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Optical and Quantum Electronics
Erschienen in: Optical and Quantum Electronics 1/2024

01.01.2024

Physical and electrochemical properties of ammonium nickel phosphate by hydrothermal synthesis: phase transition from nickel phosphide to ammonium nickel phosphate

verfasst von: Ehsan Farahi, Nafiseh Memarian

Erschienen in: Optical and Quantum Electronics | Ausgabe 1/2024

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Abstract

In this paper, one step synthesis of ammonium nickel phosphate hydrate (ANP) by hydrothermal method has been studied. Here we have used red phosphorus and nickel chloride as precursors. This is the first time that the synthesis of ANP using red phosphorus precursor is reported. The addition of a certain amount of HMT surfactant caused a phase transition from Ni2P to ANP. The XRD analysis along with the Raman spectroscopy confirmed the complete formation of the ANP phase without any impurity or secondary phase. The morphological analysis revealed a complete change of morphology from nanostructures to microplates by the addition of HMT. ANP sample showed a reasonably high specific surface area which makes it a convenient material for electrochemical activities. The energy storage performance of this compound was studied by different electrochemical analyses such as CV, GCD, and EIS. The ANP sample showed a reasonably high specific capacitance of 587.4 Fg−1 at 1 Ag−1. Low charge resistance and high specific capacitance make this compound suitable as a cathode material for energy storage systems specially in supercapacitors.
Vorheriger Artikel Fine band gap tuning via Sr incorporated PbTiO3 for optoelectronic application: a DFT study
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Metadaten
Titel
Physical and electrochemical properties of ammonium nickel phosphate by hydrothermal synthesis: phase transition from nickel phosphide to ammonium nickel phosphate
verfasst von
Ehsan Farahi
Nafiseh Memarian
Publikationsdatum
01.01.2024
Verlag
Springer US
Erschienen in
Optical and Quantum Electronics / Ausgabe 1/2024
Print ISSN: 0306-8919
Elektronische ISSN: 1572-817X
DOI
https://doi.org/10.1007/s11082-023-05776-8

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