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Cellulose

Erschienen in:

01.08.2012 | Original Paper

Comparing microcrystalline with spherical nanocrystalline cellulose from waste cotton fabrics

verfasst von: Rui Xiong, Xinxing Zhang, Dong Tian, Zehang Zhou, Canhui Lu

Erschienen in: Cellulose | Ausgabe 4/2012

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Abstract

Microcrystalline cellulose (MCC) and spherical nanocrystalline cellulose (SNCC) were successfully prepared from waste cotton fabrics through acid hydrolysis. The comparative analysis of the morphology and structure between the obtained MCC and SNCC was carried out. The SNCC suspension exhibited higher stability than the MCC suspension. Transmission electron microscopy in combination with atomic force microscopy showed that the cellulose nanospheres with average size of 35 nm were achieved, while the average particle size of MCC was 49 μm. The MCC and SNCC had similar functional groups and crystalline structure as confirmed by Fourier transform infrared spectroscopy and X-ray diffraction analysis, respectively. Viscometric average molecular weight measurement and thermo gravimetric analysis indicated that the degree of polymerization and thermal stability of SNCC was lower than that of MCC. These results should improve understanding of the characteristics of MCC and SNCC derived from waste cotton fabrics and lead to many new applications.

Vorheriger Artikel Comparative properties of cellulose nano-crystals from native and mercerized cotton fibers

Nächster Artikel Morphological evolution of curauá fibers under acid hydrolysis

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Titel: Comparing microcrystalline with spherical nanocrystalline cellulose from waste cotton fabrics
verfasst von: Rui Xiong
Xinxing Zhang
Dong Tian
Zehang Zhou
Canhui Lu
Publikationsdatum: 01.08.2012
Verlag: Springer Netherlands
Erschienen in: Cellulose / Ausgabe 4/2012
Print ISSN: 0969-0239
Elektronische ISSN: 1572-882X
DOI: https://doi.org/10.1007/s10570-012-9730-4

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