Skip to main content
Erschienen in: Journal of Materials Engineering and Performance 3/2018

22.01.2018

Coarsening of AA6013-T6 Precipitates During Sheet Warm Forming Applications

verfasst von: M. Di Ciano, S. DiCecco, S. Esmaeili, M. A. Wells, M. J. Worswick

Erschienen in: Journal of Materials Engineering and Performance | Ausgabe 3/2018

Einloggen

Aktivieren Sie unsere intelligente Suche, um passende Fachinhalte oder Patente zu finden.

search-config
loading …

Abstract

The use of warm forming for AA6xxx-T6 sheet is of interest to improve its formability; however, the effect warm forming may have on the coarsening of precipitates and the mechanical strength of these sheets has not been well studied. In this research, the coarsening behavior of AA6013-T6 precipitates has been explored, in the temperature range of 200-300 °C, and time of 30 s up to 50 h. Additionally, the effect of warm deformation on coarsening behavior was explored using: (1) simulated warm forming tests in a Gleeble thermo-mechanical simulator and (2) bi-axial warm deformation tests. Using a strong obstacle model to describe the yield strength (YS) evolution of the AA6013-T6 material, and a Lifshitz, Slyozov, and Wagner (LSW) particle coarsening law to describe the change in precipitate size with time, the coarsening kinetics were modeled for this alloy. The coarsening kinetics in the range of 220-300 °C followed a trend similar to that previously found for AA6111 for the 180-220 °C range. There was strong evidence that coarsening kinetics were not altered due to warm deformation above 220 °C. For warm forming between 200 and 220 °C, the YS of the AA6013-T6 material increased slightly, which could be attributed to strain hardening during warm deformation. Finally, a non-isothermal coarsening model was used to assess the potential reduction in the YS of AA6013-T6 for practical processing conditions related to auto-body manufacturing. The model calculations showed that 90% of the original AA6013-T6 YS could be maintained, for warm forming temperatures up to 280 °C, if the heating schedule used to get the part to the warm forming temperature was limited to 1 min.

Sie haben noch keine Lizenz? Dann Informieren Sie sich jetzt über unsere Produkte:

Springer Professional "Wirtschaft+Technik"

Online-Abonnement

Mit Springer Professional "Wirtschaft+Technik" erhalten Sie Zugriff auf:

  • über 102.000 Bücher
  • über 537 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Finance + Banking
  • Management + Führung
  • Marketing + Vertrieb
  • Maschinenbau + Werkstoffe
  • Versicherung + Risiko

Jetzt Wissensvorsprung sichern!

Springer Professional "Technik"

Online-Abonnement

Mit Springer Professional "Technik" erhalten Sie Zugriff auf:

  • über 67.000 Bücher
  • über 390 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Maschinenbau + Werkstoffe




 

Jetzt Wissensvorsprung sichern!

Literatur
1.
Zurück zum Zitat P.K. Mallick, Ed., Materials, Design and Manufacturing for Lightweight Vehicles, Elsevier, Amsterdam, 2010 P.K. Mallick, Ed., Materials, Design and Manufacturing for Lightweight Vehicles, Elsevier, Amsterdam, 2010
2.
Zurück zum Zitat A. Burnham, Updated Vehicle Specifications in the GREET Vehicle-Cycle Model. Argonne National Laboratory, 2012. A. Burnham, Updated Vehicle Specifications in the GREET Vehicle-Cycle Model. Argonne National Laboratory, 2012.
3.
Zurück zum Zitat S.S. Hecker, Formability of Aluminum Alloy Sheets, J. Eng. Mater. Technol., 1975, 97, p 66–73CrossRef S.S. Hecker, Formability of Aluminum Alloy Sheets, J. Eng. Mater. Technol., 1975, 97, p 66–73CrossRef
4.
Zurück zum Zitat F. Shehata, M.J. Painter, and R. Pearce, The Warm Forming of Aluminium/Magnesium Alloy Sheet, J. Mech. Work. Technol., 1978, 2, p 279–290CrossRef F. Shehata, M.J. Painter, and R. Pearce, The Warm Forming of Aluminium/Magnesium Alloy Sheet, J. Mech. Work. Technol., 1978, 2, p 279–290CrossRef
5.
Zurück zum Zitat R.A. Ayres, H.W. Lanning, B. Taylor, R. Heimbuch, and W.G. Brazier, Warm Forming the GM V-6 Oil Pan in Aluminum, No. 780180. SAE Technical Paper, 1978 R.A. Ayres, H.W. Lanning, B. Taylor, R. Heimbuch, and W.G. Brazier, Warm Forming the GM V-6 Oil Pan in Aluminum, No. 780180. SAE Technical Paper, 1978
6.
Zurück zum Zitat R. Bagheriasl and M.J. Worswick, Formability of AA3003 Brazing Sheet at Elevated Temperatures: Limiting Dome Height Experiments and Determination of Forming Limit Diagrams, Int. J. Mater. Form., 2015, 8, p 229–244CrossRef R. Bagheriasl and M.J. Worswick, Formability of AA3003 Brazing Sheet at Elevated Temperatures: Limiting Dome Height Experiments and Determination of Forming Limit Diagrams, Int. J. Mater. Form., 2015, 8, p 229–244CrossRef
7.
Zurück zum Zitat G. Kamyar, R. Bagheriasl, and M.J. Worswick, Analysis of Nonisothermal Deep Drawing of Aluminum Alloy Sheet with Induced Anisotropy and Rate Sensitivity at Elevated Temperatures, J. Manuf. Sci. Eng., 2014, 136(011006–1), p 16 G. Kamyar, R. Bagheriasl, and M.J. Worswick, Analysis of Nonisothermal Deep Drawing of Aluminum Alloy Sheet with Induced Anisotropy and Rate Sensitivity at Elevated Temperatures, J. Manuf. Sci. Eng., 2014, 136(011006–1), p 16
8.
Zurück zum Zitat W.S. Miller, L. Zhaung, J. Bottema et al., Recent Development in Aluminium Alloys for the Automotive Industry, Mater. Sci. Eng. A, 2000, 280A, p 37–49CrossRef W.S. Miller, L. Zhaung, J. Bottema et al., Recent Development in Aluminium Alloys for the Automotive Industry, Mater. Sci. Eng. A, 2000, 280A, p 37–49CrossRef
9.
Zurück zum Zitat D. Li and A.K. Ghosh, Tensile Deformation Behavior of Aluminum Alloys at Warm Forming Temperatures, Mater. Sci. Eng. A, 2003, 352A, p 279–286CrossRef D. Li and A.K. Ghosh, Tensile Deformation Behavior of Aluminum Alloys at Warm Forming Temperatures, Mater. Sci. Eng. A, 2003, 352A, p 279–286CrossRef
10.
Zurück zum Zitat D. Li and A.K. Ghosh, Biaxial Warm Forming Behavior of Aluminum Sheet Alloys, J. Mater. Process. Technol., 2004, 145, p 281–293CrossRef D. Li and A.K. Ghosh, Biaxial Warm Forming Behavior of Aluminum Sheet Alloys, J. Mater. Process. Technol., 2004, 145, p 281–293CrossRef
11.
Zurück zum Zitat S. Dicecco, C. Butcher, and M.J. Worswick, et al., Determination of Forming Limit Diagrams of AA6013-T6 Aluminum Alloy Sheet Using a Time and Position Dependent Localized Necking Criterion, Proceedings International Deep Drawing Research Group, IDDRG, Linz, Austria, June 12-15, 2016 S. Dicecco, C. Butcher, and M.J. Worswick, et al., Determination of Forming Limit Diagrams of AA6013-T6 Aluminum Alloy Sheet Using a Time and Position Dependent Localized Necking Criterion, Proceedings International Deep Drawing Research Group, IDDRG, Linz, Austria, June 12-15, 2016
12.
Zurück zum Zitat P.E. Krajewski, The Warm Ductility of Commercial Aluminum Alloy Sheets, No. 2005-01-1388. SAE Technical Paper, 2005 P.E. Krajewski, The Warm Ductility of Commercial Aluminum Alloy Sheets, No. 2005-01-1388. SAE Technical Paper, 2005
13.
Zurück zum Zitat S. Esmaeili, D.J. Lloyd, and W.J. Poole, A Yield Strength Model for the Al-Mg-Si-Cu Alloy AA6111, Acta Mater., 2003, 51, p 2243–2257CrossRef S. Esmaeili, D.J. Lloyd, and W.J. Poole, A Yield Strength Model for the Al-Mg-Si-Cu Alloy AA6111, Acta Mater., 2003, 51, p 2243–2257CrossRef
14.
Zurück zum Zitat S. Esmaeili, X. Wang, D.J. Lloyd, and W.J. Poole, On the Precipitation-Hardening Behavior of the Al-Mg-Si-Cu Alloy AA6111, Metall. Mater. Trans. B, 2003, 34A, p 751–763 S. Esmaeili, X. Wang, D.J. Lloyd, and W.J. Poole, On the Precipitation-Hardening Behavior of the Al-Mg-Si-Cu Alloy AA6111, Metall. Mater. Trans. B, 2003, 34A, p 751–763
15.
Zurück zum Zitat S. Esmaeili and D.J. Lloyd, Effect of Composition on Clustering Reactions in AlMgSi (Cu) Alloys, Scr. Mater., 2004, 50, p 155–158CrossRef S. Esmaeili and D.J. Lloyd, Effect of Composition on Clustering Reactions in AlMgSi (Cu) Alloys, Scr. Mater., 2004, 50, p 155–158CrossRef
16.
Zurück zum Zitat S. Esmaeili, D. Vaumousse, M. Zandbergen et al., A Study on the Early-Stage Decomposition in the Al-Mg-Si-Cu Alloy AA6111 by Electrical Resistivity and Three-Dimensional Atom Probe, Philos. Mag., 2007, 87, p 3797–3816CrossRef S. Esmaeili, D. Vaumousse, M. Zandbergen et al., A Study on the Early-Stage Decomposition in the Al-Mg-Si-Cu Alloy AA6111 by Electrical Resistivity and Three-Dimensional Atom Probe, Philos. Mag., 2007, 87, p 3797–3816CrossRef
17.
Zurück zum Zitat S. Pogatscher, H. Antrekowitsch, H. Leitner et al., Influence of the Thermal Route on the Peak-Aged Microstructures in an Al-Mg-Si Aluminum Alloy, Scr. Mater., 2013, 68, p 158–161CrossRef S. Pogatscher, H. Antrekowitsch, H. Leitner et al., Influence of the Thermal Route on the Peak-Aged Microstructures in an Al-Mg-Si Aluminum Alloy, Scr. Mater., 2013, 68, p 158–161CrossRef
18.
Zurück zum Zitat M. Liu, B. Klobes, and K. Maier, On the Age-Hardening of an Al-Zn-Mg-Cu Alloy: A Vacancy Perspective, Scr. Mater., 2011, 64, p 21–24CrossRef M. Liu, B. Klobes, and K. Maier, On the Age-Hardening of an Al-Zn-Mg-Cu Alloy: A Vacancy Perspective, Scr. Mater., 2011, 64, p 21–24CrossRef
19.
Zurück zum Zitat S. Esmaeili, D.J. Lloyd, and W.J. Poole, Modeling of Precipitation Hardening for the Naturally Aged Al-Mg-Si-Cu Alloy AA6111, Acta Mater., 2003, 51, p 3467–3481CrossRef S. Esmaeili, D.J. Lloyd, and W.J. Poole, Modeling of Precipitation Hardening for the Naturally Aged Al-Mg-Si-Cu Alloy AA6111, Acta Mater., 2003, 51, p 3467–3481CrossRef
20.
Zurück zum Zitat X. Wang, S. Esmaeili, and D.J. Lloyd, The Sequence of Precipitation in the Al-Mg-Si-Cu Alloy AA6111, Metall. Mater. Trans. A, 2006, 37A, p 2691–2699CrossRef X. Wang, S. Esmaeili, and D.J. Lloyd, The Sequence of Precipitation in the Al-Mg-Si-Cu Alloy AA6111, Metall. Mater. Trans. A, 2006, 37A, p 2691–2699CrossRef
21.
Zurück zum Zitat S. Esmaeili and D.J. Lloyd, Modeling of Precipitation Hardening in Pre-aged AlMgSi (Cu) Alloys, Acta Mater., 2005, 53, p 5257–5271CrossRef S. Esmaeili and D.J. Lloyd, Modeling of Precipitation Hardening in Pre-aged AlMgSi (Cu) Alloys, Acta Mater., 2005, 53, p 5257–5271CrossRef
22.
Zurück zum Zitat S. Esmaeili, D.J. Lloyd, and W.J. Poole, Effect of Natural Aging on the Resistivity Evolution During Artificial Aging of the Aluminum Alloy AA6111, Mater. Lett., 2005, 59, p 575–577CrossRef S. Esmaeili, D.J. Lloyd, and W.J. Poole, Effect of Natural Aging on the Resistivity Evolution During Artificial Aging of the Aluminum Alloy AA6111, Mater. Lett., 2005, 59, p 575–577CrossRef
23.
Zurück zum Zitat S. Esmaeili and D.J. Lloyd, The Role of Copper in the Precipitation Kinetics of 6000 Series Al Alloys, Mater. Sci. Forum, 2006, 519–521, p 169–176CrossRef S. Esmaeili and D.J. Lloyd, The Role of Copper in the Precipitation Kinetics of 6000 Series Al Alloys, Mater. Sci. Forum, 2006, 519–521, p 169–176CrossRef
24.
Zurück zum Zitat D. Bryant, The Effects of Preaging Treatments on Aging Kinetics and Mechanical Properties in AA6111 Aluminum Autobody Sheet, Metall. Mater. Trans. A, 1999, 30A, p 1999–2006CrossRef D. Bryant, The Effects of Preaging Treatments on Aging Kinetics and Mechanical Properties in AA6111 Aluminum Autobody Sheet, Metall. Mater. Trans. A, 1999, 30A, p 1999–2006CrossRef
25.
Zurück zum Zitat S. Esmaeili and D.J. Lloyd, Characterization of the Evolution of the Volume Fraction of Precipitates in Aged AlMgSiCu Alloys Using DSC Technique, Mater. Charact., 2005, 55, p 307–319CrossRef S. Esmaeili and D.J. Lloyd, Characterization of the Evolution of the Volume Fraction of Precipitates in Aged AlMgSiCu Alloys Using DSC Technique, Mater. Charact., 2005, 55, p 307–319CrossRef
26.
Zurück zum Zitat W.A. Johnson and R.F. Mehl, Reaction Kinetics in Process of Nucleation and Growth, Trans AIME, 1939, 135, p 396–415 W.A. Johnson and R.F. Mehl, Reaction Kinetics in Process of Nucleation and Growth, Trans AIME, 1939, 135, p 396–415
27.
Zurück zum Zitat M. Avrami, Kinetics of Phase Change. I, General Theory, J. Chem. Phys., 1939, 7, p 1103–1112CrossRef M. Avrami, Kinetics of Phase Change. I, General Theory, J. Chem. Phys., 1939, 7, p 1103–1112CrossRef
28.
Zurück zum Zitat A.N. Kolmogorov, On the Statistical Theory of the Crystallization of Metals, Bull. Acad. Sci. USSR Math. Ser., 1937, 1, p 355–359 A.N. Kolmogorov, On the Statistical Theory of the Crystallization of Metals, Bull. Acad. Sci. USSR Math. Ser., 1937, 1, p 355–359
29.
Zurück zum Zitat I.M. Lifshitz and V.V. Slyozov, The Kinetics of Precipitation from Supersaturated Solid Solutions, Phys. Stat. Sol., 1961, 19, p 35–50 I.M. Lifshitz and V.V. Slyozov, The Kinetics of Precipitation from Supersaturated Solid Solutions, Phys. Stat. Sol., 1961, 19, p 35–50
30.
Zurück zum Zitat C.Z. Wagner, Theory of Precipitate Change by Redissolution, Z. Elektrochem., 1961, 65, p 581–591 C.Z. Wagner, Theory of Precipitate Change by Redissolution, Z. Elektrochem., 1961, 65, p 581–591
31.
Zurück zum Zitat M. Kolar, K.O. Pedersen, S. Gulbrandsen-Dahl et al., Effect of Pre-deformation on Mechanical Response of an Artificially Aged Al-Mg-Si Alloy, Mater. Trans., 2011, 52, p 1356–1362CrossRef M. Kolar, K.O. Pedersen, S. Gulbrandsen-Dahl et al., Effect of Pre-deformation on Mechanical Response of an Artificially Aged Al-Mg-Si Alloy, Mater. Trans., 2011, 52, p 1356–1362CrossRef
32.
Zurück zum Zitat K. Teichmann, C.D. Marioara, K.O. Pedersen et al., The Effect of Simultaneous Deformation and Annealing on the Precipitation Behaviour and Mechanical Properties of an Al-Mg-Si Alloy, Mater. Sci. Eng. A, 2003, 565A, p 228–235 K. Teichmann, C.D. Marioara, K.O. Pedersen et al., The Effect of Simultaneous Deformation and Annealing on the Precipitation Behaviour and Mechanical Properties of an Al-Mg-Si Alloy, Mater. Sci. Eng. A, 2003, 565A, p 228–235
33.
Zurück zum Zitat R.S. Yassar, D.P. Field, and H. Weiland, The Effect of Predeformation on the β ″and β′ Precipitates and the Role of Q′ Phase in an Al-Mg-Si Alloy; AA6022, Scr. Mater., 2005, 53, p 299–303CrossRef R.S. Yassar, D.P. Field, and H. Weiland, The Effect of Predeformation on the β ″and β′ Precipitates and the Role of Q′ Phase in an Al-Mg-Si Alloy; AA6022, Scr. Mater., 2005, 53, p 299–303CrossRef
34.
Zurück zum Zitat R.S. Yassar, D.P. Field, and H. Weiland, The Effect of Cold Deformation on the Kinetics of the β″ Precipitates in an Al-Mg-Si Alloy, Metall. Mater. Trans. A, 2005, 36A, p 2059–2065CrossRef R.S. Yassar, D.P. Field, and H. Weiland, The Effect of Cold Deformation on the Kinetics of the β″ Precipitates in an Al-Mg-Si Alloy, Metall. Mater. Trans. A, 2005, 36A, p 2059–2065CrossRef
35.
Zurück zum Zitat ASTM Standard E1097-12, Standard Guide for Determination of Various Elements by Direct Current Plasma Atomic Emission Spectrometry. ASTM International, 2012 ASTM Standard E1097-12, Standard Guide for Determination of Various Elements by Direct Current Plasma Atomic Emission Spectrometry. ASTM International, 2012
36.
Zurück zum Zitat ASTM Standard E8/E8M-11, Standard Test Methods for Tension Testing of Metallic Materials. ASTM International, 2011 ASTM Standard E8/E8M-11, Standard Test Methods for Tension Testing of Metallic Materials. ASTM International, 2011
37.
Zurück zum Zitat H.L. Trajano, J.D. DeMartini, M.H. Studer, and C.E. Wyman, Comparison of the Effectiveness of a Fluidized Sand Bath and a Steam Chamber for Reactor Heating, Ind. Eng. Chem. Res., 2013, 52, p 4932–4938CrossRef H.L. Trajano, J.D. DeMartini, M.H. Studer, and C.E. Wyman, Comparison of the Effectiveness of a Fluidized Sand Bath and a Steam Chamber for Reactor Heating, Ind. Eng. Chem. Res., 2013, 52, p 4932–4938CrossRef
38.
Zurück zum Zitat H.R. Shercliff and M.F. Ashby, A Process Model for Age Hardening of Aluminium Alloys—II. Applications of the Model, Acta Metall. Mater., 1990, 38, p 1803–1812CrossRef H.R. Shercliff and M.F. Ashby, A Process Model for Age Hardening of Aluminium Alloys—II. Applications of the Model, Acta Metall. Mater., 1990, 38, p 1803–1812CrossRef
39.
Zurück zum Zitat J. Go, Modelling the Interaction Between Recovery, Recrystallization and Precipitation in AA6111. University of British Columbia Ph.D. Thesis, Vancouver, Canada, 2006. J. Go, Modelling the Interaction Between Recovery, Recrystallization and Precipitation in AA6111. University of British Columbia Ph.D. Thesis, Vancouver, Canada, 2006.
40.
Zurück zum Zitat T.L. Bergman, F.P. Incropera, and A.S. Lavine, Fundamentals of Heat and Mass Transfer, Wiley, New York, 2011 T.L. Bergman, F.P. Incropera, and A.S. Lavine, Fundamentals of Heat and Mass Transfer, Wiley, New York, 2011
Metadaten
Titel
Coarsening of AA6013-T6 Precipitates During Sheet Warm Forming Applications
verfasst von
M. Di Ciano
S. DiCecco
S. Esmaeili
M. A. Wells
M. J. Worswick
Publikationsdatum
22.01.2018
Verlag
Springer US
Erschienen in
Journal of Materials Engineering and Performance / Ausgabe 3/2018
Print ISSN: 1059-9495
Elektronische ISSN: 1544-1024
DOI
https://doi.org/10.1007/s11665-018-3161-9

Weitere Artikel der Ausgabe 3/2018

Journal of Materials Engineering and Performance 3/2018 Zur Ausgabe

    Marktübersichten

    Die im Laufe eines Jahres in der „adhäsion“ veröffentlichten Marktübersichten helfen Anwendern verschiedenster Branchen, sich einen gezielten Überblick über Lieferantenangebote zu verschaffen.