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Journal of Materials Engineering and Performance

Erschienen in:

17.05.2021

Development of Nanocomposite Coating by Hybrid Gas Condensation Process and Magnetron Sputtering Equipment: Electrochemical Characteristics and Surface Analysis

verfasst von: S. A. Salehizadeh, R. Serra, I. Carvalho, A. Cavaleiro, S. Carvalho

Erschienen in: Journal of Materials Engineering and Performance | Ausgabe 6/2021

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Abstract

In the present work, a combination of conventional dc magnetron sputtering technique and gas condensation process was utilized to deposit a Ag–Au/a:C nanocomposite coating for application in stents. Quantitative evaluation of Ag⁺ release to the solution revealed a sharp increase of Ag⁺ releasing in the first 2 days of immersion, which continues but with a slower rate up to 14 days reaching a value close to 50 ppb. Atomic force microscopy surface morphology depicted that the roughness of the coating, S_rms, increases after immersion from 5.86 to 14.22. X-ray photoelectron spectroscopy analysis showed two wide bands at 368.30 and 374.30 eV corresponding to the Ag 3d spin-orbit doublets for non-immersed coating. It was found that the Ag content drops to 5% of the initial concentration as the coating is exposed to artificial urine, due to the high affinity of Ag surface nanoparticles to solution anions. This Ag dissolution to artificial urine is followed by reprecipitating Ag salt clusters with a size less than 3 nm on the surface and the formation of a highly oxidized surface. The formation of the oxidation layer as a result of exposure of the coating to the solution is further confirmed by electrochemical impedance spectroscopy and polarization measurements. It was depicted the resistance of the coating increase from 1.80 to 2.86 MΩ as the coating is immersed into the solution for 14 days. The corrosion potential and corrosion current values collected from the polarization plot of the immersed coating were found to be −0.73 and 0.14, respectively, depicting the protecting character of the coating against the deteriorating solution. It was suggested that the formation of the oxidation layer on the coating surface seals the pores of the coating avoiding solution penetration to the substrate and consequently protecting it against corrosion.

Vorheriger Artikel Development and Characterization of High Emittance and Low-Thickness Plasma Electrolytic Oxidation Coating on Ti6Al4V for Spacecraft Application

Nächster Artikel Nitrogen Incorporation into Ta Thin Films Deposited over Ti6Al4V: A Detailed Material and Surface Characterization

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Titel: Development of Nanocomposite Coating by Hybrid Gas Condensation Process and Magnetron Sputtering Equipment: Electrochemical Characteristics and Surface Analysis
verfasst von: S. A. Salehizadeh
R. Serra
I. Carvalho
A. Cavaleiro
S. Carvalho
Publikationsdatum: 17.05.2021
Verlag: Springer US
Erschienen in: Journal of Materials Engineering and Performance / Ausgabe 6/2021
Print ISSN: 1059-9495
Elektronische ISSN: 1544-1024
DOI: https://doi.org/10.1007/s11665-021-05864-4

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