Skip to main content

2020 | OriginalPaper | Buchkapitel

Metallurgical Analysis of Direct Aging Effect on Tensile and Creep Properties in Inconel 718 Forgings

verfasst von : Alexis Nicolaÿ, Jean-Michel Franchet, Nathalie Bozzolo, Jonathan Cormier

Erschienen in: Superalloys 2020

Verlag: Springer International Publishing

Aktivieren Sie unsere intelligente Suche, um passende Fachinhalte oder Patente zu finden.

search-config
loading …

Abstract

Performing the double aging thermal treatment on Inconel 718 forged components directly after forging instead of the standard thermal treatment sequence including a solution annealing step before the double aging is known to be beneficial to mechanical properties. In this work, this so-called direct aging (DA) effect has been assessed for tensile properties at room temperature and for creep properties at 650 °C/750 MPa. Mechanical characteristics obtained on direct aged specimens are compared to those obtained on specimens submitted to the standard thermal treatment sequence (i.e., including a solution heat treatment) and tested in the same conditions. The classical effect of direct aging thermal treatment is obtained; better tensile and creep properties are reached for DA specimens. However, contrary to what is generally assumed, fine microstructural characterizations in specimen threads reveal that the direct aging effect cannot be attributed to a higher residual strain hardening level preserved in the microstructure. It is actually shown that its beneficial effect on mechanical properties is due to a lower δ phase content obtained in microstructures having undergone such a treatment rather than the standard sequence. On the one hand, it has indeed been demonstrated that, counter-intuitively, the δ phase content actually increased during the “solution” treatment performed at 955 °C for 1 h. On the other hand, the relationship between mechanical properties and microstructural features (grain size, δ phase content, residual forging strain hardening level) has been analyzed in detail, and differences in mechanical behavior are mainly controlled by this increased amount of δ phase which deteriorates the mechanical properties. On the contrary, no significant effect of residual forging strain hardening on tensile and creep properties has been found for the investigated conditions.

Sie haben noch keine Lizenz? Dann Informieren Sie sich jetzt über unsere Produkte:

Springer Professional "Wirtschaft+Technik"

Online-Abonnement

Mit Springer Professional "Wirtschaft+Technik" erhalten Sie Zugriff auf:

  • über 102.000 Bücher
  • über 537 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Finance + Banking
  • Management + Führung
  • Marketing + Vertrieb
  • Maschinenbau + Werkstoffe
  • Versicherung + Risiko

Jetzt Wissensvorsprung sichern!

Springer Professional "Technik"

Online-Abonnement

Mit Springer Professional "Technik" erhalten Sie Zugriff auf:

  • über 67.000 Bücher
  • über 390 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Maschinenbau + Werkstoffe




 

Jetzt Wissensvorsprung sichern!

Literatur
1.
Zurück zum Zitat Texier D, Gómez AC, Pierret S, Franchet JM, Pollock TM, Villechaise P, Cormier J (2016) Microstructural Features Controlling the Variability in Low-Cycle Fatigue Properties of Alloy Inconel 718DA at Intermediate Temperature. Metall. Mater. Trans. A. 47:1096–1109. Texier D, Gómez AC, Pierret S, Franchet JM, Pollock TM, Villechaise P, Cormier J (2016) Microstructural Features Controlling the Variability in Low-Cycle Fatigue Properties of Alloy Inconel 718DA at Intermediate Temperature. Metall. Mater. Trans. A. 47:1096–1109.
2.
Zurück zum Zitat Williams JC, Starke Jr EA (2003) Progress in structural materials for aerospace systems. Acta Mat. 51:5775–5799. Williams JC, Starke Jr EA (2003) Progress in structural materials for aerospace systems. Acta Mat. 51:5775–5799.
3.
Zurück zum Zitat Paulonis D, Oblack J, Duvall D (1969) Precipitation in nickel-base alloy 718. Transactions of the ASM 62 611–622. Paulonis D, Oblack J, Duvall D (1969) Precipitation in nickel-base alloy 718. Transactions of the ASM 62 611–622.
4.
Zurück zum Zitat Oblak JM, Paulonis DF, Duvall DS (1974) Coherency strengthening in Ni base alloys hardened by DO22 γ” precipitates. Metallurgical Transactions 5(1):143–153. Oblak JM, Paulonis DF, Duvall DS (1974) Coherency strengthening in Ni base alloys hardened by DO22 γ” precipitates. Metallurgical Transactions 5(1):143–153.
5.
Zurück zum Zitat Han Y, Deb P, Chaturvedi MC (1982) Coarsening behaviour of γ” and γ’ particles in Inconel alloy 718. Metal Science 16:555–562. Han Y, Deb P, Chaturvedi MC (1982) Coarsening behaviour of γ” and γ’ particles in Inconel alloy 718. Metal Science 16:555–562.
6.
Zurück zum Zitat Chaturvedi MC, Han Y (1983) Strengthening mechanisms in Inconel 718 superalloy. Metal Science 17:145–149. Chaturvedi MC, Han Y (1983) Strengthening mechanisms in Inconel 718 superalloy. Metal Science 17:145–149.
7.
Zurück zum Zitat Fayman YC (1987) Microstructural characterization and elemental partitioning in a direct-aged superalloy (DA 718). Materials Science and Engineering 92:159–171. Fayman YC (1987) Microstructural characterization and elemental partitioning in a direct-aged superalloy (DA 718). Materials Science and Engineering 92:159–171.
8.
Zurück zum Zitat Horvath W et al. (2001) The effectiveness of direct ageing on Inconel 718 forgings produced at high strain rates as obtained on a screw press. Paper presented at the 5th international symposium on Superalloys 718, 625, 706 and Various Derivatives, Pittsburgh, Pennsylvania, 17–20 June 2001. Horvath W et al. (2001) The effectiveness of direct ageing on Inconel 718 forgings produced at high strain rates as obtained on a screw press. Paper presented at the 5th international symposium on Superalloys 718, 625, 706 and Various Derivatives, Pittsburgh, Pennsylvania, 17–20 June 2001.
9.
Zurück zum Zitat Schafrik RE et al. (2001) Application of alloy 718 in GE aircraft engines: past, present and next five years. Paper presented at the 5th international symposium on Superalloys 718, 625, 706 and Various Derivatives, Pittsburgh, Pennsylvania, 17–20 June 2001. Schafrik RE et al. (2001) Application of alloy 718 in GE aircraft engines: past, present and next five years. Paper presented at the 5th international symposium on Superalloys 718, 625, 706 and Various Derivatives, Pittsburgh, Pennsylvania, 17–20 June 2001.
10.
Zurück zum Zitat Theska F, Stanojevic A, Oberwinkler B, Ringer SP, Primig S (2018) On conventional versus direct ageing of Alloy 718. Acta Mat. 156:116–124. Theska F, Stanojevic A, Oberwinkler B, Ringer SP, Primig S (2018) On conventional versus direct ageing of Alloy 718. Acta Mat. 156:116–124.
11.
Zurück zum Zitat Oberwinkler B et al. (2016) Integrated process modeling for the mechanical properties optimization of Direct Aged alloy 718 engine disks. Paper presented at the 13th international symposium of Superalloys, Seven Springs, Pennsylvania, 11–15 September 2016. Oberwinkler B et al. (2016) Integrated process modeling for the mechanical properties optimization of Direct Aged alloy 718 engine disks. Paper presented at the 13th international symposium of Superalloys, Seven Springs, Pennsylvania, 11–15 September 2016.
12.
Zurück zum Zitat Guedou JY et al. (1994) Development of damage tolerant Inco 718 for high temperature usage. Paper presented at the 3rd international symposium on Superalloys 718, 625, 706 and Various Derivatives, Pittsburgh, Pennsylvania, 27–29 June 1994. Guedou JY et al. (1994) Development of damage tolerant Inco 718 for high temperature usage. Paper presented at the 3rd international symposium on Superalloys 718, 625, 706 and Various Derivatives, Pittsburgh, Pennsylvania, 27–29 June 1994.
13.
Zurück zum Zitat Nicolaÿ A, Franchet JM, Cormier J, Mansour H, De Graef M, Seret A, Bozzolo N (2019) Discrimination of dynamically and post-dynamically recrystallized grains based on EBSD data: application to Inconel 718. JOM 273:135–147. Nicolaÿ A, Franchet JM, Cormier J, Mansour H, De Graef M, Seret A, Bozzolo N (2019) Discrimination of dynamically and post-dynamically recrystallized grains based on EBSD data: application to Inconel 718. JOM 273:135–147.
14.
Zurück zum Zitat Seret A, Moussa C, Bernacki M, Signorelli R, Bozzolo N (2019) Estimation of geometrically necessary dislocation density from filtered EBSD data by a local linear adaptation of smoothing splines. J. Appl. Crystallogr. 52:548–563. Seret A, Moussa C, Bernacki M, Signorelli R, Bozzolo N (2019) Estimation of geometrically necessary dislocation density from filtered EBSD data by a local linear adaptation of smoothing splines. J. Appl. Crystallogr. 52:548–563.
15.
Zurück zum Zitat Nicolaÿ A, Fiorucci G, Franchet JM, Cormier J, Bozzolo N (2019) Influence of strain rate on subsolvus dynamic and post-dynamic recrystallization kinetics of Inconel 718. Acta Mat. 174:406–417. Nicolaÿ A, Fiorucci G, Franchet JM, Cormier J, Bozzolo N (2019) Influence of strain rate on subsolvus dynamic and post-dynamic recrystallization kinetics of Inconel 718. Acta Mat. 174:406–417.
16.
Zurück zum Zitat Cheng M, Zhang HY, Zhang SH (2012) Microstructure evolution of delta-processed IN718 during holding period after hot deformation. J. Mater. Sci. 47:251–256. Cheng M, Zhang HY, Zhang SH (2012) Microstructure evolution of delta-processed IN718 during holding period after hot deformation. J. Mater. Sci. 47:251–256.
17.
Zurück zum Zitat Humphreys J, Rohrer GS, Rollett A, (2017) The Structure and Energy of Grain Boundaries. In: Recrystallization and Related Annealing Phenomena (Third Edition), Elsevier, p 109–143. Humphreys J, Rohrer GS, Rollett A, (2017) The Structure and Energy of Grain Boundaries. In: Recrystallization and Related Annealing Phenomena (Third Edition), Elsevier, p 109–143.
18.
Zurück zum Zitat Guest RP et al. (2005) The Dynamic and Metadynamic Recrystallisation of IN 718. Paper presented at the 6th international symposium on Superalloys 718, 625, 706 and Various Derivatives, Pittsburgh, Pennsylvania, 2–5 October 2005. Guest RP et al. (2005) The Dynamic and Metadynamic Recrystallisation of IN 718. Paper presented at the 6th international symposium on Superalloys 718, 625, 706 and Various Derivatives, Pittsburgh, Pennsylvania, 2–5 October 2005.
19.
Zurück zum Zitat He DG, Lin YC, Chen MS, Li L (2017) Kinetics equations and microstructural evolution during metadynamic recrystallization in a nickel-based superalloy with δ phase. J. Alloys Compd. 690:971–978. He DG, Lin YC, Chen MS, Li L (2017) Kinetics equations and microstructural evolution during metadynamic recrystallization in a nickel-based superalloy with δ phase. J. Alloys Compd. 690:971–978.
20.
Zurück zum Zitat Wang Y, Shao WZ, Zhen L, Zhang XM (2008) Microstructure evolution during dynamic recrystallization of hot deformed superalloy 718. Mater. Sci. Eng. A 486:321–332. Wang Y, Shao WZ, Zhen L, Zhang XM (2008) Microstructure evolution during dynamic recrystallization of hot deformed superalloy 718. Mater. Sci. Eng. A 486:321–332.
21.
Zurück zum Zitat Park NK, Kim IS, Na YS, Yeom JT (2001) Hot forging of a nickel-base superalloy. J. Mater. Process. Technol. 111:98–102. Park NK, Kim IS, Na YS, Yeom JT (2001) Hot forging of a nickel-base superalloy. J. Mater. Process. Technol. 111:98–102.
22.
Zurück zum Zitat Zhou LX, Baker TN (1994) Effects of strain rate and temperature on deformation behaviour of IN 718 during high temperature deformation. Mater. Sci. Eng. A 177:1–9. Zhou LX, Baker TN (1994) Effects of strain rate and temperature on deformation behaviour of IN 718 during high temperature deformation. Mater. Sci. Eng. A 177:1–9.
23.
Zurück zum Zitat Lin YC, He DG, Chen MS, Chen XM, Zhao CY, Ma X, Long ZL (2016) EBSD analysis of evolution of dynamic recrystallization grains and δ phase in a nickel-based superalloy during hot compressive deformation. Mater. Des. 97:13–24. Lin YC, He DG, Chen MS, Chen XM, Zhao CY, Ma X, Long ZL (2016) EBSD analysis of evolution of dynamic recrystallization grains and δ phase in a nickel-based superalloy during hot compressive deformation. Mater. Des. 97:13–24.
24.
Zurück zum Zitat Desvallées Y et al. (1994) Delta phase in Inconel 718: mechanical properties and forging process requirements. Paper presented at the 3rd international symposium on Superalloys 718, 625, 706 and Various Derivatives, Pittsburgh, Pennsylvania, 27–29 June 1994. Desvallées Y et al. (1994) Delta phase in Inconel 718: mechanical properties and forging process requirements. Paper presented at the 3rd international symposium on Superalloys 718, 625, 706 and Various Derivatives, Pittsburgh, Pennsylvania, 27–29 June 1994.
25.
Zurück zum Zitat Li S et al. (1994) The effect of δ-phase on crack propagation under creep and fatigue conditions in alloy 718. Paper presented at the 3rd international symposium on Superalloys 718, 625, 706 and Various Derivatives, Pittsburgh, Pennsylvania, 27–29 June 1994. Li S et al. (1994) The effect of δ-phase on crack propagation under creep and fatigue conditions in alloy 718. Paper presented at the 3rd international symposium on Superalloys 718, 625, 706 and Various Derivatives, Pittsburgh, Pennsylvania, 27–29 June 1994.
26.
Zurück zum Zitat Takahashi T et al. (1997) Effects of grain boundary precipitation on creep rupture properties of alloys 706 and 718 turbine disk forging. Paper presented at the 4th international symposium on Superalloys 718, 625, 706 and Various Derivatives, Pittsburgh, Pennsylvania, 15–18 June 1997. Takahashi T et al. (1997) Effects of grain boundary precipitation on creep rupture properties of alloys 706 and 718 turbine disk forging. Paper presented at the 4th international symposium on Superalloys 718, 625, 706 and Various Derivatives, Pittsburgh, Pennsylvania, 15–18 June 1997.
27.
Zurück zum Zitat Valle LCM, Araujo LS, Gabriel SB, Dille J, De Almeida LH (2013) The effect of δ phase on the mechanical properties of an Inconel 718 superalloy. J. of Mater. Sci. Eng. and Perf. 22:1512–1518. Valle LCM, Araujo LS, Gabriel SB, Dille J, De Almeida LH (2013) The effect of δ phase on the mechanical properties of an Inconel 718 superalloy. J. of Mater. Sci. Eng. and Perf. 22:1512–1518.
28.
Zurück zum Zitat Anderson M, Thielin AL, Bridier F, Bocher P, Savoie J (2017) δ phase precipitation in Inconel 718 and associated mechanical properties. Mater. Sci. Eng. A 679:48–55. Anderson M, Thielin AL, Bridier F, Bocher P, Savoie J (2017) δ phase precipitation in Inconel 718 and associated mechanical properties. Mater. Sci. Eng. A 679:48–55.
29.
Zurück zum Zitat Krol T, Baither D, Nembach E (2004) The formation of precipitate free zones along grain boundaries in a superalloy and the ensuing effects on its plastic deformation. Acta mat. 52:2095–2108. Krol T, Baither D, Nembach E (2004) The formation of precipitate free zones along grain boundaries in a superalloy and the ensuing effects on its plastic deformation. Acta mat. 52:2095–2108.
Metadaten
Titel
Metallurgical Analysis of Direct Aging Effect on Tensile and Creep Properties in Inconel 718 Forgings
verfasst von
Alexis Nicolaÿ
Jean-Michel Franchet
Nathalie Bozzolo
Jonathan Cormier
Copyright-Jahr
2020
DOI
https://doi.org/10.1007/978-3-030-51834-9_54

    Marktübersichten

    Die im Laufe eines Jahres in der „adhäsion“ veröffentlichten Marktübersichten helfen Anwendern verschiedenster Branchen, sich einen gezielten Überblick über Lieferantenangebote zu verschaffen.