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Journal of Nanoparticle Research

Erschienen in:

01.06.2011 | Research Paper

Morphology modification of TiO₂ nanotubes by controlling the starting material crystallite size for chemical synthesis

verfasst von: Jang-Yul Kim, Tohru Sekino, Dong Jin Park, Shun-Ichiro Tanaka

Erschienen in: Journal of Nanoparticle Research | Ausgabe 6/2011

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Abstract

TiO₂ nanotubes (NTs) were prepared by low-temperature chemical synthesis using anatase TiO₂ particles with different crystallite sizes in a NaOH solution followed by water washing and HCl neutralization. The synthesized TiO₂ NTs showed diverse morphologies depending on the starting materials. The crystallite size of TiO₂ raw materials increased with an increase in annealing temperature, and larger TiO₂ NTs, around 31 nm in diameter, were obtained from large raw powder with a crystallite size of 117 nm. X-ray diffraction and Raman spectroscopy revealed that the obtained TiO₂ NT exhibited lower crystallinity; however, Raman vibration seems to be more likely than a rutile structure.

Vorheriger Artikel Synthesis and characterization of hollow nanoparticles of crystalline Gd2O3

Nächster Artikel Self-organization of bimetallic PdAu nanoparticles on SiO2 surface

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Titel: Morphology modification of TiO2 nanotubes by controlling the starting material crystallite size for chemical synthesis
verfasst von: Jang-Yul Kim
Tohru Sekino
Dong Jin Park
Shun-Ichiro Tanaka
Publikationsdatum: 01.06.2011
Verlag: Springer Netherlands
Erschienen in: Journal of Nanoparticle Research / Ausgabe 6/2011
Print ISSN: 1388-0764
Elektronische ISSN: 1572-896X
DOI: https://doi.org/10.1007/s11051-010-9990-6

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