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Erschienen in:

01.02.2012

A physico-chemical characterisation of new raw materials for microcrystalline cellulose manufacturing

verfasst von: Tommi Virtanen, Kirsi Svedström, Seppo Andersson, Laura Tervala, Mika Torkkeli, Matti Knaapila, Nina Kotelnikova, Sirkka Liisa Maunu, Ritva Serimaa

Erschienen in: Cellulose | Ausgabe 1/2012

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Abstract

A detailed physico-chemical characterisation of potential new cellulose sources (rice husk, hemp stalk, and coniferous needles), and microcrystalline cellulose (MCC) manufactured from them, was made in this work. The length and the width of the cellulose crystallites were determined by wide-angle X-ray scattering (WAXS), crystallinities were studied by means of WAXS and solid state cross polarisation magic angle spinning ¹³C nuclear magnetic resonance (NMR) spectroscopy, and the packing and the cross-sectional shape of the microfibrils were determined by small-angle X-ray scattering. When MCC was prepared from rice husks and hemp stalks an acceptable yield was obtained. Crystallinities obtained with solid state NMR spectroscopy and WAXS were highest for MCC prepared from hemp stalks, and lowest for rice husk MCC. The crystallite sizes of MCC samples studied in this work varied more than in those MCC samples which were prepared from conventional plant sources, and crystallite size and cellulose crystallinity were related. When taking into account rather high values of specific surface, hemp stalks and rice husks appear as a promising raw materials for MCC production.

Vorheriger Artikel N-halamines from rice straw

Nächster Artikel Fragment analysis of different size-reduced lignocellulosic pulps by hydrodynamic fractionation

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Titel: A physico-chemical characterisation of new raw materials for microcrystalline cellulose manufacturing
verfasst von: Tommi Virtanen
Kirsi Svedström
Seppo Andersson
Laura Tervala
Mika Torkkeli
Matti Knaapila
Nina Kotelnikova
Sirkka Liisa Maunu
Ritva Serimaa
Publikationsdatum: 01.02.2012
Verlag: Springer Netherlands
Erschienen in: Cellulose / Ausgabe 1/2012
Print ISSN: 0969-0239
Elektronische ISSN: 1572-882X
DOI: https://doi.org/10.1007/s10570-011-9636-6

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