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Journal of Materials Science

Erschienen in:

01.09.2014

Solvothermal synthesis of magnetite hollow submicrospheres and mesoporous nanoparticles

verfasst von: Xiaolei Wang, Jin Yu, Guimei Shi, Ge Xu, Zhidong Zhang

Erschienen in: Journal of Materials Science | Ausgabe 17/2014

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Abstract

Magnetite hollow submicrospheres and mesoporous nanoparticles have been synthesized by a solvothermal approach with assistant of hexamethylenetetramine (HMT) and poly(vinyl pyrrolidone) (PVP). Experimental results showed that the morphology of magnetite was transformed from hollow to solid submicrospheres with increasing amount of HMT. Moreover, without addition of PVP or appropriate addition of external water, mesoporous nanoparticles were obtained. A probable gaseous bubble template mechanism was proposed for the formation of magnetite hollow and mesoporous nanostructures based on experimental observations. Magnetic measurement results revealed that all of the samples were ferromagnetic at room temperature.

Vorheriger Artikel Dynamic morphology instability in epitaxial ZnO/AZO (aluminum-doped ZnO) core–shell nanowires

Nächster Artikel Wear behavior of Au–ZnO nanocomposite films for electrical contacts

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Titel: Solvothermal synthesis of magnetite hollow submicrospheres and mesoporous nanoparticles
verfasst von: Xiaolei Wang
Jin Yu
Guimei Shi
Ge Xu
Zhidong Zhang
Publikationsdatum: 01.09.2014
Verlag: Springer US
Erschienen in: Journal of Materials Science / Ausgabe 17/2014
Print ISSN: 0022-2461
Elektronische ISSN: 1573-4803
DOI: https://doi.org/10.1007/s10853-014-8323-z

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