384-17 standard test method for microindentation hardness of materials. West Conshohocken: ASTM International, 2017. ASTM E384-17 standard test method for microindentation hardness of materials. West Conshohocken: ASTM International, 2017.
48.
Zurück zum Zitat ASTM E399-19 standard test method for linear-elastic plane-strain fracture toughness KIc of metallic materials. West Conshohocken: ASTM International, 2019. ASTM E399-19 standard test method for linear-elastic plane-strain fracture toughness KIc of metallic materials. West Conshohocken: ASTM International, 2019.
Metadaten
Titel
Characterization Techniques
verfasst von
Jose Martin Herrera Ramirez
Raul Perez Bustamante
Cesar Augusto Isaza Merino
Ana Maria Arizmendi Morquecho
Copyright-Jahr
2020
DOI
https://doi.org/10.1007/978-3-030-48122-3_8

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