Skip to main content
Erschienen in: Tribology Letters 3/2013

01.03.2013 | Original Paper

Analysis of AFM Images of Self-Structured Surface Textures by Directional Fractal Signature Method

verfasst von: Marcin Wolski, Pawel Podsiadlo, Gwidon W. Stachowiak

Erschienen in: Tribology Letters | Ausgabe 3/2013

Einloggen

Aktivieren Sie unsere intelligente Suche, um passende Fachinhalte oder Patente zu finden.

search-config
loading …

Abstract

A new method, called augmented blanket with rotating grid (ABRG), has been proposed in our recent work on characterizing roughness and directionality of self-structured surface textures. This is the first method that calculates fractal dimensions (FDs) at individual scales and directions for the entire surface image data and does not require the data to be Brownian fractal. However, before the ABRG method can be used in real applications, effects of atomic force microscope (AFM) imaging conditions on FDs need to be evaluated first. In this paper, computer-generated AFM images with three different resolutions, 48 combinations of tip radii and cone angles, and 15 noise levels were used in the tests. The images represent isotropic self-structured surface textures with small, medium and large motif sizes, and anisotropic surfaces exhibiting two dominating directions. For isotropic surfaces, the ABRG method is not significantly affected (i.e. FDs changes <5 %) by image resolution, tip size (for surfaces with large motifs) and noise (except the level above 8 %). For anisotropic surfaces, the method exhibits large changes in FDs (up to −34 %). The results obtained show that the ABRG method can be effective in analysing the AFM images of self-structured surface textures. However, some precautions should be taken with anisotropic and isotropic surfaces with small motifs.

Sie haben noch keine Lizenz? Dann Informieren Sie sich jetzt über unsere Produkte:

Springer Professional "Wirtschaft+Technik"

Online-Abonnement

Mit Springer Professional "Wirtschaft+Technik" erhalten Sie Zugriff auf:

  • über 102.000 Bücher
  • über 537 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Finance + Banking
  • Management + Führung
  • Marketing + Vertrieb
  • Maschinenbau + Werkstoffe
  • Versicherung + Risiko

Jetzt Wissensvorsprung sichern!

Springer Professional "Technik"

Online-Abonnement

Mit Springer Professional "Technik" erhalten Sie Zugriff auf:

  • über 67.000 Bücher
  • über 390 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Maschinenbau + Werkstoffe




 

Jetzt Wissensvorsprung sichern!

Literatur
1.
Zurück zum Zitat Maboudian, R., Ashurst, W.R., Carraro, C.: Tribological challenges in micromechanical systems. Tribol. Lett. 12, 95–100 (2002)CrossRef Maboudian, R., Ashurst, W.R., Carraro, C.: Tribological challenges in micromechanical systems. Tribol. Lett. 12, 95–100 (2002)CrossRef
2.
Zurück zum Zitat Verma, A., Uzun, O., Hu, Y.H., Hu, Y., Han, H.S., Watson, N., Chen, S.L., Irvine, D.J., Stellacci, F.: Surface structure-regulated cell-membrane penetration by monolayer-protected nanoparticles. Nat. Mater. 7, 588–595 (2008)CrossRef Verma, A., Uzun, O., Hu, Y.H., Hu, Y., Han, H.S., Watson, N., Chen, S.L., Irvine, D.J., Stellacci, F.: Surface structure-regulated cell-membrane penetration by monolayer-protected nanoparticles. Nat. Mater. 7, 588–595 (2008)CrossRef
3.
Zurück zum Zitat Pons-Siepermann, I.C., Glotzer, S.C.: Design of patchy particles using quaternary self-assembled monolayers. ACS Nano 6, 3919–3924 (2012)CrossRef Pons-Siepermann, I.C., Glotzer, S.C.: Design of patchy particles using quaternary self-assembled monolayers. ACS Nano 6, 3919–3924 (2012)CrossRef
4.
Zurück zum Zitat Klutse, C.K., Mayer, A., Wittkamper, J., Cullum, B.M.: Applications of self-assembled monolayers in surface-enhanced Raman scattering. J. Nanotechnol. 2012, Article ID 319038 (2012) Klutse, C.K., Mayer, A., Wittkamper, J., Cullum, B.M.: Applications of self-assembled monolayers in surface-enhanced Raman scattering. J. Nanotechnol. 2012, Article ID 319038 (2012)
5.
Zurück zum Zitat Ahmadi-Kandjani, S., Barille, R., Dabos-Seignon, S., Nunzi, J.M., Ortyl, E., Kucharski, S.: Self-induced diffraction grating storage in polymer films. Mol. Cryst. Liq. Cryst. 446, 99–109 (2006)CrossRef Ahmadi-Kandjani, S., Barille, R., Dabos-Seignon, S., Nunzi, J.M., Ortyl, E., Kucharski, S.: Self-induced diffraction grating storage in polymer films. Mol. Cryst. Liq. Cryst. 446, 99–109 (2006)CrossRef
6.
Zurück zum Zitat Nakano, M.: Tribological properties of self-assembled monolayers. In: Biresaw, G., Mittal, K. (eds.) Surfactants in Tribology, vol. 2, pp. 3–15. CRC Press, Boca Raton (2011)CrossRef Nakano, M.: Tribological properties of self-assembled monolayers. In: Biresaw, G., Mittal, K. (eds.) Surfactants in Tribology, vol. 2, pp. 3–15. CRC Press, Boca Raton (2011)CrossRef
7.
Zurück zum Zitat Kaufmann, C., Mani, G., Marton, D., Johnson, D., Agrawal, C.M.: Long-term stability of self-assembled monolayers on electropolished L605 cobalt chromium alloy for stent applications. J. Biomed. Mater. Res. B: Appl. Biomater. 98B, 280–289 (2011)CrossRef Kaufmann, C., Mani, G., Marton, D., Johnson, D., Agrawal, C.M.: Long-term stability of self-assembled monolayers on electropolished L605 cobalt chromium alloy for stent applications. J. Biomed. Mater. Res. B: Appl. Biomater. 98B, 280–289 (2011)CrossRef
8.
Zurück zum Zitat Kudernac, T., Shabelina, N., Mamdouh, W., Hoger, S., De Feyter, S.: STM visualisation of counterions and the effect of charges on self-assembled monolayers of macrocycles. Beilstein J. Nanotechnol. 2, 674–680 (2011)CrossRef Kudernac, T., Shabelina, N., Mamdouh, W., Hoger, S., De Feyter, S.: STM visualisation of counterions and the effect of charges on self-assembled monolayers of macrocycles. Beilstein J. Nanotechnol. 2, 674–680 (2011)CrossRef
9.
Zurück zum Zitat Hurst, K.M., Ansari, N., Roberts, C.B., Ashurst, W.R.: Self-assembled monolayer-immobilized gold nanoparticles as durable, anti-stiction coatings for MEMS. J. Microelectromech. Syst. 20, 424–435 (2011)CrossRef Hurst, K.M., Ansari, N., Roberts, C.B., Ashurst, W.R.: Self-assembled monolayer-immobilized gold nanoparticles as durable, anti-stiction coatings for MEMS. J. Microelectromech. Syst. 20, 424–435 (2011)CrossRef
10.
Zurück zum Zitat Miyake, K., Hori, Y., Ikeda, T., Asakawa, M., Shimizu, T., Sasaki, S.: Alkyl chain length dependence of the self-organized structure of alkyl-substituted phthalocyanines. Langmuir 24, 4708–4714 (2008)CrossRef Miyake, K., Hori, Y., Ikeda, T., Asakawa, M., Shimizu, T., Sasaki, S.: Alkyl chain length dependence of the self-organized structure of alkyl-substituted phthalocyanines. Langmuir 24, 4708–4714 (2008)CrossRef
11.
Zurück zum Zitat Miyake, K., Fukuta, M., Asakawa, M., Hori, Y., Ikeda, T., Shimizu, T.: Molecular motion of surface-immobilized double-decker phthalocyanine complexes. J. Am. Chem. Soc. 131, 17808–17813 (2009)CrossRef Miyake, K., Fukuta, M., Asakawa, M., Hori, Y., Ikeda, T., Shimizu, T.: Molecular motion of surface-immobilized double-decker phthalocyanine complexes. J. Am. Chem. Soc. 131, 17808–17813 (2009)CrossRef
12.
Zurück zum Zitat Bhushan, B., Kulkarni, A.V., Koinkar, V.N.: Microtribological characterization of self-assembled and Langmuir–Blodgett monolayers by atomic and friction force microscopy. Langmuir 11, 3189–3198 (1995)CrossRef Bhushan, B., Kulkarni, A.V., Koinkar, V.N.: Microtribological characterization of self-assembled and Langmuir–Blodgett monolayers by atomic and friction force microscopy. Langmuir 11, 3189–3198 (1995)CrossRef
13.
Zurück zum Zitat Russell, P., Batchelor, D., Thornton, J.: SEM and AFM: Complementary Techniques for High Resolution Surface Investigations. Bruker Corporation, Billerica (2010) Russell, P., Batchelor, D., Thornton, J.: SEM and AFM: Complementary Techniques for High Resolution Surface Investigations. Bruker Corporation, Billerica (2010)
14.
Zurück zum Zitat Eaton, P., West, P.: Atomic Force Microscopy. Oxford University Press, Oxford (2010) Eaton, P., West, P.: Atomic Force Microscopy. Oxford University Press, Oxford (2010)
15.
Zurück zum Zitat Faucheux, N., Schweiss, R., Lutzow, K., Werner, C., Groth, T.: Self-assembled monolayers with different terminating groups as model substrates for cell adhesion studies. Biomaterials 25, 2721–2730 (2004)CrossRef Faucheux, N., Schweiss, R., Lutzow, K., Werner, C., Groth, T.: Self-assembled monolayers with different terminating groups as model substrates for cell adhesion studies. Biomaterials 25, 2721–2730 (2004)CrossRef
16.
Zurück zum Zitat Zhuang, Y.X., Hansen, O., Knieling, T., Wang, C., Rombach, P., Lang, W., Benecke, W., Kehlenbeck, M., Koblitz, J.: Vapor-phase self-assembled monolayers for anti-stiction applications in MEMS. J. Microelectromech. Syst. 16, 1451–1460 (2007)CrossRef Zhuang, Y.X., Hansen, O., Knieling, T., Wang, C., Rombach, P., Lang, W., Benecke, W., Kehlenbeck, M., Koblitz, J.: Vapor-phase self-assembled monolayers for anti-stiction applications in MEMS. J. Microelectromech. Syst. 16, 1451–1460 (2007)CrossRef
17.
Zurück zum Zitat Losego, M.D., Guske, J.T., Efremenko, A., Maria, J.P., Franzen, S.: Characterizing the molecular order of phosphonic acid self-assembled monolayers on indium tin oxide surfaces. Langmuir 27, 11883–11888 (2011)CrossRef Losego, M.D., Guske, J.T., Efremenko, A., Maria, J.P., Franzen, S.: Characterizing the molecular order of phosphonic acid self-assembled monolayers on indium tin oxide surfaces. Langmuir 27, 11883–11888 (2011)CrossRef
18.
Zurück zum Zitat Yin, J.J., Ye, G., Wang, X.G.: Self-structured surface patterns on molecular azo glass films induced by laser light irradiation. Langmuir 26, 6755–6761 (2010)CrossRef Yin, J.J., Ye, G., Wang, X.G.: Self-structured surface patterns on molecular azo glass films induced by laser light irradiation. Langmuir 26, 6755–6761 (2010)CrossRef
19.
Zurück zum Zitat Wang, X.L., Yin, J.J., Wang, X.G.: Photoinduced self-structured surface pattern on a molecular azo glass film: structure-property relationship and wavelength correlation. Langmuir 27, 12666–12676 (2011)CrossRef Wang, X.L., Yin, J.J., Wang, X.G.: Photoinduced self-structured surface pattern on a molecular azo glass film: structure-property relationship and wavelength correlation. Langmuir 27, 12666–12676 (2011)CrossRef
20.
Zurück zum Zitat Lam, K.T., Ji, L.W.: Fractal analysis of InGaN self-assemble quantum dots grown by MOCVD. Microelectron. J. 38, 905–909 (2007)CrossRef Lam, K.T., Ji, L.W.: Fractal analysis of InGaN self-assemble quantum dots grown by MOCVD. Microelectron. J. 38, 905–909 (2007)CrossRef
21.
Zurück zum Zitat Consolin, N., Leite, F.L., Carvalho, E.R., Venancio, E.C., Vaz, C.M.R., Mattoso, L.H.C.: Study of poly(o-ethoxyaniline) interactions with herbicides and evaluation of conductive polymer potential used in electrochemical sensors. J. Braz. Chem. Soc. 18, 577–584 (2007)CrossRef Consolin, N., Leite, F.L., Carvalho, E.R., Venancio, E.C., Vaz, C.M.R., Mattoso, L.H.C.: Study of poly(o-ethoxyaniline) interactions with herbicides and evaluation of conductive polymer potential used in electrochemical sensors. J. Braz. Chem. Soc. 18, 577–584 (2007)CrossRef
22.
Zurück zum Zitat Wolski, M., Podsiadlo, P., Stachowiak, G.W.: Directional fractal signature analysis of trabecular bone: evaluation of different methods to detect early osteoarthritis in knee radiographs. Proc. Inst. Mech. Eng. H 223, 211–236 (2009) Wolski, M., Podsiadlo, P., Stachowiak, G.W.: Directional fractal signature analysis of trabecular bone: evaluation of different methods to detect early osteoarthritis in knee radiographs. Proc. Inst. Mech. Eng. H 223, 211–236 (2009)
23.
Zurück zum Zitat Wolski, M., Podsiadlo, P., Stachowiak, G.W.: Directional fractal signature analysis of self-structured surface textures. Tribol. Lett. 47, 323–340 (2012)CrossRef Wolski, M., Podsiadlo, P., Stachowiak, G.W.: Directional fractal signature analysis of self-structured surface textures. Tribol. Lett. 47, 323–340 (2012)CrossRef
24.
Zurück zum Zitat Love, J.C., Estroff, L.A., Kriebel, J.K., Nuzzo, R.G., Whitesides, G.M.: Self-assembled monolayers of thiolates on metals as a form of nanotechnology. Chem. Rev. 105, 1103–1169 (2005)CrossRef Love, J.C., Estroff, L.A., Kriebel, J.K., Nuzzo, R.G., Whitesides, G.M.: Self-assembled monolayers of thiolates on metals as a form of nanotechnology. Chem. Rev. 105, 1103–1169 (2005)CrossRef
25.
Zurück zum Zitat Villarrubia, J.S.: Algorithms for scanned probe microscope image simulation, surface reconstruction, and tip estimation. J. Res. Natl. Inst. Stand. Technol. 102, 425–454 (1997)CrossRef Villarrubia, J.S.: Algorithms for scanned probe microscope image simulation, surface reconstruction, and tip estimation. J. Res. Natl. Inst. Stand. Technol. 102, 425–454 (1997)CrossRef
26.
Zurück zum Zitat Russ, J.C.: The Image Processing Handbook. CRC Press, Boca Raton (1999) Russ, J.C.: The Image Processing Handbook. CRC Press, Boca Raton (1999)
27.
Zurück zum Zitat Podsiadlo, P., Stachowiak, G.W.: Scale-invariant analysis of wear particle surface morphology. II. Fractal dimension. Wear 242, 180–188 (2000)CrossRef Podsiadlo, P., Stachowiak, G.W.: Scale-invariant analysis of wear particle surface morphology. II. Fractal dimension. Wear 242, 180–188 (2000)CrossRef
28.
Zurück zum Zitat Simpson, G.J., Sedin, D.L., Rowlen, K.L.: Surface roughness by contact versus tapping mode atomic force microscopy. Langmuir 15, 1429–1434 (1999)CrossRef Simpson, G.J., Sedin, D.L., Rowlen, K.L.: Surface roughness by contact versus tapping mode atomic force microscopy. Langmuir 15, 1429–1434 (1999)CrossRef
29.
Zurück zum Zitat Hristu, R., Stanciu, S., Stanciu, G., Capan, I., Guner, B., Erdogan, M.: Influence of atomic force microscopy acquisition parameters on thin film roughness analysis. Microsc. Res. Technol. 75, 921–927 (2012)CrossRef Hristu, R., Stanciu, S., Stanciu, G., Capan, I., Guner, B., Erdogan, M.: Influence of atomic force microscopy acquisition parameters on thin film roughness analysis. Microsc. Res. Technol. 75, 921–927 (2012)CrossRef
30.
Zurück zum Zitat Mannelquist, A., Almqvist, N., Fredriksson, S.: Influence of tip geometry on fractal analysis of atomic force microscopy images. Appl. Phys. A Mater. Sci. Process. 66, S891–S895 (1998)CrossRef Mannelquist, A., Almqvist, N., Fredriksson, S.: Influence of tip geometry on fractal analysis of atomic force microscopy images. Appl. Phys. A Mater. Sci. Process. 66, S891–S895 (1998)CrossRef
31.
Zurück zum Zitat Klapetek, P., Ohlidal, I., Bilek, J.: Influence of the atomic force microscope tip on the multifractal analysis of rough surfaces. Ultramicroscopy 102, 51–59 (2004)CrossRef Klapetek, P., Ohlidal, I., Bilek, J.: Influence of the atomic force microscope tip on the multifractal analysis of rough surfaces. Ultramicroscopy 102, 51–59 (2004)CrossRef
32.
Zurück zum Zitat Aue, J., DeHosson, J.T.M.: Influence of atomic force microscope tip-sample interaction on the study of scaling behavior. Appl. Phys. Lett. 71, 1347–1349 (1997)CrossRef Aue, J., DeHosson, J.T.M.: Influence of atomic force microscope tip-sample interaction on the study of scaling behavior. Appl. Phys. Lett. 71, 1347–1349 (1997)CrossRef
33.
Zurück zum Zitat Thormann, E., Pettersson, T., Kettle, J., Claesson, P.M.: Probing material properties of polymeric surface layers with tapping mode AFM: which cantilever spring constant, tapping amplitude and amplitude set point gives good image contrast and minimal surface damage? Ultramicroscopy 110, 313–319 (2010)CrossRef Thormann, E., Pettersson, T., Kettle, J., Claesson, P.M.: Probing material properties of polymeric surface layers with tapping mode AFM: which cantilever spring constant, tapping amplitude and amplitude set point gives good image contrast and minimal surface damage? Ultramicroscopy 110, 313–319 (2010)CrossRef
34.
Zurück zum Zitat Westra, K.L., Thomson, D.J.: Effect of tip shape on surface roughness measurements from atomic-force microscopy images of thin-films. J. Vac. Sci. Technol. B 13, 344–349 (1995)CrossRef Westra, K.L., Thomson, D.J.: Effect of tip shape on surface roughness measurements from atomic-force microscopy images of thin-films. J. Vac. Sci. Technol. B 13, 344–349 (1995)CrossRef
Metadaten
Titel
Analysis of AFM Images of Self-Structured Surface Textures by Directional Fractal Signature Method
verfasst von
Marcin Wolski
Pawel Podsiadlo
Gwidon W. Stachowiak
Publikationsdatum
01.03.2013
Verlag
Springer US
Erschienen in
Tribology Letters / Ausgabe 3/2013
Print ISSN: 1023-8883
Elektronische ISSN: 1573-2711
DOI
https://doi.org/10.1007/s11249-012-0088-4

Weitere Artikel der Ausgabe 3/2013

Tribology Letters 3/2013 Zur Ausgabe

    Marktübersichten

    Die im Laufe eines Jahres in der „adhäsion“ veröffentlichten Marktübersichten helfen Anwendern verschiedenster Branchen, sich einen gezielten Überblick über Lieferantenangebote zu verschaffen.